CN105018790A - Preparation method of medical graphene enhanced titanium alloy bars - Google Patents
Preparation method of medical graphene enhanced titanium alloy bars Download PDFInfo
- Publication number
- CN105018790A CN105018790A CN201510476617.5A CN201510476617A CN105018790A CN 105018790 A CN105018790 A CN 105018790A CN 201510476617 A CN201510476617 A CN 201510476617A CN 105018790 A CN105018790 A CN 105018790A
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- Prior art keywords
- titanium alloy
- rod bar
- solution
- alloy rod
- powder
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 229910001069 Ti alloy Inorganic materials 0.000 title claims abstract description 78
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 19
- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 19
- 238000005242 forging Methods 0.000 claims abstract description 42
- 238000000576 coating method Methods 0.000 claims abstract description 22
- 238000005507 spraying Methods 0.000 claims abstract description 16
- 238000010438 heat treatment Methods 0.000 claims abstract description 10
- 239000000243 solution Substances 0.000 claims description 58
- 239000000843 powder Substances 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 30
- 238000001816 cooling Methods 0.000 claims description 24
- 238000009413 insulation Methods 0.000 claims description 24
- 238000000034 method Methods 0.000 claims description 23
- 239000011248 coating agent Substances 0.000 claims description 21
- 239000007789 gas Substances 0.000 claims description 20
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 claims description 20
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 16
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 16
- 230000007547 defect Effects 0.000 claims description 16
- 239000010936 titanium Substances 0.000 claims description 16
- 229910052719 titanium Inorganic materials 0.000 claims description 13
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 12
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 12
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 12
- 239000003513 alkali Substances 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- 230000008569 process Effects 0.000 claims description 12
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 claims description 12
- 239000007921 spray Substances 0.000 claims description 12
- 241000252506 Characiformes Species 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 10
- 235000021110 pickles Nutrition 0.000 claims description 10
- 229940001516 sodium nitrate Drugs 0.000 claims description 10
- 235000010344 sodium nitrate Nutrition 0.000 claims description 10
- 239000004317 sodium nitrate Substances 0.000 claims description 10
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 8
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 8
- 239000000084 colloidal system Substances 0.000 claims description 8
- 239000008367 deionised water Substances 0.000 claims description 8
- 238000007598 dipping method Methods 0.000 claims description 8
- 230000004927 fusion Effects 0.000 claims description 8
- 238000005554 pickling Methods 0.000 claims description 8
- FZHAPNGMFPVSLP-UHFFFAOYSA-N silanamine Chemical compound [SiH3]N FZHAPNGMFPVSLP-UHFFFAOYSA-N 0.000 claims description 8
- 238000007669 thermal treatment Methods 0.000 claims description 8
- 239000010955 niobium Substances 0.000 claims description 7
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 6
- 229910052684 Cerium Inorganic materials 0.000 claims description 6
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 6
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 claims description 6
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 6
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 6
- 239000004411 aluminium Substances 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 6
- 239000007864 aqueous solution Substances 0.000 claims description 6
- UREZNYTWGJKWBI-UHFFFAOYSA-M benzethonium chloride Chemical compound [Cl-].C1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 UREZNYTWGJKWBI-UHFFFAOYSA-M 0.000 claims description 6
- 229910052796 boron Inorganic materials 0.000 claims description 6
- 229910052804 chromium Inorganic materials 0.000 claims description 6
- 239000011651 chromium Substances 0.000 claims description 6
- 229910052733 gallium Inorganic materials 0.000 claims description 6
- 229910052735 hafnium Inorganic materials 0.000 claims description 6
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims description 6
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Substances C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 claims description 6
- 229910052742 iron Inorganic materials 0.000 claims description 6
- 229910052758 niobium Inorganic materials 0.000 claims description 6
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims description 6
- 230000003647 oxidation Effects 0.000 claims description 6
- 238000007254 oxidation reaction Methods 0.000 claims description 6
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 239000011775 sodium fluoride Substances 0.000 claims description 6
- 235000013024 sodium fluoride Nutrition 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 229910052715 tantalum Inorganic materials 0.000 claims description 6
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims description 6
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 6
- 229910052720 vanadium Inorganic materials 0.000 claims description 6
- 239000010456 wollastonite Substances 0.000 claims description 6
- 229910052882 wollastonite Inorganic materials 0.000 claims description 6
- 229910052726 zirconium Inorganic materials 0.000 claims description 6
- 229910002804 graphite Inorganic materials 0.000 claims description 5
- 239000010439 graphite Substances 0.000 claims description 5
- -1 graphite alkene Chemical class 0.000 claims description 5
- 229910052582 BN Inorganic materials 0.000 claims description 4
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 4
- 239000004593 Epoxy Substances 0.000 claims description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 4
- 239000006004 Quartz sand Substances 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- 238000010306 acid treatment Methods 0.000 claims description 4
- 230000032683 aging Effects 0.000 claims description 4
- 238000005275 alloying Methods 0.000 claims description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 4
- 239000012159 carrier gas Substances 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 239000000470 constituent Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 238000001035 drying Methods 0.000 claims description 4
- 238000011010 flushing procedure Methods 0.000 claims description 4
- 230000033444 hydroxylation Effects 0.000 claims description 4
- 238000005805 hydroxylation reaction Methods 0.000 claims description 4
- 238000002347 injection Methods 0.000 claims description 4
- 239000007924 injection Substances 0.000 claims description 4
- 238000005461 lubrication Methods 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 238000000465 moulding Methods 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 4
- 239000001301 oxygen Substances 0.000 claims description 4
- 229910052760 oxygen Inorganic materials 0.000 claims description 4
- 238000002161 passivation Methods 0.000 claims description 4
- 238000007750 plasma spraying Methods 0.000 claims description 4
- 238000005488 sandblasting Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000006104 solid solution Substances 0.000 claims description 4
- 239000002904 solvent Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 229910021642 ultra pure water Inorganic materials 0.000 claims description 4
- 239000012498 ultrapure water Substances 0.000 claims description 4
- 238000010792 warming Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 4
- 230000000415 inactivating effect Effects 0.000 claims description 2
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 claims 2
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims 2
- 239000000463 material Substances 0.000 abstract description 8
- 229910045601 alloy Inorganic materials 0.000 abstract description 6
- 239000000956 alloy Substances 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 5
- 210000000988 bone and bone Anatomy 0.000 abstract description 4
- 238000005457 optimization Methods 0.000 abstract 1
- 210000001519 tissue Anatomy 0.000 abstract 1
- 239000010408 film Substances 0.000 description 6
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 5
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 3
- 238000005260 corrosion Methods 0.000 description 3
- 239000007943 implant Substances 0.000 description 3
- 239000010409 thin film Substances 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000001338 self-assembly Methods 0.000 description 2
- 206010061218 Inflammation Diseases 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000017423 tissue regeneration Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Landscapes
- Materials For Medical Uses (AREA)
- Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
Abstract
Description
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CN201510476617.5A CN105018790B (en) | 2015-08-06 | 2015-08-06 | A kind of preparation method of medical graphite alkene enhancing titanium alloy rod bar |
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CN201510476617.5A CN105018790B (en) | 2015-08-06 | 2015-08-06 | A kind of preparation method of medical graphite alkene enhancing titanium alloy rod bar |
Publications (2)
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CN105018790A true CN105018790A (en) | 2015-11-04 |
CN105018790B CN105018790B (en) | 2017-12-19 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108249422A (en) * | 2018-03-02 | 2018-07-06 | 武汉理工大学 | The rapid generation of graphene film surface metalation pad |
CN108342615A (en) * | 2018-03-06 | 2018-07-31 | 青岛可健可康负离子技术有限公司 | A kind of preparation method of anion emission needle |
CN112342419A (en) * | 2020-09-23 | 2021-02-09 | 华南理工大学 | Method for preparing TiC reinforced titanium-based composite material based on cross-linked modified sintered titanium hydride |
Citations (6)
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CN101658693A (en) * | 2008-08-25 | 2010-03-03 | 中国科学院上海硅酸盐研究所 | Magnesium silicate coat-titanium or titanium alloy hard tissue substituting material and preparation method thereof |
CN101709474A (en) * | 2009-11-26 | 2010-05-19 | 攀钢集团江油长城特殊钢有限公司 | Alkali-acid washing method for titanium alloy |
CN101724764A (en) * | 2009-12-10 | 2010-06-09 | 中南大学 | Process for preparing biomedical beta-titanium alloy |
CN103320734A (en) * | 2013-06-26 | 2013-09-25 | 西安赛特金属材料开发有限公司 | Production method of medical fine-grain titanium/titanium alloy bar |
CN103757676A (en) * | 2013-12-11 | 2014-04-30 | 中国航空工业标准件制造有限责任公司 | Pyrophosphate electrocoppering method of titanium alloy |
CN104018145A (en) * | 2014-06-11 | 2014-09-03 | 上海交通大学 | Method for preparing graphene film on surface of titanium alloy |
-
2015
- 2015-08-06 CN CN201510476617.5A patent/CN105018790B/en active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101658693A (en) * | 2008-08-25 | 2010-03-03 | 中国科学院上海硅酸盐研究所 | Magnesium silicate coat-titanium or titanium alloy hard tissue substituting material and preparation method thereof |
CN101709474A (en) * | 2009-11-26 | 2010-05-19 | 攀钢集团江油长城特殊钢有限公司 | Alkali-acid washing method for titanium alloy |
CN101724764A (en) * | 2009-12-10 | 2010-06-09 | 中南大学 | Process for preparing biomedical beta-titanium alloy |
CN103320734A (en) * | 2013-06-26 | 2013-09-25 | 西安赛特金属材料开发有限公司 | Production method of medical fine-grain titanium/titanium alloy bar |
CN103757676A (en) * | 2013-12-11 | 2014-04-30 | 中国航空工业标准件制造有限责任公司 | Pyrophosphate electrocoppering method of titanium alloy |
CN104018145A (en) * | 2014-06-11 | 2014-09-03 | 上海交通大学 | Method for preparing graphene film on surface of titanium alloy |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108249422A (en) * | 2018-03-02 | 2018-07-06 | 武汉理工大学 | The rapid generation of graphene film surface metalation pad |
CN108249422B (en) * | 2018-03-02 | 2020-01-14 | 武汉理工大学 | Method for quickly generating metallized welding point on surface of graphene film |
CN108342615A (en) * | 2018-03-06 | 2018-07-31 | 青岛可健可康负离子技术有限公司 | A kind of preparation method of anion emission needle |
CN108342615B (en) * | 2018-03-06 | 2019-05-31 | 青岛可健可康负离子技术有限公司 | A kind of preparation method of anion emission needle |
CN112342419A (en) * | 2020-09-23 | 2021-02-09 | 华南理工大学 | Method for preparing TiC reinforced titanium-based composite material based on cross-linked modified sintered titanium hydride |
CN112342419B (en) * | 2020-09-23 | 2022-04-15 | 华南理工大学 | Method for preparing TiC reinforced titanium-based composite material based on cross-linked modified sintered titanium hydride |
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CN105018790B (en) | 2017-12-19 |
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