CN105018723A - Chemical combination and efficient filter pressing device in manganese electrolysis process - Google Patents
Chemical combination and efficient filter pressing device in manganese electrolysis process Download PDFInfo
- Publication number
- CN105018723A CN105018723A CN201510396116.6A CN201510396116A CN105018723A CN 105018723 A CN105018723 A CN 105018723A CN 201510396116 A CN201510396116 A CN 201510396116A CN 105018723 A CN105018723 A CN 105018723A
- Authority
- CN
- China
- Prior art keywords
- chemical combination
- pipe
- inlet pipe
- way tap
- pressing device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Structures Of Non-Positive Displacement Pumps (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
The invention discloses a chemical combination and efficient filter pressing device in a manganese electrolysis process. The device comprises an inlet pipe, an outlet pipe, two centrifugal pumps and two filter presses, wherein the inlet pipe is branched into two pipes; one of the two pipes is connected with the outlet pipe by one three-way cock and one centrifugal pump; and the other one of the two pipes is connected with the outlet pipe by the other centrifugal pump and another three-way cock; the two three-way cocks are vertically communicated by a middle connecting pipe; the inlet pipe is connected with a manganese solution flowing tank; the flowing tank has an inverted conical bottom structure; the two filter presses are connected with the outlet pipe by the three-way cocks after parallel connection; and the flowing tank is connected with an air blowing chemical combination barrel. The device skillfully uses two three-way cocks for realizing free switching operation of serial and parallel connection of the centrifugal pumps, improves the filter pressing efficiency, and has the characteristics of simple structure and difficult generation of operation errors; the conical bottom of the flowing tank facilitates to output manganese solution and ore slag; and the air blowing chemical combination barrel skillfully uses a gas ring body consisting of a conical surface ring and a screen hole cylindrical surface ring, so that the oxygen dissolving capacity of the chemical combination barrel is greatly improved, the implementation of an oxidation reaction and the subsequent electrolysis operation are facilitated.
Description
Technical field
The present invention relates to the chemical combination in a kind of electrolytic manganese process and efficient filter-pressing device.
Background technology
Electrolytic manganese carries out by manganese ore pulverizing, chemical combination, removal of impurities, carries out the hydrometallurgy process of electrolysis after allotment again, and wherein chemical combination is exactly, in chemical combination bucket, manganese mineral powder pulp is added the process that sulfuric acid carries out chemical reaction.Chemical combination can obtain solubility manganous sulfate, is convenient to the electrolysis procedure carrying out the later stage.
At present; the chemical combination bucket volume of commercial application can reach hundreds of cubes, needs, to blasting air in chemical combination bucket to the spilling of the oxygenolysis and part obnoxious flavour material that realize some impurity, to be both conducive to protection of the environment in chemical combination process; also realize electrolytic solution to refine, be conducive to the efficient electrolysis in later stage.
But chemical combination bucket blasts air carries out removal of impurities reaction by the less conditionality of concentration of oxygen gas, so generally take mass flow air to blast in actual applications, and take multitube chemical combination bottom of the barrel to import accelerating oxidation effect, but also there is large, the inefficient defect of energy consumption.Therefore, the dissolved oxygen ability improving chemical combination bucket seems extremely important.
Need after chemical combination completes to remove solid slag by press filtration, to obtain the solution needed for electrolysis.Therefore, press filtration is also very important unit step in electrolytic manganese process.
Press filtration in electrolytic manganese process, general is all plate and frame(type)filter press, and select impeller pump as filter pressing pump, pressure-filtering process obtains filtrate, filter residue progressively runs up to optimal filling degree in pressure filter simultaneously, carry out respective handling again, finally complete the cyclical operation process of filter residue cleaning, the object of press filtration realizes solid-liquid separation exactly.In the starting stage of press filtration operation, owing to being complete empty in pressure filter, concerning filter pressing pump, the quick large discharge input carrying out less lift is the ideal operation state of now press filtration operation; But increase along with filter cake accumulates rear resistance in pressure filter, when particularly stopping close to press filtration, have peak pressure expanded state, therefore, larger lift can be had to be to best requirement by the press filtration performance of pressure filter in press filtration the second half.
But in press filtration operation, existing impeller pump all cannot adapt to such process automatically, reaches efficient, high-quality ideal operation state.When general impeller pump carries out press filtration operation, be all that the early stage lift of press filtration is lower, but flow is large, makes motor be in overload, especially easily motor damage; To the press filtration middle and later periods, press filtration resistance strengthens rapidly, and the flow quantity of impeller pump reduces rapidly, although at this moment motor is operated in the low power state of underloading, efficiency of press filtering is very low; Although filter pressing pump has H-Max output state, because pressing filtering liquid flow is less, the serviceability of pressure filter cannot be given full play to and increase work efficiency.
Therefore, impeller pump is made to coordinate pressure filter, the press filtration whole process in electrolytic manganese process is made all to reach ideal operation state, the optimum performance playing press filtration is difficult to realize, if but look for another way, adopt the free shifter of two impeller pump series and parallels to complete press filtration work, make it in press filtration in early days by two impeller pump parallel connections, realize fast, less energy-consumption, the efficient press filtration of large discharge; In press filtration, two impeller pumps are connected by latter stage, obtain high-lift transport capacity, after meeting, journey press filtration resistance is large, but still applicable flow can be had to embody efficient press filtration and give full play to the feature of pressure filter performance, so free shifter of two impeller pump series and parallels is adopted to break through pressure filtering technique bottleneck in electrolytic manganese process, reach the ideal operation state of press filtration, there is the actual application value of particularly important.
Summary of the invention
The technical problem to be solved in the present invention overcomes the deficiencies in the prior art exactly, chemical combination in a kind of electrolytic manganese process and efficient filter-pressing device are provided, this apparatus structure is simple, practical, the series and parallel that can realize two centrifugal pump device freely switches, and chemical combination process dissolved oxygen works very well, dissolved oxygen, oxidizing reaction are thoroughly quick, several times more efficient than traditional way.
For overcoming the deficiencies in the prior art, the present invention takes following technical scheme:
Chemical combination in a kind of electrolytic manganese process and efficient filter-pressing device, comprise inlet pipe, go out pipe, two impeller pumps and two pressure filter, it is characterized in that: inlet pipe branches into two pipelines, article one, pipeline is connected pipe through three-way tap with impeller pump, and another pipeline is connected pipe through another impeller pump with another three-way tap; The upper and lower UNICOM of union in two three-way tap warps; Inlet pipe connects manganese solution chute, and chute has the bottom construction of back taper; Connect pipe through three-way tap after two pressure filter parallel connections, three-way tap controls the closed of two parallel branches and disconnects; Chute connects air blast chemical combination bucket.
Described air blast chemical combination bucket comprises staving, motor and step-down gear and stir shaft, and stir shaft inserts in staving, and motor and step-down gear drive stir shaft to rotate, and stir shaft is fixed with Double-layer stirring paddle; Be provided with the compression ring body that taper-face ring and sieve aperture cylinder ring are formed in staving, aspiration tube front end is fixed on compression ring body, and aspiration tube venting port is at the inner higher place of compression ring body.
Be provided with spout bottom described staving, spout connects output control valve.
This device, by swivel tee cock, can realize freely switching of two impeller pump series and parallel structures, the press filtration in electrolytic manganese process can be made to operate and reach optimum Working; Air blast chemical combination bucket greatly improves the dissolved oxygen ability of chemical combination bucket, is conducive to the carrying out of oxidizing reaction and follow-up electrolysis procedure.
Compared with prior art, beneficial effect of the present invention is also:
The optimum working performance reaching impeller pump needed for press filtration in electrolytic manganese process is switched by the series and parallel of impeller pump; The free blocked operation of series and parallel of two impeller pumps is achieved by rationally succinct circuit design and three-way tap; Compared with the series and parallel pipeline valve shifter of routine, threeway plug valve can greatly reduce the consumption of pipeline and valve, and simplifies the blocked operation of series and parallel, avoids the mistake occurred in common pipe valve system series and parallel handoff procedure; The chute cone end of back taper, be conducive to the outflow of manganese solution; The break-make of three-way tap to two press filtration branch roads in parallel can control arbitrarily, and convenient degree will outclass valve; Air blast chemical combination barrel structure is simple, practical, and the ingenious compression ring body utilizing taper-face ring and sieve aperture cylinder ring to form, greatly improves the dissolved oxygen ability of chemical combination bucket, be conducive to the carrying out of oxidizing reaction and follow-up electrolysis procedure.
Structure of the present invention is simple, and cost is low, practical, has a extensive future.
Accompanying drawing explanation
Fig. 1 is parallel-connection structure schematic diagram of the present invention.
Fig. 2 is cascaded structure schematic diagram of the present invention.
Fig. 3 is the two dimensional structure schematic diagram of air blast chemical combination bucket.
In figure, each label represents:
1, inlet pipe; 2, pipe is gone out; 3, middle union; 4, three-way tap; 5, three-way tap; 6, impeller pump; 7, impeller pump; 24, manganese solution chute; 30, pressure filter; 41, motor and step-down gear; 42, stir shaft; 43, stirring rake; 44, staving; 45, spout; 46, output control valve; 47, aspiration tube; 48, taper-face ring; 49, sieve aperture cylinder ring; 50, aspiration tube venting port.
Embodiment
Now by reference to the accompanying drawings, the present invention is illustrated further.
Chemical combination as shown in Figure 1, Figure 2 and Figure 3 in electrolytic manganese process and efficient filter-pressing device, comprise inlet pipe 1, two impeller pumps (6,7), go out pipe 2 and two pressure filter 30, inlet pipe 1 branches into two pipelines, article one, pipeline is connected pipe 2 through three-way tap 4 with impeller pump 7, and another pipeline is connected pipe 2 through another impeller pump 6 with another three-way tap 5; Union about 3 UNICOM in two three-way tap 4,5 warps; Inlet pipe 1 connects manganese solution chute 24, and chute 24 has the bottom construction of back taper; Connect pipe 2 through three-way tap after the parallel connection of two pressure filter 30, three-way tap controls the closed of two parallel branches and disconnects; Chute 24 connects air blast chemical combination bucket.
Described air blast chemical combination bucket comprises staving 44, motor and step-down gear 41 and stir shaft 42, and stir shaft 42 inserts in staving 44, and motor and step-down gear 41 drive stir shaft 42 to rotate, and stir shaft are fixed with Double-layer stirring paddle 43; Be provided with the compression ring body that taper-face ring 48 is formed with sieve aperture cylinder ring 49 in staving, aspiration tube 7 front end is fixed on compression ring body, and aspiration tube venting port 50 is at the inner higher place of compression ring body.
Be provided with spout 45 bottom described staving 44, spout 45 connects output control valve 46.
Fig. 1 and Fig. 2 is same device different states, and the manganese solution chute cone end is conducive to manganese solution and pulverous slag delivers into pressure filter 30.
Fig. 1 is impeller pump 6,7 conveyance fluid in parallel, and the first branch road of inlet pipe 1 is for connecting impeller pump 6, and impeller pump 6 goes out the lower end of pipe union three way cock 5, is merged into out pipe 2 from upper end; Second branch road of water inlet pipe 1 is enter impeller pump 7 after union three way cock 4, and export through pressurization, be incorporated in out pipe 2, realize two branch road two parallel pumps, carry out large discharge output, middle union 3 is blocking state.
After two three-way taps are operated as shown in Figure 2, first branch road of inlet pipe 1 is for connecting impeller pump 6, centrifugal lower end of pumping pipe union three way cock 5, importing three-way tap 4 upper end is exported by middle union 3 from right-hand member, go out to enter impeller pump 7 from three-way tap 4 right-hand member, realize double pump series connection, the liquid carrying out lift superposition exports.Three-way tap 4 left end forms blocking-up to inlet pipe 1, and three-way tap 5 upper end realizes blocking isolation to going out pipe 2.
Manipulate two three-way tap combinations, the series and parallel that can realize two impeller pumps freely switches, and the system making it to form more rationally can adapt to the efficient press filtration operation in electrolytic manganese process, meets the requirement of electrolytic manganese industry.
The compression ring body that the taper-face ring 48 that air blast chemical combination bucket increases the making of anticorrosion stainless steel by common chemical combination bucket is formed with sieve aperture cylinder ring 49, is fixed on compression ring body by aspiration tube 47 front end, and aspiration tube venting port 50 is at the inner higher place of compression ring body.During work, ore pulp is generally lower than the suitable height of chemical combination bunghole part, and agitator is applicable to rotating speed and rotates, and is promoted downwards by ore pulp by two-layer stirring rake 43, completes and stirs and effectively prevent ore pulp from sinking to the bottom.
Root's blower is pressed to provide source of the gas during air blast chemical combination bucket generally adopts, by Valve controlling aspiration tube 7, pressurized air is imported chemical combination bucket 44 deep, aspiration tube venting port 50 is arranged in portion on the upper side in taper-face ring, the air now blasted forms air ring in ring, and air can be overflowed by sieve aperture cylinder ring 49 dispersing and disintegrating and enter chemical combination bucket; When air-flow is larger, gas can be inner along the membranaceous chemical combination bucket that overflow into by cylinder ring 49, reaches good gas-to-liquid contact, realizes in gas that oxygen is to the dissolving mass transfer of liquid phase, and accelerating oxidation reacts, and realizes removal of impurities object.
The air that pressurized air contacts with liquid level pressure in taper-face ring 48, cylinder ring is overflowed in sieve aperture refinement and liquid phase realize that microbubble shape pressure contacts, cylinder ring contacts with liquid phase pressure once again for 49 times after membranaceous spilling gas spreads, promote dissolved oxygen mass transfer, be conducive to oxidizing reaction to carry out, gas has enough time and path forms and liquid phase to be uniformly mixed bottom chemical combination bucket 44 in uphill process simultaneously, continue contact dissolved oxygen mass transfer, carried by downward liquid stream simultaneously when fining air bubbles rises and can liquid phase be returned to, realizing dissolved oxygen once again.Big area, multi-step, pressure changeable dissolve multimode synergy, promote dissolved oxygen and carry out efficiently useful oxidizing reaction.
Air blast chemical combination bucket dissolved oxygen works very well, dissolved oxygen, oxidizing reaction are thoroughly quick, several times more efficient than traditional way.
Above-mentioned just preferred embodiment of the present invention, not does any pro forma restriction to the present invention.Any those of ordinary skill in the art, when not departing from technical solution of the present invention scope, can utilize the technology contents of above-mentioned announcement to make many possible variations and modification to technical solution of the present invention, or being revised as the Equivalent embodiments of equivalent variations.Therefore, every content not departing from technical solution of the present invention, according to the technology of the present invention essence to any simple modification made for any of the above embodiments, equivalent variations and modification, all should drop in the scope of technical solution of the present invention protection.
Claims (3)
1. the chemical combination in an electrolytic manganese process and efficient filter-pressing device, comprise inlet pipe, go out pipe, two impeller pumps and two pressure filter, it is characterized in that: inlet pipe branches into two pipelines, article one, pipeline is connected pipe through three-way tap with impeller pump, and another pipeline is connected pipe through another impeller pump with another three-way tap; The upper and lower UNICOM of union in two three-way tap warps; Inlet pipe connects manganese solution chute, and chute has the bottom construction of back taper; Connect pipe through three-way tap after two pressure filter parallel connections, three-way tap controls the closed of two parallel branches and disconnects; Chute connects air blast chemical combination bucket.
2. the chemical combination according to claim 1 in electrolytic manganese process and efficient filter-pressing device, it is characterized in that: described air blast chemical combination bucket comprises staving, motor and step-down gear and stir shaft, stir shaft inserts in staving, and motor and step-down gear drive stir shaft to rotate, and stir shaft is fixed with Double-layer stirring paddle; Be provided with the compression ring body that taper-face ring and sieve aperture cylinder ring are formed in staving, aspiration tube front end is fixed on compression ring body, and aspiration tube venting port is at the inner higher place of compression ring body.
3. the chemical combination according to claim 2 in electrolytic manganese process and efficient filter-pressing device, it is characterized in that: be provided with spout bottom described staving, spout connects output control valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510396116.6A CN105018723B (en) | 2015-07-08 | 2015-07-08 | Chemical combination and efficient filter-pressing device in electrolytic manganese process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510396116.6A CN105018723B (en) | 2015-07-08 | 2015-07-08 | Chemical combination and efficient filter-pressing device in electrolytic manganese process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105018723A true CN105018723A (en) | 2015-11-04 |
| CN105018723B CN105018723B (en) | 2017-12-19 |
Family
ID=54409021
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510396116.6A Expired - Fee Related CN105018723B (en) | 2015-07-08 | 2015-07-08 | Chemical combination and efficient filter-pressing device in electrolytic manganese process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105018723B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87213415U (en) * | 1987-09-17 | 1988-08-10 | 空军油料研究所 | Series/parallel self-priming type centrifugal pump |
| CN202047113U (en) * | 2011-04-18 | 2011-11-23 | 深圳市正金贵金属有限公司 | Noble metal cooling and filtering device |
| CN204034360U (en) * | 2014-09-26 | 2014-12-24 | 吉首大学 | Fill rinsing type ore pulp filter press |
| WO2015043560A1 (en) * | 2013-09-25 | 2015-04-02 | Sms Siemag Ag | Production of high-grade manganese from ferromanganese by means of vaporization in a vacuum induction plant |
| CN104607076A (en) * | 2015-03-03 | 2015-05-13 | 吉首大学 | Thick slurry stirring chemical combination bucket |
-
2015
- 2015-07-08 CN CN201510396116.6A patent/CN105018723B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87213415U (en) * | 1987-09-17 | 1988-08-10 | 空军油料研究所 | Series/parallel self-priming type centrifugal pump |
| CN202047113U (en) * | 2011-04-18 | 2011-11-23 | 深圳市正金贵金属有限公司 | Noble metal cooling and filtering device |
| WO2015043560A1 (en) * | 2013-09-25 | 2015-04-02 | Sms Siemag Ag | Production of high-grade manganese from ferromanganese by means of vaporization in a vacuum induction plant |
| CN204034360U (en) * | 2014-09-26 | 2014-12-24 | 吉首大学 | Fill rinsing type ore pulp filter press |
| CN104607076A (en) * | 2015-03-03 | 2015-05-13 | 吉首大学 | Thick slurry stirring chemical combination bucket |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105018723B (en) | 2017-12-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN204380572U (en) | A kind of liquid backflow agitating device | |
| CN105018723A (en) | Chemical combination and efficient filter pressing device in manganese electrolysis process | |
| CN104911346A (en) | Combined and efficient filter pressing device in electrolytic manganese process | |
| CN104911347A (en) | Device for carrying out chemical combination and efficient filter pressing in manganese electrolyzing process | |
| CN104928466A (en) | Device for conducting chemical combination and efficient filter pressing in electrolytic manganese process | |
| CN204727932U (en) | Efficient filter-pressing device in electrolytic manganese process | |
| CN204752866U (en) | Device of high -efficient filter -pressing carries out in electrolytic manganese technology | |
| CN204959008U (en) | High -efficient filter pressing device in electrolytic zinc technology | |
| CN204737999U (en) | Device of high -efficient filter -pressing carries out in electrolytic zinc technology | |
| CN104922952B (en) | Chemical combination in electrolytic zinc technique and efficient filter-pressing device | |
| CN2836903Y (en) | Diversion barrel type dissolver | |
| CN210636047U (en) | Stirring-free continuous lithium leaching reaction tank | |
| CN204752824U (en) | Device of high -efficient filter -pressing carries out in electrolytic zinc technology | |
| CN204982000U (en) | Device of high -efficient filter -pressing carries out in electrolytic manganese technology | |
| CN204752823U (en) | High -efficient filter pressing device in electrolytic manganese technology | |
| CN105000590A (en) | Chemical combination and efficient filter pressing device in electrolytic zinc process | |
| CN204849051U (en) | High -efficient filter pressing device in electrolytic zinc technology | |
| CN206607014U (en) | A kind of liquid reagent filling components | |
| CN104911348A (en) | Combined and efficient filter pressing device in electrolytic zinc process | |
| CN105154668A (en) | Device for conducting combination and efficient filter pressing in zinc electrolysis process | |
| CN207749162U (en) | A kind of zinc metal sheet displacement prepares the device of Spongy Cadmium | |
| CN204767663U (en) | Carry out basic magnesium carbonate in device of high -efficient filter -pressing | |
| CN104984576A (en) | Pump circulation anti-blocking type device for efficiently pressing and filtering basic magnesium carbonate | |
| CN220531416U (en) | Stirring system for continuous leaching of rare earth roasting ore | |
| CN214218817U (en) | Acidic leaching residue CCD countercurrent washing interstage mixing device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Feng Quanxing Inventor before: Yao Maojun Inventor before: Yin Yongzhong |
|
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20171123 Address after: No. 52, Xiao Zhong house, Nanping Road, tower peak Town, Lanshan County, Yongzhou, Hunan Applicant after: Hunan double tribe information consulting service limited liability company Address before: 416000 Hunan, Xiangxi Tujia and Miao Autonomous Prefecture, Jishou City People's road, No. 120 Applicant before: Jishou University |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171219 Termination date: 20180708 |