The content of the invention
The object of the present invention is to provide a kind of method, this method can carry out effective evaluation to interleaving agent, and evaluate knot
Fruit can directly apply to scene.
To achieve these goals, the present invention provides a kind of human-cutting high slope interleaving agent evaluation method, and this method includes:Determine
The physical characteristic of the interleaving agent, the physical characteristic include the compatibility with fracturing fluid;In the definite interleaving agent and the pressure
Split liquid compatibility it is good in the case of, detect floating/subsidence velocity of the interleaving agent in the fracturing fluid;Determine described
Block intensity in the stratum of interleaving agent;And output evaluation result.
Further, the floating/subsidence velocity of the interleaving agent is average speed, wherein, by record it is described every
The average speed is calculated from the time of particle floating/sinking a distance in the fracturing fluid of agent.
Further, intensity is blocked on the stratum for determining the interleaving agent includes:The fracturing fluid is set to flow through by described
The interlayer of interleaving agent composition;And determine that intensity δ is blocked on the stratum of the interleaving agent by below equation2:
Wherein, δ1Intensity, V are blocked for the interleaving agent under experiment condition1For the stream of the fracturing fluid under experiment condition
Speed, μ1The viscosity after the interleaving agent, V are flowed through for the fracturing fluid under experiment condition2For the stream of the fracturing fluid under formation condition
Body flow velocity, and μ2For the viscosity after the excessively described interleaving agent of formation condition fracturing liquid stream.
Further, this method further includes:Detect described in pressure difference and measurement that the fracturing fluid is flowed through before and after the interlayer
The thickness of interlayer;And block intensity δ by what below equation determined the interleaving agent under experiment condition1:
δ1=Δ P/L,
Wherein, Δ P is that the fracturing fluid flows through pressure difference before and after the interlayer, and the thickness that L is the interlayer.
Further, the formation condition is simulated by heating and pressurizeing to the experiment condition.
Further, the physical characteristic of the interleaving agent further includes at least one of person:The mesh number of the interleaving agent, body
Density and real density.
Further, the fracturing fluid is the base fluid configured by guar gum and water.
Further, the base fluid concentration is at least one of person:0.1%th, 0.15%, 0.2%, 0.25% and 0.3%.
Through the above technical solutions, physical characteristic evaluation, floating/lower settling velocity can be carried out to interleaving agent synthesis to be evaluated
Intensity evaluation is evaluated and blocked to degree, so that effective evaluation is carried out to interleaving agent, and evaluation method considers the application on stratum
Environment, therefore the result evaluated can directly apply to scene.
Other features and advantages of the present invention will be described in detail in subsequent specific embodiment part.
Embodiment
The embodiment of the present invention is described in detail below in conjunction with attached drawing.It should be appreciated that this place is retouched
The embodiment stated is merely to illustrate and explain the present invention, and is not intended to limit the invention.
Fig. 1 is a kind of human-cutting high slope interleaving agent evaluation method flow chart of embodiment according to the present invention.As shown in Figure 1,
The human-cutting high slope interleaving agent evaluation method that embodiment of the present invention provides, including:S101, determines that the physics of the interleaving agent is special
Property, which includes the compatibility with fracturing fluid;S102, it is good in the compatibility for determining the interleaving agent and the fracturing fluid
In the case of good, floating/subsidence velocity of the interleaving agent in the fracturing fluid is detected;S103, determines the interleaving agent
Block intensity in stratum;And S104, export evaluation result.Through the above technical solutions, interleaving agent to be evaluated can be integrated
Carry out physical characteristic evaluation, floating/subsidence velocity evaluation and block intensity evaluation, so that effective evaluation is carried out to interleaving agent,
And evaluation method considers the application environment on stratum(Temperature and pressure), therefore the result evaluated can directly apply to scene.
In embodiments, the fracturing fluid used in evaluation method according to the present invention can be to be configured by guar gum and water
Base fluid.For example, guar gum base fluid concentration can be at least one of person:0.1%th, 0.15%, 0.2%, 0.25% and 0.3%.Pass through
Floating/subsidence velocity of interleaving agent to be measured is detected in the guar gum base fluid of various concentrations, can verify that the comprehensive performance of interleaving agent
And applicability.
In evaluation procedure progress, after certain density interleaving agent adds base fluid, the most particle meeting of interleaving agent
Container bottom or liquid level are deposited or floated up to fast speed.And since the particle diameter of every kind of interleaving agent is there may be difference, cause
Sink between the particle of single interleaving agent or ascent rate difference can be very big.And be possible to occur between particle unite sinking or
Rising phenomenon, so as to accelerate sinking or the ascent rate of interleaving agent.These situations are brought to the measurement of interleaving agent float-and-sink rate
Difficulty.Therefore, in a preferred embodiment, floating/subsidence velocity of interleaving agent can be average speed, wherein it is possible to
The time of particle floating/sinking a distance in the fracturing fluid by recording the interleaving agent is average fast to calculate this
Degree.Spent total time is moved a certain distance by recording most of particles, asks for average speed, though the average speed cannot
The sedimentation of accurate reaction interleaving agent or floating rule, but can be referred to as one, can be from macroscopically characterizing different interleaving agents
Sinking or ascent rate.
The principle of the present invention is further illustrated below by a specific embodiment.
In embodiments, using human-cutting high slope interleaving agent evaluation method provided by the invention to following four interleaving agent into
Row evaluation, wherein, in floating agent:S1 is the floating agent of certain oil field production, and S2 is the hollow glass micropearl of certain company production;Sink
In agent:X1 is 80/100 mesh haydite, and X2 is 100/120 mesh haydite.
It is possible, firstly, to made with the base fluid that guar gum and clear water configuration concentration are respectively 0.1%, 0.15%, 0.2%, 0.25%, 0.3%
For fracturing fluid.Capillary viscosimeter can be used to measure the viscosity of each guar gum concentration base fluid.The guar gum base fluid of various concentrations is corresponding
Viscosity is as shown in table 1.
Table 1
Physical method can be utilized, be determined by experiment the physical characteristic of above-mentioned interleaving agent, i.e., volume density, real density, with
And their compatibilities under room temperature and formation temperature conditions with fracturing fluid, measurement result are as shown in table 2.
Table 2
Title |
Mesh number |
Volume density g/cm3 |
Real density g/cm3 |
With fracturing fluid compatibility |
S1 |
5~180 |
0.70 |
0.90 |
It is good |
S2 |
16~50 |
0.52 |
0.83 |
It is good |
X1 |
80/100 |
1.75 |
2.65 |
It is good |
X2 |
100/120 |
1.85 |
2.81 |
It is good |
For the interleaving agent good with the compatibility of fracturing fluid, can continue to detect its floating/sinking in fracturing fluid
Speed.For that then cannot can eliminate or be evaluated as not can be selected with the interleaving agent of fracturing fluid excellent fit 5.Detection interleaving agent exists
Floating/subsidence velocity in fracturing fluid can be carried out by way of experiment.Experiment can select common instrument, for example, electric
Sub- balance, glass bar, magnetic stirring apparatus, beaker, graduated cylinder, stopwatch etc..It can be detected in the following way:To filling guar gum
A certain concentration is added inside the graduated cylinder of base fluid(Sand ratio)Heavy formula/floating diversion agent(That is interleaving agent), stirred evenly with glass bar
Afterwards, the time sunk/floated needed for certain distance with stopwatch record interleaving agent, sinking/ascent rate is calculated.Isolation can be changed
Agent concentration repeats the above process, and the concentration of change guar gum base fluid repeats the above process.It can be drawn using the data measured
Floating/subsidence velocity and guar gum concentration and interleaving agent concentration relationship curve are as shown in Figure 2.
From figure 2 it can be seen that interleaving agent sinking/ascent rate is reduced with the increase of guar gum base fluid concentration, its
In, the subsidence velocity of sinking agent X1 is better than X2, and the ascent rate of floating agent S1 is better than S2.It is exemplified below and how determines difference
Interleaving agent blocks intensity.
Fig. 3 is the apparatus structure schematic diagram for implementing human-cutting high slope interleaving agent evaluation method provided by the invention.Fig. 3 is shown
The core flow test instrument that can be used is detected to the intensity of blocking of interleaving agent, can be included:Constant flow pump 1, intermediate receptacle
2nd, pressure gauge 3, confined pressure pump 4, metering device 5, confined pressure pipe 8 and the hollow cylinder container 6 for being provided at both ends with steel column plug 7.It is above-mentioned
Element is connected by pipeline, and valve is provided with pipeline.Interleaving agent to be measured wherein is placed in hollow cylinder container 6, the open circles
Column container 6 and the contact surface of steel column plug 7 can be provided with strainer.Working status by controlling confined pressure pump 4 can be with analog isolation
The state of agent, for example, corresponding to the natural packing state of interleaving agent when being not added with confined pressure, the hollow cylindrical chamber 6 when applying confined pressure
Middle interleaving agent rock core length L can reduce.Can be to pipeline, steel column and strainer under the conditions of same traffic by pressure gauge 3
Pressure difference measures.
In embodiments, can utilize device four kinds of interleaving agents of detection shown in Fig. 3 blocks intensity, by detecting
Fracturing fluid is stated to flow through the pressure difference before and after interleaving agent interlayer and measure the thickness of the interlayer;And pass through below equation(1)Determine
The interleaving agent blocks intensity δ under experiment condition1:
δ1=Δ P/L(1)
Wherein, Δ P is that the fracturing fluid flows through pressure difference before and after the interlayer, and the thickness that L is the interlayer(Or section
It is long).It is as shown in table 3 that what four kinds of interleaving agents measured under experimental conditions blocks intensity.
Table 3
Wherein, independent test line and strainer additional pressure drop, can obtain additional pressure drop, for example, 1.2KPa.In table
Blocking in intensity for 3 calculating, subtracts the pressure drop that pipeline and strainer add.
According to Darcy's law(2):
Wherein, Q is the flow under given pressure difference, and L is experiment interleaving agent rock core length, and μ is fracturing fluid viscosity, and Δ p is real
Pressure difference is tested, and A is interleaving agent rock core cross-sectional area.
Measured above by experiment and block intensity under experiment condition.Can be to the screening of interleaving agent under experiment condition
Gear intensity, which be converted under formation condition, blocks intensity.Utilize Darcy formula, it is assumed that 1m interleaving agents produce in stratum
Pressure drop is δ 2, and it is δ 1 that intensity is blocked under experiment condition, then can obtain following equation(3):
Wherein, δ1Intensity, V are blocked for interleaving agent under experiment condition1For the flow velocity of experiment condition fracturing liquid, μ1For reality
Fracturing fluid flows through the viscosity after interleaving agent, V under the conditions of testing2For the fluid flow rate of formation condition fracturing liquid, and μ2For stratum bar
Part fracturing liquid stream crosses the viscosity after interleaving agent.In embodiments, can be by being heated to experiment condition(Such as to open circles
Column container 6 heats)And pressurization(Such as to hollow cylinder container 6 plus confined pressure)To simulate to obtain formation condition.
Herein, slabbing seam morphological Simulation result is approximately assumed over the ground.According to professional software(Such as Fracpro-PT
Software)To the analog result of Different Strata condition, it is 42m that crack can be reduced to major semiaxis, the ellipse that semi-minor axis is about 20m
Model, and assume that fluid is equal along crack periphery percolation flow velocity in seam, finally combines the fluid efficiency that scene provides, can estimate
The percolation flow velocity of fluid in stratum.
Calculating based on the model hypothesis, when pump note discharge capacity is 3m3During/min, edge of crack liquid flow velocity in stratum
V2=98.3cm/min, flow velocity V during experiment test1=1.132cm/min, experiment condition fracturing liquid stream cross the viscosity after interleaving agent
μ1=3.04mPa·s(It can be taken as 3mPas), formation condition fracturing liquid can be obtained by heating and pressurizeing to experiment condition
It is about 2mPas by the filtrate viscosity after interleaving agent, so blocking intensity in stratum the multiple of intensity being blocked with ground and be about
52 times, can obtain interleaving agent under formation condition accordingly blocks intensity, is shown in Table 4.
Table 4
Integrated comparative sinking speed understands that floating agent S1 and sinking agent X2 positive effects are better than other two kinds with intensity is blocked
Interleaving agent(It is big to block intensity, isolation effect is good, and interleaving agent is more excellent), so as to obtain the isolation for being adapted to onsite application by evaluation
Agent.Then, the dosage of interleaving agent can further combined with the Fracturing design software analog result of specialty, be calculated.
The preferred embodiment of the present invention is described in detail above in association with attached drawing, still, the present invention is not limited to above-mentioned reality
The detail in mode is applied, in the range of the technology design of the present invention, a variety of letters can be carried out to technical scheme
Monotropic type, for example, interleaving agent interlayer or interleaving agent rock core, these simple variants belong to protection scope of the present invention.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance
In the case of shield, it can be combined by any suitable means.In order to avoid unnecessary repetition, the present invention to it is various can
The combination of energy no longer separately illustrates.
In addition, various embodiments of the present invention can be combined randomly, as long as it is without prejudice to originally
The thought of invention, it should equally be considered as content disclosed in this invention.