CN104911348A - Combined and efficient filter pressing device in electrolytic zinc process - Google Patents

Combined and efficient filter pressing device in electrolytic zinc process Download PDF

Info

Publication number
CN104911348A
CN104911348A CN201510396120.2A CN201510396120A CN104911348A CN 104911348 A CN104911348 A CN 104911348A CN 201510396120 A CN201510396120 A CN 201510396120A CN 104911348 A CN104911348 A CN 104911348A
Authority
CN
China
Prior art keywords
pipe
steam
ring
chemical combination
way
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510396120.2A
Other languages
Chinese (zh)
Inventor
姚茂君
银永忠
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jishou University
Original Assignee
Jishou University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jishou University filed Critical Jishou University
Priority to CN201510396120.2A priority Critical patent/CN104911348A/en
Publication of CN104911348A publication Critical patent/CN104911348A/en
Pending legal-status Critical Current

Links

Abstract

The invention discloses a combined and efficient filter pressing device in electrolytic zinc process, wherein an inlet pipe branch 1 is connected with an outlet pipe through a three-way cock and one centrifugal pump, a branch 2 is connected with the output pipe through another one centrifugal pump and another one three-way cock, the two centrifugal pumps are driven through a motor, gears of the two three-way cocks are engaged with each other, one of the gears is driven by an active gear to achieve rotating switching of the two three-way cocks, and the gears are up and down communicated through a middle connecting pipe, and an inlet pipe is connected with a zinc solution chute with an inverted conical bottom structure. Two filter presses are connected with the outlet pipe after being connected in parallel and the zinc solution chute is connected with a steam heating combined barrel. The combined and efficient filter pressing device in electrolytic zinc process skillfully utilizes the two three-way cocks, achieves series and parallel free switching operation of the centrifugal pumps, improves filter pressing efficiency, and has the advantages that the structure is simple and the operation is not easy to go wrong. A conical bottom of the zinc solution chute is beneficial to output zinc solution and mineral waste residues. The steam heating combined barrel skillfully utilizes a steam dissolved ring which is formed through a conical ring and a mesh cylinder ring, improves dissolved temperature rising effect, and completely does not have noise interference.

Description

The device of chemical combination and efficient press filtration is carried out in a kind of electrolytic zinc technique
Technical field
The present invention relates in a kind of electrolytic zinc technique the device carrying out chemical combination and efficient press filtration.
Background technology
Electrolytic zinc carries out by zinc ore pulverizing, chemical combination, removal of impurities, carries out the hydrometallurgy process of electrolysis after allotment again, and wherein chemical combination is exactly, in chemical combination bucket, zinc ore powder pulp is added the process that sulfuric acid carries out chemical reaction.Chemical combination can obtain solubility zinc sulfate, is convenient to the electrolysis procedure carrying out the later stage.
At present, the chemical combination bucket volume of commercial application can reach hundreds of cubes, needs to add steam to promote the carrying out of combination reaction to chemical combination bucket in chemical combination process, has both realized the refining of electrolytic solution, and has also been conducive to the efficient electrolysis in later stage.
But chemical combination bucket adds steam realizes solution warms, if operate by traditional mode, the whole process adding liquid phase intensification at steam has intense noise and vibration, and operator often produces stronger infrasound injury sense.Therefore, the operator scheme that change conventional vapor adds, reduces noise and vibration, eliminates infrasound interference injury, all significant for protecting laborer and improving Working environment.
Need after chemical combination completes to remove solid slag by press filtration, to obtain the solution needed for electrolysis.Therefore, press filtration is also very important unit step in electrolytic zinc technique.
Press filtration in electrolytic zinc technique, general is all plate and frame(type)filter press, and select impeller pump as filter pressing pump, pressure-filtering process obtains filtrate, filter residue progressively runs up to optimal filling degree in pressure filter simultaneously, carry out respective handling again, finally complete the cyclical operation process of filter residue cleaning, the object of press filtration realizes solid-liquid separation exactly.In the starting stage of press filtration operation, owing to being complete empty in pressure filter, concerning filter pressing pump, the quick large discharge input carrying out less lift is the ideal operation state of now press filtration operation; But increase along with filter cake accumulates rear resistance in pressure filter, when particularly stopping close to press filtration, have peak pressure expanded state, therefore, larger lift can be had to be to best requirement by the press filtration performance of pressure filter in press filtration the second half.
But in press filtration operation, existing impeller pump all cannot adapt to such process automatically, reaches efficient, high-quality ideal operation state.When general impeller pump carries out press filtration operation, be all that the early stage lift of press filtration is lower, but flow is large, makes motor be in overload, especially easily motor damage; To the press filtration middle and later periods, press filtration resistance strengthens rapidly, and the flow quantity of impeller pump reduces rapidly, although at this moment motor is operated in the low power state of underloading, efficiency of press filtering is very low; Although filter pressing pump has H-Max output state, because pressing filtering liquid flow is less, the serviceability of pressure filter cannot be given full play to and increase work efficiency.
Therefore, impeller pump is made to coordinate pressure filter, the press filtration whole process in electrolytic zinc technique is made all to reach ideal operation state, the optimum performance playing press filtration is difficult to realize, if but look for another way, adopt the convenient shifter of two impeller pump series and parallels to complete press filtration work, make it in press filtration in early days by two impeller pump parallel connections, realize fast, less energy-consumption, the efficient press filtration of large discharge; In press filtration, two impeller pumps are connected by latter stage, obtain high-lift transport capacity, after meeting, journey press filtration resistance is large, but still applicable flow can be had to embody efficient press filtration and give full play to the feature of pressure filter performance, so convenient shifter of two impeller pump series and parallels is adopted to break through pressure filtering technique bottleneck in electrolytic zinc technique, reach the ideal operation state of press filtration, there is the actual application value of particularly important.
Summary of the invention
The technical problem to be solved in the present invention overcomes the deficiencies in the prior art exactly, the device carrying out chemical combination and efficient press filtration is provided in a kind of electrolytic zinc technique, this apparatus structure is simple, practical, the convenient switching of series and parallel of two centrifugal pump device can be realized, and chemical combination process is tranquil quick, disturbs without infrasound.
For overcoming the deficiencies in the prior art, the present invention takes following technical scheme:
Carry out a device for chemical combination and efficient press filtration in electrolytic zinc technique, comprise inlet pipe, go out pipe, two impeller pumps and two pressure filter, it is characterized in that: two impeller pumps pass through belt transmission by same motor; Inlet pipe branches into two pipelines, and a pipeline is connected pipe through three-way tap with impeller pump, and another pipeline is connected pipe through another impeller pump with another three-way tap; Two three-way taps are equipped with gear driven Spool rotating, and the gear of two three-way taps engages each other and has driving toothed gear to drive one, and the rotation realizing two three-way taps switches, the upper and lower UNICOM of union in two three-way tap warps; Inlet pipe connects zinc solution chute, and chute has the bottom construction of back taper; Connect pipe after two pressure filter parallel connections, two branch roads in parallel are equipped with control valve; Chute connects steam heating chemical combination bucket.
Described steam heating chemical combination bucket comprises staving, motor and step-down gear and stir shaft, and stir shaft inserts in staving, and motor and step-down gear drive stir shaft to rotate, and stir shaft is fixed with Double-layer stirring paddle; Be provided with the steam that taper-face ring and sieve aperture cylinder ring form in the middle part of staving and dissolve ring, vapour pipe front end is fixed on steam and dissolves on ring, and vapour pipe venting port dissolves the inner higher place of ring at steam.
Be provided with spout bottom described staving, spout connects output control valve.
This device is rotated by driven by motor driving toothed gear, can single-power gear-linked stroke, accurately fast switches manipulation, the convenient switching realizing two impeller pump series and parallel structures, the press filtration in electrolytic zinc technique can be made to operate and reach optimum Working; It is fabulous that steam heating chemical combination bucket dissolves temperature rise effect, tranquil quick, than traditional way environmental protection.
Compared with prior art, beneficial effect of the present invention is also:
The optimum working performance reaching impeller pump needed for press filtration in electrolytic zinc technique is switched by the series and parallel of impeller pump; By rationally succinct circuit design and single-power gear-linked stroke, accurately fast switch manipulation, the ingenious series and parallel blocked operation being achieved two impeller pumps by two three-way taps; Compared with the series and parallel pipeline valve shifter of routine, threeway plug valve can greatly reduce the consumption of pipeline and valve, and simplifies the blocked operation of series and parallel, avoids the mistake occurred in common pipe valve system series and parallel handoff procedure; The chute cone end of back taper, be conducive to the outflow of zinc solution; Two pressure filter parallel connections are convenient to wherein in a pressure filter cleaning filter residue process, and another pressure filter still normally can carry out press filtration; Steam heating chemical combination barrel structure is simple, practical, the ingenious steam utilizing taper-face ring and sieve aperture cylinder ring to form dissolves ring, greatly improve the dissolving temperature rise effect of steam, and it is tranquil quick, there is no steam noise, vibration and infrasonic interference completely, be conducive to the Working environment improving laborer, be also conducive to the carrying out promoting combination reaction.
Structure of the present invention is simple, and cost is low, practical, has a extensive future.
Accompanying drawing explanation
Fig. 1 is parallel-connection structure schematic diagram of the present invention.
Fig. 2 is cascaded structure schematic diagram of the present invention.
Fig. 3 is the two dimensional structure schematic diagram of steam heating chemical combination bucket.
In figure, each label represents:
1, inlet pipe; 2, pipe is gone out; 3, middle union; 4, three-way tap; 5, three-way tap; 6, impeller pump; 7, impeller pump; 21, driving toothed gear; 22, gear; 23, gear; 24, zinc solution chute; 30, pressure filter; 31, motor; 32, belt transmission; 33, belt transmission; 41, motor and step-down gear; 42, stir shaft; 43, stirring rake; 44, staving; 45, spout; 46, output control valve; 47, vapour pipe; 48, taper-face ring; 49, sieve aperture cylinder ring; 50, vapour pipe venting port.
Embodiment
Now by reference to the accompanying drawings, the present invention is illustrated further.
Carry out the device of chemical combination and efficient press filtration as shown in Figure 1, Figure 2 and Figure 3 in electrolytic zinc technique, comprise inlet pipe 1, two impeller pumps (6,7), go out pipe 2 and two pressure filter, 30, two impeller pumps 6,7 are driven by same motor 31; Inlet pipe 1 branches into two pipelines, and a pipeline is connected pipe 2 through three-way tap 4 with impeller pump 7, and another pipeline is connected pipe 2 through another impeller pump 6 with another three-way tap 5; Two three-way taps 4,5 are equipped with gear 22,23 and drive Spool rotating, the gear 22,23 of two three-way taps engages each other and has driving toothed gear 21 to drive one, the rotation realizing two three-way taps 4,5 switches, union about 3 UNICOM in two three-way tap 4,5 warps; Inlet pipe 1 connects zinc solution chute 24, and chute 24 has the bottom construction of back taper; Connect pipe 2 after the parallel connection of two pressure filter 30, two branch roads in parallel are equipped with control valve; Chute 24 connects steam heating chemical combination bucket.
Described steam heating chemical combination bucket comprises staving 44, motor and step-down gear 41 and stir shaft 42, and stir shaft 42 inserts in staving 44, and motor and step-down gear 41 drive stir shaft 42 to rotate, and stir shaft 42 are fixed with Double-layer stirring paddle 43; Be provided with the steam that taper-face ring 48 and sieve aperture cylinder ring 49 form in the middle part of staving 44 and dissolve ring, vapour pipe 47 front end is fixed on steam and dissolves on ring, and vapour pipe venting port 50 is at higher place, steam dissolving ring inside.
Be provided with spout 45 bottom described staving 44, spout 45 connects output control valve 46.
The zinc solution chute cone end, is conducive to zinc solution and pulverous slag delivers into pressure filter 30.
Device is that single motor 31 drives identical two pumps work respectively by belt 32,33.Fig. 1 and Fig. 2 is same device different states, wherein driving toothed gear 21 is driven by motor deceleration Stroke Control, and first drive the gear 23 of union three way cock 5 spool, gear 23 drives the gear 22 of union three way cock 4 spool again, realize single-power gear-linked, fast switch manipulation.
Fig. 1 is impeller pump 6,7 conveyance fluid in parallel, and the first branch road of inlet pipe 1 is for connecting impeller pump 6, and impeller pump 6 goes out the lower end of pipe union three way cock 5, is merged into out pipe 2 from upper end; Second branch road of water inlet pipe 1 is enter impeller pump 7 after union three way cock right-hand member 4, exports, be incorporated in out pipe 2, realize two branch road two parallel pumps, carry out large discharge output through pressurization, and three-way tap 5 left end centering union is closed and cut off.
After two three-way taps are operated as shown in Figure 2, first branch road of inlet pipe 1 is for connecting impeller pump 6, centrifugal lower end of pumping pipe union three way cock 5, importing three-way tap 4 upper end is exported by middle union 3 from left end, go out to enter impeller pump 7 from three-way tap 4 left end, realize double pump series connection, the liquid carrying out lift superposition exports.Three-way tap 4 right-hand member forms blocking-up to inlet pipe 1, and three-way tap 5 upper end realizes blocking isolation to going out pipe 2.
As described above by single-power gear-linked, carry out stroke fast to switch accurately, interlock manipulation two three-way tap combinations, the series and parallel realizing two impeller pumps switches, the system making it to form more rationally can adapt to the efficient press filtration operation in electrolytic zinc technique, meets the requirement of electrolytic zinc industry.
Steam heating chemical combination bucket increases by common chemical combination bucket the steam that taper-face ring 48 that anticorrosion stainless steel makes and sieve aperture cylinder ring 49 form and dissolves ring, and vapour pipe 47 front end is fixed on steam and dissolves on ring, vapour pipe venting port 50 dissolves higher place, ring inside at steam.During work, ore pulp is generally lower than the suitable height of chemical combination bunghole part, and agitator is applicable to rotating speed and rotates, and is promoted downwards by ore pulp by two-layer stirring rake, completes and stirs and effectively prevent ore pulp from sinking to the bottom.
Steam heating chemical combination bucket generally adopts boiler to provide steam, by Valve controlling vapour pipe 47, steam is imported steam ring in the middle part of chemical combination bucket, vapour pipe venting port 50 is arranged in portion on the upper side in taper-face ring 48, steam forms steam ring in taper-face ring 48, steam ring top forms septate heat transfer by taper-face ring 48 makes solution warms, inner by also carrying out high-efficiency heating to solution to the absorption of liquid phase level mass transfer.After a large amount of steam adds, excess steam can be overflowed by sieve aperture cylinder ring 49 dispersing and disintegrating, enters chemical combination bucket microbubble shape and liquid phase effect mass transfer, makes solution warms; When steam flow is larger, steam can overflow into chemical combination bucket internal divergence along membranaceous 49 times by cylinder ring, also fully contacts liquid phase and forms mass transfer and heat up, realize the diffusion of multipath Quick steam by liquid phase scrubbing, reach chemical combination bucket liquid phase and to be rapidly heated object.
Steam overflows cylinder ring 49 in taper-face ring 48 steam with the contact lysis of liquid level pressure, sieve aperture refinement realizes with liquid phase that microbubble shape pressure contacts, cylinder ring contacts with liquid phase pressure once again for 49 times after membranaceous spilling vapor diffusion, improves steam dissolved efficiency.The multiple diffusion way of steam dissolves, and has enough areas to be subject to stirring action, the uniformity of temperature in favourable chemical combination bucket simultaneously, completely eliminates the bad sensation that noise, vibration and infrasound disturb.
Steam heating chemical combination bucket temperature rise effect is fabulous, tranquil quick, than traditional way environmental protection.
Above-mentioned just preferred embodiment of the present invention, not does any pro forma restriction to the present invention.Any those of ordinary skill in the art, when not departing from technical solution of the present invention scope, can utilize the technology contents of above-mentioned announcement to make many possible variations and modification to technical solution of the present invention, or being revised as the Equivalent embodiments of equivalent variations.Therefore, every content not departing from technical solution of the present invention, according to the technology of the present invention essence to any simple modification made for any of the above embodiments, equivalent variations and modification, all should drop in the scope of technical solution of the present invention protection.

Claims (3)

1. carry out a device for chemical combination and efficient press filtration in electrolytic zinc technique, comprise inlet pipe, go out pipe, two impeller pumps and two pressure filter, it is characterized in that: two impeller pumps pass through belt transmission by same motor; Inlet pipe branches into two pipelines, and a pipeline is connected pipe through three-way tap with impeller pump, and another pipeline is connected pipe through another impeller pump with another three-way tap; Two three-way taps are equipped with gear driven Spool rotating, and the gear of two three-way taps engages each other and has driving toothed gear to drive one, and the rotation realizing two three-way taps switches, the upper and lower UNICOM of union in two three-way tap warps; Inlet pipe connects zinc solution chute, and chute has the bottom construction of back taper; Connect pipe after two pressure filter parallel connections, two branch roads in parallel are equipped with control valve; Chute connects steam heating chemical combination bucket.
2. carry out the device of chemical combination and efficient press filtration according to claim 1 in electrolytic zinc technique, it is characterized in that: described steam heating chemical combination bucket comprises staving, motor and step-down gear and stir shaft, stir shaft inserts in staving, motor and step-down gear drive stir shaft to rotate, and stir shaft is fixed with Double-layer stirring paddle; Be provided with the steam that taper-face ring and sieve aperture cylinder ring form in the middle part of staving and dissolve ring, vapour pipe front end is fixed on steam and dissolves on ring, and vapour pipe venting port dissolves the inner higher place of ring at steam.
3. carry out the device of chemical combination and efficient press filtration according to claim 2 in electrolytic zinc technique, it is characterized in that: be provided with spout bottom described staving, spout connects output control valve.
CN201510396120.2A 2015-07-08 2015-07-08 Combined and efficient filter pressing device in electrolytic zinc process Pending CN104911348A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510396120.2A CN104911348A (en) 2015-07-08 2015-07-08 Combined and efficient filter pressing device in electrolytic zinc process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510396120.2A CN104911348A (en) 2015-07-08 2015-07-08 Combined and efficient filter pressing device in electrolytic zinc process

Publications (1)

Publication Number Publication Date
CN104911348A true CN104911348A (en) 2015-09-16

Family

ID=54080787

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510396120.2A Pending CN104911348A (en) 2015-07-08 2015-07-08 Combined and efficient filter pressing device in electrolytic zinc process

Country Status (1)

Country Link
CN (1) CN104911348A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87213415U (en) * 1987-09-17 1988-08-10 空军油料研究所 Series/parallel self-priming type centrifugal pump
JPH08150306A (en) * 1994-11-28 1996-06-11 Tanii Kogyo Kk Method for washing filter press filter cloth for cement base waste water
CN202942877U (en) * 2012-11-30 2013-05-22 泸溪蓝天冶化有限责任公司 Chemical combination barrel
CN204034360U (en) * 2014-09-26 2014-12-24 吉首大学 Fill rinsing type ore pulp filter press
CN204057992U (en) * 2014-09-12 2014-12-31 上饶市鼎鑫金属化工有限公司 Moist chemical synthesis manganese oxide atmospheric oxidation device

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87213415U (en) * 1987-09-17 1988-08-10 空军油料研究所 Series/parallel self-priming type centrifugal pump
JPH08150306A (en) * 1994-11-28 1996-06-11 Tanii Kogyo Kk Method for washing filter press filter cloth for cement base waste water
CN202942877U (en) * 2012-11-30 2013-05-22 泸溪蓝天冶化有限责任公司 Chemical combination barrel
CN204057992U (en) * 2014-09-12 2014-12-31 上饶市鼎鑫金属化工有限公司 Moist chemical synthesis manganese oxide atmospheric oxidation device
CN204034360U (en) * 2014-09-26 2014-12-24 吉首大学 Fill rinsing type ore pulp filter press

Similar Documents

Publication Publication Date Title
CN204716559U (en) Two centrifugal pump devices of the convenient switching of a kind of series and parallel
CN104922952B (en) Chemical combination in electrolytic zinc technique and efficient filter-pressing device
CN104911348A (en) Combined and efficient filter pressing device in electrolytic zinc process
CN105154668A (en) Device for conducting combination and efficient filter pressing in zinc electrolysis process
CN204752866U (en) Device of high -efficient filter -pressing carries out in electrolytic manganese technology
CN204737999U (en) Device of high -efficient filter -pressing carries out in electrolytic zinc technology
CN105000590A (en) Chemical combination and efficient filter pressing device in electrolytic zinc process
CN204959008U (en) High -efficient filter pressing device in electrolytic zinc technology
CN204727932U (en) Efficient filter-pressing device in electrolytic manganese process
CN104895802A (en) Double-centrifugal-pump device free in serial connection and parallel connection switching
CN202081195U (en) Oiling agent head tank device with cleaning function
CN204767663U (en) Carry out basic magnesium carbonate in device of high -efficient filter -pressing
CN112375916B (en) Copper-cobalt hydrometallurgy filtering and washing system and operation mode thereof
CN204752824U (en) Device of high -efficient filter -pressing carries out in electrolytic zinc technology
CN204982000U (en) Device of high -efficient filter -pressing carries out in electrolytic manganese technology
CN204723831U (en) Sugar-cane juice is carried out the device of efficient press filtration
CN104911346A (en) Combined and efficient filter pressing device in electrolytic manganese process
CN204849051U (en) High -efficient filter pressing device in electrolytic zinc technology
CN104928466A (en) Device for conducting chemical combination and efficient filter pressing in electrolytic manganese process
CN204752823U (en) High -efficient filter pressing device in electrolytic manganese technology
CN204752753U (en) High -efficient filter pressing device of sugar -cane juice
CN104911347A (en) Device for carrying out chemical combination and efficient filter pressing in manganese electrolyzing process
CN105018723A (en) Chemical combination and efficient filter pressing device in manganese electrolysis process
CN204752754U (en) Carry out sugar -cane juice in device of high -efficient filter -pressing
CN104984576A (en) Pump circulation anti-blocking type device for efficiently pressing and filtering basic magnesium carbonate

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20150916

RJ01 Rejection of invention patent application after publication