CN105012196A - Method for preparing spray-type facial mask fluid for removing chloasma - Google Patents
Method for preparing spray-type facial mask fluid for removing chloasma Download PDFInfo
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- CN105012196A CN105012196A CN201510469926.XA CN201510469926A CN105012196A CN 105012196 A CN105012196 A CN 105012196A CN 201510469926 A CN201510469926 A CN 201510469926A CN 105012196 A CN105012196 A CN 105012196A
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Abstract
The invention relates to a method for preparing a spray-type facial mask fluid for removing chloasma, and belongs to the field of cosmetic processing. According to the method, multiple traditional Chinese medicinal materials with effect of removing chloasma are synergetically applied by researching and developing the extraction process, and the extraction effect is excellent; and the spray-type facial mask fluid for removing chloasma can be prepared by high-quality traditional Chinese medicinal stock solution and the formula of the chloasma-removing facial mask by means of flash sterilization. Nature and purity of component extraction are strictly controlled, purity and curative effect of ingredients are maintained to achieve double effects of beautifying external skin and improving internal tissue for consumers by means of contact between natural ingredients and natural skin. By adopting the spray-type design, the facial mask fluid has the advantages of facial mask stock solution reduction, low carbon and environmental friendliness in comparison with traditional carrier facial masks.
Description
Technical field
The present invention relates to a kind of preparation method of functions of removing chloasma aerosol type facial mask liquid, belong to cosmetics manufacture field.
Background technology
Loving beauty is part of human nature.Along with growth in the living standard, the requirement of people to quality of life is more and more higher, more and more pay attention to the natural whitening of skin, and facial area seems particularly important.Chloasma is a kind of acquired pigmentation dermatosis, and be the limitation caused by many reasons, scrambling change o f skin colour, clinical manifestation is symmetry pigmentation, in butterfly aliform, the lighter is yellowish or light brown, and some lamellar intersperses among buccal both sides, multiple with outside under eye; Severe one is distributed in face in deeply brown or light/dark balance.Primary disease is mainly in young and middle-aged women, and generally without any subjective symptoms, the course of disease is obstinate, has a strong impact on patient attractive in appearance, brings many worries and misery to patient mental and life aspect.
Chloasma pathogeny is complicated, and melanocyte is too much the performance of its central pathological.Its definite pathogenesis is not bright so far, it is generally acknowledged relevant with the factors such as Melanin Metabolism exception, endocrine disturbance, gestation, oral contraceptive, inherited genetic factors, oxygen-derived free radicals, ultraviolet radiation, tryrosinase dysfunction, the black pigment of skin Developmental and Metabolic Disorder that wherein endocrine disturbance, heredity, ultraviolet radiation etc. cause is the main cause of its morbidity.
Modern medical therapy chloasma mainly comprises the agent of use lucifuge, and system uses vitamins, tranamic acid, melatonin etc.; But it is basic based on local topical chemical decolorization; Also have Chemical peeling horny layer or chemical skin sand to grind off and destroy melanin granule etc. except melanocyte and with dye laser., most methods because causing the toxic and side effects such as uneven depigmentation, telangiectasis, contact dermatitis or itself is unstable, slow curative effect easily recurs, and has the fraud causing permanent decolouring and drug induccd moth patch, and fails to apply.
At present, the composite skin care item of plurality of Chinese emerge in an endless stream, but, due to the factors such as Chinese medicine ingredients molecular weight is large impact, it is inconsistent that various component proposes stripping, and absorb inharmonious, the assimilation effect of Chinese medicinal skin care product is not good, skin effect is not obvious, cannot play clean white, the control oil of Chinese medicine, the return of spring, anti-anaphylaxis, the advantageous effect such as anti-ageing.
Summary of the invention
The technical problem that the present invention mainly solves: uneven depigmentation can be caused for treating chloasma at present, telangiectasis, the toxic and side effects such as contact dermatitis or instability itself, slow curative effect easily recurs, and cause the present situations such as permanent decolouring and drug induccd moth patch, provide a kind of preparation method of functions of removing chloasma aerosol type facial mask liquid, the method is the research and development by extraction process, by the multiple Chinese medicine synergistic application with functions of removing chloasma effect, and extraction effect is excellent, the Chinese medicine stock solution of high-quality, freckle-removing mask formula in addition, instantaneous sterilizing obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
In order to solve the problems of the technologies described above, the technical solution adopted in the present invention is:
(1) 10 ~ 20g Cortex Phellodendri is taken, 10 ~ 15g Herba Taraxaci, 5 ~ 10g Radix Rubiae, and 10 ~ 20g Flos Lonicerae, put into the fragment that pulverizer breaks into 1 ~ 2cm, fragment is carried out supercritical carbon dioxide extraction 30 ~ 60min, extraction temperature is 55 ~ 65 DEG C, and extracting pressure is 10 ~ 15MPa;
(2) 20 ~ 40g Rhizoma Smilacis Glabrae is taken again, 10 ~ 20g Radix Sangusorbae, 5 ~ 15g Radix Paeoniae Rubra, 10 ~ 20g Fructus Kochiae and 10 ~ 20g Radix Isatidis, load in filtration paper cylinder after pulverizer is pulverized, filtration paper cylinder is put into cable type extractor according, and connects receiving flask, the three filter ethane that bottle amasss 2/3 are added in receiving flask, carry out condensing reflux, after extracting 6 ~ 12h, catcher is placed in baking oven and dries, ether is volatilized and separates out Chinese medicinal powder, oven temperature is 105 ~ 110 DEG C;
(3) by above-mentioned extraction and the Chinese medicinal powder mix homogeneously that extracts, and the deionized water and stirring adding its volume 8 ~ 10 times is even, obtains Chinese medicine mixed liquor, for subsequent use;
(4) by mass percent 5 ~ 7% glycerol, 4 ~ 6%1,3-butanediol, 0.1 ~ 0.3% hyaluronic acid, 2 ~ 4% Chinese medicine mixed liquors, 0.5 ~ 0.8% carbomer, 0.5 ~ 0.8% triethanolamine, 0.3 ~ 0.5% Polyethylene Glycol, 80 ~ 85% deionized waters, stir and obtain facial film stock solution compositions;
(5) above-mentioned facial film stock solution compositions is carried out magnetic agitation, rotating speed is 100 ~ 200r/min, mixing time 10 ~ 15min, put into centrifuge separation afterwards and obtain facial film serosity, centrifuge speed is 10000 ~ 12000r/min, then carry out quick-freezing sterilizing, then Infrared Heating is recovered, and obtains facial film stock solution;
(7) be that 1:100 ~ 1:150 dilutes facial film stock solution by stock solution and water volume ratio, inspection, bottling, obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
Described quick-freezing sterilizing methods utilizes liquid nitrogen to carry out instantaneous sterilizing at-40 ~-30 DEG C, sterilization time 10 ~ 15s.
Described Infrared Heating temperature is 70 ~ 80 DEG C, and the time is 20 ~ 30min.
The invention has the beneficial effects as follows:
(1) natural sex, the pure property of the extraction of strict control composition, and keep the consummate and curative effect of composition;
(2) by the multiple Chinese medicine synergistic application with functions of removing chloasma effect, and extraction effect is excellent, and the Chinese medicine stock solution of high-quality, as formula, makes every effort to allow consumer's touching by natural component and natural skin, reaches in beautifying outer flesh and improving the double effects managed;
(3) adopt atomizing design, compare traditional carrier facial film, more save facial film stock solution, low-carbon environment-friendly.
Detailed description of the invention
Take 10 ~ 20g Cortex Phellodendri, 10 ~ 15g Herba Taraxaci, 5 ~ 10g Radix Rubiae, and 10 ~ 20g Flos Lonicerae, put into the fragment that pulverizer breaks into 1 ~ 2cm, fragment is carried out supercritical carbon dioxide extraction 30 ~ 60min, extraction temperature is 55 ~ 65 DEG C, and extracting pressure is 10 ~ 15MPa; Take 20 ~ 40g Rhizoma Smilacis Glabrae again, 10 ~ 20g Radix Sangusorbae, 5 ~ 15g Radix Paeoniae Rubra, 10 ~ 20g Fructus Kochiae and 10 ~ 20g Radix Isatidis, load in filtration paper cylinder after pulverizer is pulverized, filtration paper cylinder is put into cable type extractor according, and connects receiving flask, the ether that bottle amasss 2/3 is added in bottle, carry out condensing reflux, after extracting 6 ~ 12h, catcher is placed in baking oven and dries, ether is volatilized and separates out Chinese medicinal powder, oven temperature is 105 ~ 110 DEG C; By above-mentioned extraction and the Chinese medicinal powder mix homogeneously that extracts, and the deionized water and stirring adding its volume 8 ~ 10 times is even, for subsequent use; In blender, 5 ~ 7% glycerol are added by mass percent, 4 ~ 6%1,3-butanediol, 0.1 ~ 0.3% hyaluronic acid, 2 ~ 4% Chinese medicine mixed liquors, 0.5 ~ 0.8% carbomer, 0.5 ~ 0.8% triethanolamine, 0.3 ~ 0.5% Polyethylene Glycol, 80 ~ 85% deionized waters, stir and obtain facial film stock solution compositions; Above-mentioned facial film stock solution compositions is carried out magnetic agitation, rotating speed is 100 ~ 200r/min, mixing time 10 ~ 15min, put into centrifuge separation afterwards and obtain facial film serosity, centrifuge speed is 10000 ~ 12000r/min, then carry out quick-freezing sterilizing, then Infrared Heating is recovered, and obtains facial film stock solution; Be that 1:100 ~ 1:150 dilutes facial film stock solution by stock solution and water volume ratio, inspection, bottling, obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
Occupation mode of the present invention is: cleaned by face after getting up early morning and before sleeping evening, get the present invention and be evenly sprayed to face, wash away, use and can find positive effect in 15 ~ 30 days after crossing 15 ~ 20min.
Take 10g Cortex Phellodendri, 10g Herba Taraxaci, 5g Radix Rubiae, and 10g Flos Lonicerae, put into the fragment that pulverizer breaks into 1cm, fragment is carried out supercritical carbon dioxide extraction 30min, extraction temperature is 55 DEG C, and extracting pressure is 10MPa; Take 20g Rhizoma Smilacis Glabrae again, 10g Radix Sangusorbae, 5g Radix Paeoniae Rubra, the 10g Fructus Kochiae and 10g Radix Isatidis, load in filtration paper cylinder after pulverizer is pulverized, filtration paper cylinder is put into cable type extractor according, and connects receiving flask, the ether that bottle amasss 2/3 is added in bottle, carry out condensing reflux, after extracting 6h, catcher is placed in baking oven and dries, ether is volatilized and separates out Chinese medicinal powder, oven temperature is 105 DEG C; By above-mentioned extraction and the Chinese medicinal powder mix homogeneously that extracts, and the deionized water and stirring adding its volume 8 times is even, for subsequent use; In blender, add 5% glycerol by mass percent, 4%1,3-butanediol, 0.1% hyaluronic acid, 2% Chinese medicine mixed liquor, 0.5% carbomer, 0.5% triethanolamine, 0.3% Polyethylene Glycol, 80% deionized water, stir and obtain facial film stock solution compositions; Above-mentioned facial film stock solution compositions is carried out magnetic agitation, and rotating speed is 100r/min, and mixing time is 10min, put into centrifuge separation afterwards and obtain facial film serosity, centrifuge speed is 10000r/min, then carries out quick-freezing sterilizing, Infrared Heating is recovered again, obtains facial film stock solution; Be that 1:100 dilutes facial film stock solution by stock solution and water volume ratio, inspection, bottling, obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
After patient with chloasma is got up early morning and before sleep, face is cleaned evening, get the present invention and be evenly sprayed to face, wash away after mistake 15min, use 15 days rear face chloasma obviously to reduce.
Take 15g Cortex Phellodendri, 13g Herba Taraxaci, 8g Radix Rubiae, and 15g Flos Lonicerae, put into the fragment that pulverizer breaks into 1 ~ 2cm, fragment is carried out supercritical carbon dioxide extraction 40min, extraction temperature is 60 DEG C, and extracting pressure is 13MPa; Take 30g Rhizoma Smilacis Glabrae again, 15g Radix Sangusorbae, 10g Radix Paeoniae Rubra, the 15g Fructus Kochiae and 15g Radix Isatidis, load in filtration paper cylinder after pulverizer is pulverized, filtration paper cylinder is put into cable type extractor according, and connects receiving flask, the ether that bottle amasss 2/3 is added in bottle, carry out condensing reflux, after extracting 9h, catcher is placed in baking oven and dries, ether is volatilized and separates out Chinese medicinal powder, oven temperature is 108 DEG C; By above-mentioned extraction and the Chinese medicinal powder mix homogeneously that extracts, and the deionized water and stirring adding its volume 9 times is even, for subsequent use; In blender, add 6% glycerol by mass percent, 5%1,3-butanediol, 0.2% hyaluronic acid, 3% Chinese medicine mixed liquor, 0.6% carbomer, 0.7% triethanolamine, 0.4% Polyethylene Glycol, 83% deionized water, stir and obtain facial film stock solution compositions; Above-mentioned facial film stock solution compositions is carried out magnetic agitation, and rotating speed is 150r/min, mixing time 13min, put into centrifuge separation afterwards and obtain facial film serosity, centrifuge speed is 11000r/min, then carries out quick-freezing sterilizing, Infrared Heating is recovered again, obtains facial film stock solution; Be that 1:120 dilutes facial film stock solution by stock solution and water volume ratio, inspection, bottling, obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
After patient with chloasma is got up early morning and before sleep, face is cleaned evening, get the present invention and be evenly sprayed to face, wash away after mistake 20min, use 20 days rear face chloasma obviously to reduce.
Take 20g Cortex Phellodendri, 15g Herba Taraxaci, 10g Radix Rubiae, and 20g Flos Lonicerae, put into the fragment that pulverizer breaks into 2cm, fragment is carried out supercritical carbon dioxide extraction 60min, extraction temperature is 65 DEG C, and extracting pressure is 15MPa; Take 40g Rhizoma Smilacis Glabrae again, 20g Radix Sangusorbae, 15g Radix Paeoniae Rubra, the 20g Fructus Kochiae and 20g Radix Isatidis, load in filtration paper cylinder after pulverizer is pulverized, filtration paper cylinder is put into cable type extractor according, and connects receiving flask, the ether that bottle amasss 2/3 is added in bottle, carry out condensing reflux, after extracting 12h, catcher is placed in baking oven and dries, ether is volatilized and separates out Chinese medicinal powder, oven temperature is 110 DEG C; By above-mentioned extraction and the Chinese medicinal powder mix homogeneously that extracts, and the deionized water and stirring adding its volume 10 times is even, for subsequent use; In blender, add 7% glycerol by mass percent, 6%1,3-butanediol, 0.3% hyaluronic acid, 4% Chinese medicine mixed liquor, 0.8% carbomer, 0.8% triethanolamine, 0.5% Polyethylene Glycol, 85% deionized water, stir and obtain facial film stock solution compositions; Above-mentioned facial film stock solution compositions is carried out magnetic agitation, and rotating speed is 200r/min, mixing time 15min, put into centrifuge separation afterwards and obtain facial film serosity, centrifuge speed is 12000r/min, then carries out quick-freezing sterilizing, Infrared Heating is recovered again, obtains facial film stock solution; Be that 1:150 dilutes facial film stock solution by stock solution and water volume ratio, inspection, bottling, obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
After patient with chloasma is got up early morning and before sleep, face is cleaned evening, get the present invention and be evenly sprayed to face, wash away after mistake 30min, use 30 days rear face chloasma obviously to reduce.
Claims (3)
1. a preparation method for functions of removing chloasma aerosol type facial mask liquid, is characterized in that concrete preparation process is:
(1) 10 ~ 20g Cortex Phellodendri is taken, 10 ~ 15g Herba Taraxaci, 5 ~ 10g Radix Rubiae, and 10 ~ 20g Flos Lonicerae, put into the fragment that pulverizer breaks into 1 ~ 2cm, fragment is carried out supercritical carbon dioxide extraction 30 ~ 60min, extraction temperature is 55 ~ 65 DEG C, and extracting pressure is 10 ~ 15MPa;
(2) 20 ~ 40g Rhizoma Smilacis Glabrae is taken again, 10 ~ 20g Radix Sangusorbae, 5 ~ 15g Radix Paeoniae Rubra, 10 ~ 20g Fructus Kochiae and 10 ~ 20g Radix Isatidis, load in filtration paper cylinder after pulverizer is pulverized, filtration paper cylinder is put into cable type extractor according, and connects receiving flask, the three filter ethane that bottle amasss 2/3 are added in receiving flask, carry out condensing reflux, after extracting 6 ~ 12h, catcher is placed in baking oven and dries, ether is volatilized and separates out Chinese medicinal powder, oven temperature is 105 ~ 110 DEG C;
(3) by above-mentioned extraction and the Chinese medicinal powder mix homogeneously that extracts, and the deionized water and stirring adding its volume 8 ~ 10 times is even, obtains Chinese medicine mixed liquor, for subsequent use;
(4) by mass percent 5 ~ 7% glycerol, 4 ~ 6%1,3-butanediol, 0.1 ~ 0.3% hyaluronic acid, 2 ~ 4% Chinese medicine mixed liquors, 0.5 ~ 0.8% carbomer, 0.5 ~ 0.8% triethanolamine, 0.3 ~ 0.5% Polyethylene Glycol, 80 ~ 85% deionized waters, stir and obtain facial film stock solution compositions;
(5) above-mentioned facial film stock solution compositions is carried out magnetic agitation, rotating speed is 100 ~ 200r/min, mixing time 10 ~ 15min, put into centrifuge separation afterwards and obtain facial film serosity, centrifuge speed is 10000 ~ 12000r/min, then carry out quick-freezing sterilizing, then Infrared Heating is recovered, and obtains facial film stock solution;
(7) be that 1:100 ~ 1:150 dilutes facial film stock solution by stock solution and water volume ratio, inspection, bottling, obtains a kind of functions of removing chloasma aerosol type facial mask liquid.
2. the preparation method of a kind of functions of removing chloasma aerosol type facial mask liquid according to claim 1, is characterized in that: described quick-freezing sterilizing methods utilizes liquid nitrogen to carry out instantaneous sterilizing at-40 ~-30 DEG C, sterilization time 10 ~ 15s.
3. the preparation method of a kind of functions of removing chloasma aerosol type facial mask liquid according to claim 1, it is characterized in that: described Infrared Heating temperature is 70 ~ 80 DEG C, the time is 20 ~ 30min.
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| CN201510469926.XA CN105012196A (en) | 2015-08-04 | 2015-08-04 | Method for preparing spray-type facial mask fluid for removing chloasma |
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| CN201510469926.XA CN105012196A (en) | 2015-08-04 | 2015-08-04 | Method for preparing spray-type facial mask fluid for removing chloasma |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726940A (en) * | 2016-12-19 | 2017-05-31 | 黄冈师范学院 | A kind of honeysuckle moisture-keeping bacterium-restraining spray and preparation method thereof |
| CN110772466A (en) * | 2019-08-29 | 2020-02-11 | 罗莹 | Preparation method of convenient traditional Chinese medicine mask |
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2015
- 2015-08-04 CN CN201510469926.XA patent/CN105012196A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106726940A (en) * | 2016-12-19 | 2017-05-31 | 黄冈师范学院 | A kind of honeysuckle moisture-keeping bacterium-restraining spray and preparation method thereof |
| CN110772466A (en) * | 2019-08-29 | 2020-02-11 | 罗莹 | Preparation method of convenient traditional Chinese medicine mask |
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Application publication date: 20151104 |