CN105018217A - Shiny-leaved yellowhorn seed oil and extraction method for bioactive substances thereof - Google Patents
Shiny-leaved yellowhorn seed oil and extraction method for bioactive substances thereof Download PDFInfo
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- CN105018217A CN105018217A CN201410178848.3A CN201410178848A CN105018217A CN 105018217 A CN105018217 A CN 105018217A CN 201410178848 A CN201410178848 A CN 201410178848A CN 105018217 A CN105018217 A CN 105018217A
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Abstract
The invention relates to shiny-leaved yellowhorn seed oil and an extraction method for bioactive substances thereof. According to the extraction method for the bioactive substances of the shiny-leaved yellowhorn seed oil, the shiny-leaved yellowhorn seed oil and the bioactive substances thereof are prepared in a one-pot mode through a dual-solvent extraction method including a fourth solvent and an alcohol compound solvent. According to the improvement and the practical value of the extraction method for the bioactive substances of the shiny-leaved yellowhorn seed oil, the shiny-leaved yellowhorn seed oil and the bioactive substances thereof can be prepared in the one-pot mode by use of the method, the purity of the seed oil is high, the extraction of the bioactive substances is simple, the method is simple and convenient and practical, the low-priced and safe effects are achieved, and the method is suitable for industrial production. According to the shiny-leaved yellowhorn seed oil and the extraction method for the bioactive substances thereof, no three wastes are generated in the whole preparation process, and environmental friendliness is achieved.
Description
Technical field
The present invention relates to the extracting method of a kind of Wood of Shinyleaf Yellowhorn seed oil and biologically active substance thereof.
Technical background
Wood of Shinyleaf Yellowhorn (Xanthoceras sorbifolia Bunge) belongs to defoliation small arbor or shrub for Sapindaceae Wood of Shinyleaf Yellowhorn, originate in northern China, seed oil yield is higher, can compare favourably with southern oil tea and from the Fructus oleae europaeae of overseas introduction, therefore have title (whole Chang Yao, the Zhang Xuezeng of " northern oil tea ", Wood of Shinyleaf Yellowhorn historical profiles, Jilin forestry science and technology, 1979,1:2325).Wood of Shinyleaf Yellowhorn seed oil length is 30.4%; Plant benevolence oil length up to 66.39%, protein content 25.75%, crude fiber content 1.6%, non-nitrogen material 3.73%; Unsaturated fatty acid content 94% in oil content, its Linoleic acid accounts for 36.9%, and oleic acid accounts for 57.16%, be super superfine high-class healthy edible oil, there is Qinghua blood lipid thing, vessel softening, remove thrombus matter, block subcutaneous lipids and formed, reduce the specific action of blood fat, cholesterol.In addition, the kind benevolence extract of Wood of Shinyleaf Yellowhorn is the very important medicine improving brain function, containing crude fat and 17 seed amino acids and saponin(e, water, candy, trace element.Its effect improves brain function, can treat enuresis disease, mental retardation and dementia etc. due to the low caused illness of brain function.At present relevant Wood of Shinyleaf Yellowhorn kind benevolence and plant shell physico-chemical analysis, adopt the research of cold-press, single solvent or biphasic solvent extraction shinyleaf yellowhorn oil there are reports (Li Jun, Li Xiabing etc., the look one mass spectroscopy qualification of shinyleaf yellowhorn oil fatty acid component, plant resources and environment, 1993,2:2832; Wang Lili, Fu Yujie, open and stand up, Wood of Shinyleaf Yellowhorn seed oil extraction process, plant research, 2008,28:509; Deng Hong, He Ling, Sun Jun, the cold press extraction of shinyleaf yellowhorn oil and physico-chemical property research, Agricultural University Of Southwest's journal, 2006,28,1027; Cao Fenghua, Chen Yang, Zhai Fengying, WANG Xiaohong, Two Liquid Phases method extraction shinyleaf yellowhorn oil and two-step approach prepare the technical study of biofuel, and Chinese science and technology paper is online, and 2006.).But adopt duo-sol extraction method to extract Wood of Shinyleaf Yellowhorn seed oil and biologically active substance, research at present report is little simultaneously.The extracting method of systematic study shinyleaf yellowhorn oil and biologically active substance has important effect to deep exploitation Wood of Shinyleaf Yellowhorn resource.
Technique (the M Thobani of a kind of uniqueness that the people such as solvent extraction Fa Shi University of Toronto Diosady develop for the feature of vegetable seed, L L Diosady.Twophase Solvent extraction of Canola [J] .J.Am.Oil Chem.Soc., 1995,72:207; M Thobani, L L Diosady.Pilotscale two-phase extraction of canola [J] .J.Am.Oil Chem.Soc., 1997,74:201.) utilize the character of dissolving each other of grease and solvent, extracted and be dissolved out, then use strict technology and equipment, remove a kind of advanced person of solvent in grease, the preparation method of science, extensively adopt in the industry such as foodstuffs industry, medicine.Up to the present, the used solvent of oil extraction has 12 kinds: dithiocarbonic anhydride; Thick hydrocarbon gasoline; Ethanol; Water substitution; Petroleum hydrocarbon; Benzene; Halogenated hydrocarbon; Virahol; Aldehyde, furfural etc.; Ketone, acetone, butanone etc.; Supercritical co; Mixed solvent.At present, domestic edible vegetable oil and fat leaches and mainly adopts No. 6 solvents, and external oil extraction generally adopts industrial normal hexane, also has and adopts pentane, octane etc.
No. 4 solvent (main component is leuna gas, butane) leaching grease technology, be a kind of brand-new grease production technology, compared with No. 6 solvent extraction grease technology of current widespread use, it has significant economic benefit and social benefit.First its outstanding advantages is " normal temperature leaching, low temperature desolventizing ", can extract grease, for the extraction of valuable oil plant and the exploitation of vegetable-protein create conditions when not destroying active substance in oil plant, vegetable-protein.Secondly steam consumption is few, and in oil production, coal consumption reduces more than 80%, thus reduces costs, and decreases the discharge of " three wastes ".Adopt No. 4 solvent-75% ethanol to be that biphasic solvent extracts shinyleaf yellowhorn oil and biologically active substance, there is no the report of document at present.
Summary of the invention
The present invention is to provide a kind of method that one kettle way extracts Wood of Shinyleaf Yellowhorn seed oil and biologically active substance thereof.
For achieving the above object, adopt No. 4 solvent-75% ethanol to be solvent pairs, utilize duo-sol extraction method, one kettle way extracts Wood of Shinyleaf Yellowhorn seed oil and biologically active substance.No. 4 solvent volume per-cent 50 ~ 85%, 75% ethanol contend per-cents 15 ~ 50% in solvent.
Extracting method is as follows: get a certain amount of (100 ~ 300g) and squeeze broken Wood of Shinyleaf Yellowhorn seed, add dehydrated alcohol 60 ~ 100mL, and Na
2cO
3on a small quantity (1 ~ 5wt%).No. 4 solvents are injected batch extractor by solvent pump, extract 4h at 35 DEG C.Stratification, filtering solids residue is Wood of Shinyleaf Yellowhorn leaching meal.No. 4 solvent layers adopt the method for underpressure distillation to reclaim No. 4 solvents and Wood of Shinyleaf Yellowhorn seed oil; Alcohol layer adopts the method for underpressure distillation to reclaim ethanol, obtains biologically active substance.
Specific embodiment 1
Get 120g and squeeze broken Wood of Shinyleaf Yellowhorn seed, add dehydrated alcohol 60mL, and 1wt%Na
2cO
3.No. 4 solvent 360mL are injected batch extractor by solvent pump, extract 4h at 35 DEG C.Stratification, filtering solids residue is Wood of Shinyleaf Yellowhorn leaching meal.No. 4 solvent layers adopt the method for underpressure distillation to reclaim No. 4 solvents and Wood of Shinyleaf Yellowhorn seed oil 90mL; Alcohol layer adopts the method for underpressure distillation to reclaim ethanol, obtains biologically active substance.
Specific embodiment 2
Get 300g and squeeze broken Wood of Shinyleaf Yellowhorn seed, add dehydrated alcohol 100mL, and 5wt%Na
2cO
3.No. 4 solvent 500mL are injected batch extractor by solvent pump, extract 4h at 35 DEG C.Stratification, filtering solids residue is Wood of Shinyleaf Yellowhorn leaching meal.No. 4 solvent layers adopt the method for underpressure distillation to reclaim No. 4 solvents and Wood of Shinyleaf Yellowhorn seed oil 220mL; Alcohol layer adopts the method for underpressure distillation to reclaim ethanol, obtains biologically active substance.
Claims (2)
1. the extracting method of a Wood of Shinyleaf Yellowhorn seed oil and biologically active substance thereof.Duo-sol extraction one kettle way is utilized to prepare Wood of Shinyleaf Yellowhorn seed oil and biologically active substance thereof.
2. the extracting method of a kind of Wood of Shinyleaf Yellowhorn seed oil as claimed in claim 1 and biologically active substance thereof, is characterized in that: prepare Wood of Shinyleaf Yellowhorn seed oil and biologically active substance thereof by the duo-sol extraction method one pot of No. 4 solvents and alcohol double solvents.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410178848.3A CN105018217A (en) | 2014-04-30 | 2014-04-30 | Shiny-leaved yellowhorn seed oil and extraction method for bioactive substances thereof |
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| CN201410178848.3A CN105018217A (en) | 2014-04-30 | 2014-04-30 | Shiny-leaved yellowhorn seed oil and extraction method for bioactive substances thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1962839A (en) * | 2006-11-23 | 2007-05-16 | 侯梦斌 | Device and method for preparing bio-extract |
| CN103409230A (en) * | 2013-07-17 | 2013-11-27 | 福建农林大学 | Method for low temperature extraction of plant oil through n-butane-ethanol-water double phase solvent |
| CN103582694A (en) * | 2011-04-06 | 2014-02-12 | 赫里开发公司 | Extraction of polar lipids by a two solvent method |
| CN103525542B (en) * | 2013-10-18 | 2015-01-21 | 北京林业大学 | Method for extracting shiny-leaved yellowhorn grease containing nervonic acid from shiny-leaved yellowhorn |
-
2014
- 2014-04-30 CN CN201410178848.3A patent/CN105018217A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1962839A (en) * | 2006-11-23 | 2007-05-16 | 侯梦斌 | Device and method for preparing bio-extract |
| CN103582694A (en) * | 2011-04-06 | 2014-02-12 | 赫里开发公司 | Extraction of polar lipids by a two solvent method |
| CN103409230A (en) * | 2013-07-17 | 2013-11-27 | 福建农林大学 | Method for low temperature extraction of plant oil through n-butane-ethanol-water double phase solvent |
| CN103525542B (en) * | 2013-10-18 | 2015-01-21 | 北京林业大学 | Method for extracting shiny-leaved yellowhorn grease containing nervonic acid from shiny-leaved yellowhorn |
Non-Patent Citations (1)
| Title |
|---|
| 杨明: "《中药药剂学》", 31 August 2008, 上海科学技术出版社 * |
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Application publication date: 20151104 |
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