CN101658472B - Pure traditional Chinese medicine emulsifiable paste for whitening and protecting skin and preparation method thereof - Google Patents
Pure traditional Chinese medicine emulsifiable paste for whitening and protecting skin and preparation method thereof Download PDFInfo
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- CN101658472B CN101658472B CN2009100190170A CN200910019017A CN101658472B CN 101658472 B CN101658472 B CN 101658472B CN 2009100190170 A CN2009100190170 A CN 2009100190170A CN 200910019017 A CN200910019017 A CN 200910019017A CN 101658472 B CN101658472 B CN 101658472B
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Abstract
The invention discloses a pure traditional Chinese medicine emulsifiable paste for whitening and protecting skin and a preparation method thereof. The pure traditional Chinese medicine emulsifiable paste for whitening and protecting skin consists of 15-45 parts of rhizoma bletillae, 15-45 parts of radix angelicae, 15-45 parts of rhizoma typhonii, 5-20 parts of saponin, 5-30 parts of rhizoma nardostachyos, 40-75 parts of castor oil, 40-70 parts of stearic acid, 20-40 parts of monoglyceride, 100-150 parts of liquid paraffin, 5-15 parts of 10 percent of nipalgin ethyl alcohol solution, 100-150 parts of glycerine, and 400-500 parts of pure water. The preparation method comprises the following steps: preparing conventional dosage of essences; mixing and suspending main materials of an extracting liquid and volatile oil into a substrate to form the stable emulsifiable paste with evenness, semi-solid, fineness, and no thawing when coated on the skin, wherein particles with the diameter larger than 180 microns are not detected, and pathogenic bacterium or escherichia coli is not detected. The preparation method comprises the preparation of main materials, the preparation of auxiliary materials, the preparation of emulsifiable paste and quality inspection. Corresponding solvents are respectively used according to the properties of each component, the effective components of the traditional Chinese medicine are extracted by using a modern extraction process, and the extracts are sequentially added into the emulsifiable paste substrate, thereby completely reserving the effective components in the traditional Chinese medicine composite with even and fine components, proper viscosity, easy skin absorption, safe use, mild function and obvious effect.
Description
Technical field
The invention belongs to the emulsifiable paste category, particularly traditional Chinese medicine emulsifiable paste of a kind of whitening and skin-protecting and preparation method thereof.
Background technology
The whitening and skin-protecting product can change human body image, improves mental attitude, plays a part favourable to the health of human body.Along with the raising of people's living standard, its kind and use crowd also constantly increase.
Whitening and skin-protecting product category in the market is various, mostly is industrial chemicals or adds the chemical drugs that some brighten, as mequinol, vitamin C, lead, hydrargyrum etc.; Though these chemical constituents suppress the effect that melanin generates external showing, and often do not have identical curative effect in vivo; More there are some to have the chemical constituent of discoloration; as hydroquinone, can directly destroy human melanocyte, because human melanocyte can not regenerate and duplicate; make skin lose a kind of natural cover for defense of self-protection, still have dispute so various countries, the world use it at present.Therefore, not every whitening product is " skin protection " all, the effect that has or even reach " whitening " by the sacrifice skin health.The whitening product that prolonged application is so often can cause the generation of cosmetic dermatosis, as swashing dermatitis, allergy dermatitis, acne cosmetica etc., uses dangerous and high price.
From tcm theory, the people is an organic whole, and the health status of appearance and health has direct relation.The essence of beauty face-whitening-nourishing is exactly health preserving, and it relates to all many-sides such as diet, sleep, motion.Its Chinese medicine health preserving just comprised enrich blood, invigorate blood circulation, QI invigorating, warming YANG, yin nourishing, promoting the circulation of QI, heat clearing away or the like.In the square medicine that the existing skin protection of China is preserved youthful looks, but both controlling nocturnal emission with astringent drugs kidney tonifying of majority, but whitening and skin-protecting has again reached the dual purpose of health preserving and skin care.
In the prior art, the skin-protection product that has some to utilize the Chinese crude drug preparation, for example:
Patent No. ZL03132343.X, name is called " containing the brilliant compound additive of cosmetic and the preparation technology and the application in cosmetics of Herba Taraxaci, Pseudobulbus Bletillae (Rhizoma Bletillae) extract ", system extracts Herba Taraxaci ultrasonic water immersion method, macroporous resin adsorption ..., the Pseudobulbus Bletillae (Rhizoma Bletillae) is ground with colloid mill, supernatant adds edible ethanol and extracts ..., both mix the back homogenizing ....Emphasis is at bactericidal antiphlogistic, the medical material kind very little, effect is single.
Patent No. ZL200310110249.X name is called " anti-acne crinkle-removing whitening Chinese medicine facial film ", adopts the Chinese medicine Radix Angelicae Dahuricae, Pseudobulbus Bletillae (Rhizoma Bletillae), Radix Ampelopsis, Rhizoma Typhonii, Radix Trichosanthis, Rhizoma Polygonati Odorati, Rhizoma Ligustici, Rhizoma Chuanxiong, Semen Fructus Trichosanthis and Semen Armeniacae Amarum, drying, and crushing screening is made.Be the mixture of Chinese powder medicine,, affect the treatment, and use inconvenience the skin poor permeability.
Patent No. ZL200310112142.9, name is called " a kind of Chinese medicine freckle removing and whitening health product and preparation technology thereof ", it is Radix Polygoni Multiflori, 20 kinds of Chinese herbal medicine such as Radix Glycyrrhizae adopt supercritical, ultrasonic extraction to get the compound extracting thing, form with arbutin, vitamin C, natural Vitamin E, nanometer cysteine compatibility, traditional Chinese medicinal materials assortment is various, complicated process of preparation, and adding multiple industrial chemicals or chemical drugs, is not pure Chinese medicinal preparation.
Summary of the invention
The purpose of this invention is to provide pure traditional Chinese medicine emulsifiable paste of a kind of whitening and skin-protecting and preparation method thereof, it can remedy the above-mentioned deficiency of prior art.
Technical scheme of the present invention is: develops a kind of pure traditional Chinese medicine emulsifiable paste of whitening and skin-protecting, it is characterized in that forming by the raw material of following weight, wherein,
15～45 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 15～45 parts of the Radixs Angelicae Dahuricae, 15～45 parts of Rhizoma Typhoniis, 5～20 parts of Fructus Gleditsia, 5～30 parts of Radix Et Rhizoma Nardostachyos, 40～75 parts of Oleum Ricini, 40～70 parts of stearic acid, 20～40 parts of monoglycerides, 100～150 parts of liquid paraffin, 5～15 parts of 10% ethyl hydroxybenzoate alcoholic solutions, 400～500 parts of 100～150 parts of glycerol and pure water; The conventional addition of essence;
The emulsifiable paste character: major ingredient extracting solution and volatile oil are suspended in the substrate, form uniform semisolid, and exquisiteness is coated nonfused stable emulsifiable paste on the skin, must not detect the particle greater than 180 μ m; Must not detect pathogenic bacterium or escherichia coli.
The pure traditional Chinese medicine emulsifiable paste of above-mentioned a kind of whitening and skin-protecting is characterized in that being made up of the raw material of following weight, wherein,
25～35 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 25～35 parts of the Radixs Angelicae Dahuricae, 25～35 parts of Rhizoma Typhoniis, 5～15 parts of Fructus Gleditsia, 10～20 parts of Radix Et Rhizoma Nardostachyos, 50～65 parts of Oleum Ricini, 50～65 parts of stearic acid, 25～35 parts of monoglycerides, 100～150 parts of liquid paraffin, 8～12 parts of 10% ethyl hydroxybenzoate alcoholic solutions, 400～500 parts of 100～150 parts of glycerol and pure water; The conventional addition of essence;
The preparation method of the pure traditional Chinese medicine emulsifiable paste of above-mentioned a kind of whitening and skin-protecting is characterized in that branch does major ingredient preparation, the adjuvant preparation, and emulsifiable paste preparation and four steps of inspection quality inspection:
(1) major ingredient preparation
1. take by weighing the dosage Pseudobulbus Bletillae (Rhizoma Bletillae),, add 20～25 times of water gagings again and decoct 4h with submergence water gaging merceration 1h; It is 1/14～1/15 of amount of water that decoction liquor is concentrated into residual volume, gets the Pseudobulbus Bletillae (Rhizoma Bletillae) decoction liquor, standby;
2. take by weighing the dosage Radix Angelicae Dahuricae, be crushed to 10～30 orders, extract 3 times with 6～8 times of amount 75% ethanol room temperatures, 3h merges 3 times extracting solution at every turn, is concentrated into residual volume for 1/30～1/40 of alcohol amount, gets Radix Angelicae Dahuricae alcohol extract, and is standby;
3. take by weighing the dosage Fructus Gleditsia, with 8～10 times of water gaging lixiviates 3 times, each 3h merges 3 times lixiviating solution under the room temperature, and being concentrated into residual volume is 1/8～1/10 of amount of water, gets Fructus Gleditsia water extract, standby;
4. take by weighing the dosage Rhizoma Typhonii, be crushed to 80～100 orders, with 8～10 times of water gagings, heating in water bath extracts 2 times down, and each 1.5h merges the water extract twice, and being concentrated into residual volume is 1/8～1/10 of amount of water, gets Rhizoma Typhonii water extract, standby;
5. take by weighing the dosage Radix Et Rhizoma Nardostachyos, be crushed to 80～100 orders, conventional steam distillation method extracts volatile oil, gets Radix et Rhizoma Nardostachyos volatile oil, and is standby;
(2) adjuvant preparation
1. take by weighing dosage Oleum Ricini, liquid paraffin, stearic acid and monoglyceride respectively, mixing is heated to fusing, gets substrate mixture 1, and is standby;
2. take by weighing dosage 10% ethyl hydroxybenzoate alcoholic solution and glycerol respectively, mix the back and add the dosage pure water, be heated to molten after even substrate mixture 2, standby;
(3) emulsifiable paste preparation
Substrate mixture 1 is joined in the substrate mixture 2, and mixing is when treating that temperature is reduced to 45 ± 5 ℃, add the Pseudobulbus Bletillae (Rhizoma Bletillae) decoction liquor respectively, Radix Angelicae Dahuricae alcohol extract, Fructus Gleditsia water extract and Rhizoma Typhonii water extract, after stirring evenly, add Radix et Rhizoma Nardostachyos volatile oil and dosage essence again, continue to be stirred to evenly, stablize emulsifiable paste;
(4) quality inspection
Require to carry out quality inspection according to cosmetics, be the traditional Chinese medicine emulsifiable paste of whitening and skin-protecting after product is qualified.
In the major ingredient that the present invention uses:
Pseudobulbus Bletillae (Rhizoma Bletillae) (Rhizoma Bletillae) is the tuber of orchid Pseudobulbus Bletillae (Rhizoma Bletillae) bletillastriatareichb.f..Mucous matter 56.75%～60.15% wherein has multiple polysaccharide (for example, bletilla mannan etc.) also to contain volatile oil, starch.The nature and flavor hardship, sweet, puckery, cold; Go into lung, kidney two warps.Tool hemostasis, the protection gastric mucosa, prevention laboratory animal intestinal adhesion, antibiotic, antifungal:. effects such as anticancer and anti-cancer, and can play the effect of plasma substitute, animal experiment is harmless to liver, lungs.
Cosmetic applications: Pseudobulbus Bletillae (Rhizoma Bletillae) can light speckle skin protection, brighten clean skin, the consolidation convergence, smooth away wrinkles, and chloasma, comedo, pimples, facial microgroove are had tangible curative effect.
The Radix Angelicae Dahuricae (Radixngelicae Dahuricae) is the root of samphire Radix angelicae dahuricae Angelica dahurica (Fisch.exHoffm.) Benth.et Hook.f.var.formosana (Boiss.) Shan et Yuan.Contain isoimperatorin (isoimperatorin), imperatorin (imperatorin), bergapton (bergapten), phellopterin (phellopterin), oxypeucedanin (oxypeucedanin) etc.; Warm in nature, acrid in the mouth; Function cures mainly wind-damp dispelling, the evacuation of pus of invigorating blood circulation, granulation promoting pain relieving.Be used for headache, toothache, nasal sinusitis, hemorrhoidal hamorrhage anal fistula, leucorrhea with red and white discharge, ulcer sores, skin pruritus.Shennong's Herbal claims the Radix Angelicae Dahuricae that moist skin is arranged, the effect of tender crease-resistant and skin Caring.
From the modern medicine angle analysis, not only contain volatile oil in the Radix Angelicae Dahuricae, also contain the material that needed by human body that various skin can absorb is wanted, and the effect of certain antibacterial therapy is arranged. therefore, have sun-proof. the effect of anti-ultraviolet, can make skin pure white, promote the melanin metabolism, the effect of brightening light speckle.The Radix Angelicae Dahuricae fragrant color of distinguishing the flavor of is white, is one of ancient beauty treatment Chinese medicine, is that the cosmetics and the cosmetics of raw material emerge in an endless stream with it on the market, Radix Angelicae Dahuricae water decoction has certain inhibitory action to external various pathogens, but and microcirculation improvement, promote the metabolism of skin, delaying decrepitude of skin.
Rhizoma Typhonii (Rhizoma Typhonii Gigantei) is the dry tuber of aroid Herba Typhonii gigantei Typhonium giganteumEngl..Contain cupreol and glucose glycoside thereof, inositol, phlegmatic temperament, sucrose etc.The nature and flavor suffering, temperature; Poisonous.Return stomach, Liver Channel.The beauty functions of Rhizoma Typhonii mainly is a beautifying face, can be used for being used to whiten, the tinea versicolor of dispelling, keloid, acne.A lot of products have used Rhizoma Typhonii, and additive or antiseptic and skin care item usually are used for improving looks.
Fructus Gleditsia (Spina Gleditsiae) is the Spina jujubae of leguminous plant Fructus Gleditsia Gleditsia sinensis Lam.; Contain gleditschiasaponin B-G (gleditsiasaaponin B-G), Palmic acid (palmitic acid), hard ester acid, oleic acid, inferior sterol, sitosterol, nonacosane (nonacosane) etc.Nature and flavor: warm in nature, acrid in the mouth.The traditional Chinese medical science, how in the treatment acne, hordeolum is used during the movable blood soft hard eliminating stagnation.
" Mingyi Bielu " carries: " all kinds of diseases and ailments on the interarea "; " Japan hanako materia medica " carries: " controlling all cold wind gas, dough cover scar defect "; Compendium of Material Medica is carried: control the not white or facial dark brown speckle of dark complexion.
Radix Et Rhizoma Nardostachyos (Radix et Rhizoma Nardostachycis) is the root and rhizome of Valerianaceae herbaceos perennial Radix Et Rhizoma Nardostachyos Nardostachyschinensis Batal. or spoon Ye Gansong Nardostachys jatamansis (D.Don) DC..Dense, the main volatile oil, nature and flavor suffering of containing of fragranced; Sweet; The spleen of returning warm in nature; The stomach warp;
Ancient prescription records and brightens, and pleases face, and skin moistening prevents and treats xerosis cutis and controls the effect of skin pruritus due to dryness.
Oleum Ricini (Ricinus communis L.) for the mature seed of euphorbia plant Semen Ricini Ricinus communis L. through squeezing and the refining fatty oil that obtains.Contain protein about 18%.Sweet in the mouth; Hot; Property is put down; Return lung; Large intestine channel; The effect laxation; Skin moistening.
Ointment preparation technology's main feature is according to each constitutive property among the present invention, uses coordinative solvent respectively, and its extracts active ingredients is come out, and extract is joined in the emulsifiable paste matrix successively again.Wherein the Radix Et Rhizoma Nardostachyos main component is a volatile oil, has strong volatility, so its extract in the end adds with essence, with the loss of minimizing composition.The ointment of preparation according to the present invention, composition is even, fine and smooth, and viscosity is suitable, is easy to skin absorbs.
In the present invention, the major ingredient Radix Angelicae Dahuricae, Pseudobulbus Bletillae (Rhizoma Bletillae), Fructus Gleditsia, Rhizoma Typhonii, Radix Et Rhizoma Nardostachyos and Oleum Ricini are nontoxic composition, are conventional using dosage; Stearic acid, monoglyceride, liquid paraffin, 10% ethyl hydroxybenzoate alcoholic solution, glycerol, essence etc. are the substrate commonly used or the additive of ointment, and their safety is extensively verified already.Therefore, the present invention has higher-security.
Advantage of the present invention:
The modern extraction process of whitening and skin-protecting emulsifiable paste utilization of the present invention is come out the extracts active ingredients of whitening and skin-protecting in the Chinese medicine, and makes ointment, has both completely kept the effective ingredient in the Chinese medicine composition, and easy to use.
The present invention is pure Chinese medicine composition, has avoided the various infringements of chemical substance to human body skin fully, functional component comes from that the cosmetics of plant are safe in utilization because of it, action temperature and, effect is remarkable; When whitening, reached the purpose of skin protection.Have the advantages that zest is little, untoward reaction is few, easy to use.
The specific embodiment
Below in conjunction with embodiment the present invention is further set forth:
Embodiment 1
Dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 45g, Radix Angelicae Dahuricae 45g, Rhizoma Typhonii 45g, Fructus Gleditsia 20g, Radix Et Rhizoma Nardostachyos 30g, Oleum Ricini 75g, stearic acid 70g, monoglyceride 40g, liquid paraffin 150g, 10% ethyl hydroxybenzoate alcoholic solution 15g, glycerol 150g and pure water 500g; The conventional addition of essence;
The method for making branch is done the major ingredient preparation, the adjuvant preparation, and emulsifiable paste preparation and four steps of inspection quality inspection:
(1) major ingredient preparation
1. take by weighing the dosage Pseudobulbus Bletillae (Rhizoma Bletillae),, add 20～25 times of water gagings again and decoct 4h with submergence water gaging merceration 1h; It is 1/14～1/15 of amount of water that decoction liquor is concentrated into residual volume, gets the Pseudobulbus Bletillae (Rhizoma Bletillae) decoction liquor, standby;
2. take by weighing the dosage Radix Angelicae Dahuricae, be crushed to 10～30 orders, extract 3 times with 6～8 times of amount 75% ethanol room temperatures, 3h merges 3 times extracting solution at every turn, is concentrated into residual volume for 1/30～1/40 of alcohol amount, gets Radix Angelicae Dahuricae alcohol extract, and is standby;
3. take by weighing the dosage Fructus Gleditsia, with 8～10 times of water gaging lixiviates 3 times, each 3h merges 3 times lixiviating solution under the room temperature, and being concentrated into residual volume is 1/8～1/10 of amount of water, gets Fructus Gleditsia water extract, standby;
4. take by weighing the dosage Rhizoma Typhonii, be crushed to 80～100 orders, with 8～10 times of water gagings, heating in water bath extracts 2 times down, and each 1.5h merges the water extract twice, and being concentrated into residual volume is 1/8～1/10 of amount of water, gets Rhizoma Typhonii water extract, standby;
5. take by weighing the dosage Radix Et Rhizoma Nardostachyos, be crushed to 80～100 orders, conventional steam distillation method extracts volatile oil, gets Radix et Rhizoma Nardostachyos volatile oil, and is standby;
(2) adjuvant preparation
1. take by weighing dosage Oleum Ricini, liquid paraffin, stearic acid and monoglyceride respectively, mixing is heated to fusing, gets substrate mixture 1, and is standby;
2. take by weighing dosage 10% ethyl hydroxybenzoate alcoholic solution and glycerol respectively, mix the back and add the dosage pure water, be heated to molten after even substrate mixture 2, standby;
(3) emulsifiable paste preparation
Substrate mixture 1 is joined in the substrate mixture 2, and mixing is when treating that temperature is reduced to 45 ± 5 ℃, add the Pseudobulbus Bletillae (Rhizoma Bletillae) decoction liquor respectively, Radix Angelicae Dahuricae alcohol extract, Fructus Gleditsia water extract and Rhizoma Typhonii water extract, after stirring evenly, add Radix et Rhizoma Nardostachyos volatile oil and dosage essence again, continue to be stirred to evenly, stablize emulsifiable paste;
(4) quality inspection
Require to carry out quality inspection according to cosmetics, be the traditional Chinese medicine emulsifiable paste of whitening and skin-protecting after product is qualified.
Product emulsifiable paste character: major ingredient extracting solution and volatile oil are suspended in the substrate, form uniform semisolid, and exquisiteness is coated nonfused stable emulsifiable paste on the skin, detect by the pharmacopeia microbial limit test, do not detect the particle greater than 180 μ m; Do not detect pathogenic bacterium or escherichia coli.
The present invention adopts pure Chinese medicine composition according to the Chinese medical discrimination theory, and wherein Pseudobulbus Bletillae (Rhizoma Bletillae) is a monarch drug, and the Radix Angelicae Dahuricae and Fructus Gleditsia are ministerial drug, and Rhizoma Typhonii is an adjuvant drug, and Radix Et Rhizoma Nardostachyos is a messenger drug.Wherein, but the Pseudobulbus Bletillae (Rhizoma Bletillae) clearing away heat and expelling wind removes the speckle skin protection, makes us flesh and slides, and is the whitening and skin-protecting key medicine; Radix Angelicae Dahuricae expelling wind and removing dampness, sensible row table, the longue skin is moist, antipruritic; Fructus Gleditsia is warm in nature, but skin moistening closes face; Kind the loosing of the hot temperature of Rhizoma Typhonii, sick and row medicine gesture on can interarea; The hot fragrant row of Radix Et Rhizoma Nardostachyos looses, and is capable to help blood, can strengthen drug effect.Above-mentioned all medicines share, and can dispel the wind, moisten flesh, whiten, skin protection.The present invention verifies through long-term clinical application, and is remarkable to the whitening and skin-protecting effect, do not find untoward reaction so far.
Embodiment 2
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 15g, Radix Angelicae Dahuricae 15g, Rhizoma Typhonii 15g, Fructus Gleditsia 5g, Radix Et Rhizoma Nardostachyos 5g, Oleum Ricini 40g, stearic acid 40g, monoglyceride 20g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 5g, glycerol 100g and pure water 400g; The conventional addition of essence; All the other are with embodiment 1.
Embodiment 3
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 25g, Radix Angelicae Dahuricae 25g, Rhizoma Typhonii 25g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 10g, Oleum Ricini 50g, stearic acid 50g, monoglyceride 25g, liquid paraffin 120g, 10% ethyl hydroxybenzoate alcoholic solution 8g, glycerol 120g and pure water 430g; The conventional addition of essence; All the other are with embodiment 1.
Embodiment 4
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 35g, Radix Angelicae Dahuricae 35g, Rhizoma Typhonii 35g, Fructus Gleditsia 15g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 65g, stearic acid 65g, monoglyceride 35g, liquid paraffin 140g, 10% ethyl hydroxybenzoate alcoholic solution 12g, glycerol 140g and pure water 480g; The essence convention amount; All the other are with embodiment 1.
Embodiment 5
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 30g, Radix Angelicae Dahuricae 30g, Rhizoma Typhonii 30g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 10g, Oleum Ricini 60g, stearic acid 50g, monoglyceride 30g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 7g, glycerol 130g and pure water 440g; The essence convention amount; All the other are with embodiment 1.
Embodiment 6
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 20g, Radix Angelicae Dahuricae 30g, Rhizoma Typhonii 30g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 65g, stearic acid 50g, monoglyceride 35g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 15g, glycerol 100g and pure water 400g; The essence convention amount; All the other are with embodiment 1.
Embodiment 7
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 30g, Radix Angelicae Dahuricae 20g, Rhizoma Typhonii 30g, Fructus Gleditsia 15g, Radix Et Rhizoma Nardostachyos 10g, Oleum Ricini 75g, stearic acid 65g, monoglyceride 30g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 10g, glycerol 130g and pure water 450g; The essence convention amount; All the other are with embodiment 1.
Embodiment 8
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 35g, Radix Angelicae Dahuricae 25g, Rhizoma Typhonii 35g, Fructus Gleditsia 15g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 75g, stearic acid 65g, monoglyceride 25g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 15g, glycerol 150g and pure water 500g; The essence convention amount; All the other are with embodiment 1.
Embodiment 9
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 30g, Radix Angelicae Dahuricae 30g, Rhizoma Typhonii 30g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 10g, Oleum Ricini 75g, stearic acid 50g, monoglyceride 30g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 7g, glycerol 130g and pure water 440g; The essence convention amount; All the other are with embodiment 1.
Embodiment 10
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 35g, Radix Angelicae Dahuricae 35g, Rhizoma Typhonii 35g, Fructus Gleditsia 5g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 60g, stearic acid 55g, monoglyceride 30g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 5g, glycerol 100g and pure water 400g; The essence convention amount; All the other are with embodiment 1.
Embodiment 11
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 25g, Radix Angelicae Dahuricae 25g, Rhizoma Typhonii 45g, Fructus Gleditsia 15g, Radix Et Rhizoma Nardostachyos 10g, Oleum Ricini 50g, stearic acid 70g, monoglyceride 25g, liquid paraffin 110g, 10% ethyl hydroxybenzoate alcoholic solution 5g, glycerol 120g and pure water 430g; The essence convention amount; All the other are with embodiment 1.
Embodiment 12
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 45g, Radix Angelicae Dahuricae 45g, Rhizoma Typhonii 45g, Fructus Gleditsia 20g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 75g, stearic acid 40g, monoglyceride 40g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 12g, glycerol 150g and pure water 500g; The essence convention amount; All the other are with embodiment 1.
Embodiment 13
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 45g, Radix Angelicae Dahuricae 35g, Rhizoma Typhonii 15g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 40g, stearic acid 70g, monoglyceride 30g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 7g, glycerol 130g and pure water 440g; The essence convention amount; All the other are with embodiment 1.
Embodiment 14
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 45g, Radix Angelicae Dahuricae 45g, Rhizoma Typhonii 15g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 30g, Oleum Ricini 65g, stearic acid 60g, monoglyceride 40g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 15g, glycerol 100g and pure water 400g; The essence convention amount; All the other are with embodiment 1.
Embodiment 15
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 25g, Radix Angelicae Dahuricae 15g, Rhizoma Typhonii 30g, Fructus Gleditsia 18g, Radix Et Rhizoma Nardostachyos 20g, Oleum Ricini 60g, stearic acid 65g, monoglyceride 30g, liquid paraffin 120g, 10% ethyl hydroxybenzoate alcoholic solution 10g, glycerol 100g and pure water 500g; The essence convention amount; All the other are with embodiment 1.
Embodiment 16
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 35g, Radix Angelicae Dahuricae 45g, Rhizoma Typhonii 25g, Fructus Gleditsia 20g, Radix Et Rhizoma Nardostachyos 25g, Oleum Ricini 40g, stearic acid 75g, monoglyceride 40g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 15g, glycerol 150g and pure water 500g; The essence convention amount; All the other are with embodiment 1.
Embodiment 17
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 45g, Radix Angelicae Dahuricae 30g, Rhizoma Typhonii 20g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 10g, Oleum Ricini 65g, stearic acid 50g, monoglyceride 40g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 15g, glycerol 130g and pure water 440g; The essence convention amount; All the other are with embodiment 1.
Embodiment 18
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 15g, Radix Angelicae Dahuricae 45g, Rhizoma Typhonii 15g, Fructus Gleditsia 20g, Radix Et Rhizoma Nardostachyos 5g, Oleum Ricini 750g, stearic acid 40g, monoglyceride 40g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 5g, glycerol 100g and pure water 400g; The essence convention amount; All the other are with embodiment 1.
Embodiment 19
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 40g, Radix Angelicae Dahuricae 40g, Rhizoma Typhonii 40g, Fructus Gleditsia 10g, Radix Et Rhizoma Nardostachyos 15g, Oleum Ricini 75g, stearic acid 40g, monoglyceride 30g, liquid paraffin 140g, 10% ethyl hydroxybenzoate alcoholic solution 10g, glycerol 100g and pure water 400g; The essence convention amount; All the other are with embodiment 1.
Embodiment 20
Dosage: dosage: Pseudobulbus Bletillae (Rhizoma Bletillae) 35g, Radix Angelicae Dahuricae 25g, Rhizoma Typhonii 35g, Fructus Gleditsia 5g, Radix Et Rhizoma Nardostachyos 15g, Oleum Ricini 60g, stearic acid 75g, monoglyceride 30g, liquid paraffin 100g, 10% ethyl hydroxybenzoate alcoholic solution 10g, glycerol 150g and pure water 400g; The essence convention amount; All the other are with embodiment 1.
Claims (3)
1. the pure traditional Chinese medicine emulsifiable paste of a whitening and skin-protecting is characterized in that being made up of the raw material of following weight, wherein,
15～45 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 15～45 parts of the Radixs Angelicae Dahuricae, 15～45 parts of Rhizoma Typhoniis, 5～20 parts of Fructus Gleditsia, 5～30 parts of Radix Et Rhizoma Nardostachyos, 40～75 parts of Oleum Ricini, 40～70 parts of stearic acid, 20～40 parts of monoglycerides, 100～150 parts of liquid paraffin, 5～15 parts of 10% ethyl hydroxybenzoate alcoholic solutions, 400～500 parts of 100～150 parts of glycerol and pure water; The essence convention amount;
The emulsifiable paste character: major ingredient extracting solution and volatile oil are suspended in the substrate, form uniform semisolid, and exquisiteness is coated nonfused stable emulsifiable paste on the skin, must not detect the particle greater than 180 μ m; Must not detect pathogenic bacterium.
2. according to the pure traditional Chinese medicine emulsifiable paste of the described a kind of whitening and skin-protecting of claim 1, it is characterized in that forming by the raw material of following weight, wherein,
25～35 parts of Pseudobulbus Bletillae (Rhizoma Bletillae), 25～35 parts of the Radixs Angelicae Dahuricae, 25～35 parts of Rhizoma Typhoniis, 5～15 parts of Fructus Gleditsia, 10～20 parts of Radix Et Rhizoma Nardostachyos, 50～65 parts of Oleum Ricini, 50～65 parts of stearic acid, 25～35 parts of monoglycerides, 100～150 parts of liquid paraffin, 8～12 parts of 10% ethyl hydroxybenzoate alcoholic solutions, 400～500 parts of 100～150 parts of glycerol and pure water; The essence convention amount.
3. according to the preparation method of the pure traditional Chinese medicine emulsifiable paste of claim 1 or 2 described a kind of whitening and skin-protectings, it is characterized in that branch does the major ingredient preparation, the adjuvant preparation, emulsifiable paste preparation and quality inspection four go on foot:
(1) major ingredient preparation
1. take by weighing the dosage Pseudobulbus Bletillae (Rhizoma Bletillae),, add 20～25 times of water gagings again and decoct 4h with submergence water gaging merceration 1h; It is 1/14～1/15 of amount of water that decoction liquor is concentrated into residual volume, gets the Pseudobulbus Bletillae (Rhizoma Bletillae) decoction liquor, standby;
2. take by weighing the dosage Radix Angelicae Dahuricae, be crushed to 10～30 orders, extract 3 times with 6～8 times of amount 75% ethanol room temperatures, 3h merges 3 times extracting solution at every turn, is concentrated into residual volume for 1/30～1/40 of alcohol amount, gets Radix Angelicae Dahuricae alcohol extract, and is standby;
3. take by weighing the dosage Fructus Gleditsia, with 8～10 times of water gaging lixiviates 3 times, each 3h merges 3 times lixiviating solution under the room temperature, and being concentrated into residual volume is 1/8～1/10 of amount of water, gets Fructus Gleditsia water extract, standby;
4. take by weighing the dosage Rhizoma Typhonii, be crushed to 80～100 orders, with 8～10 times of water gagings, heating in water bath extracts 2 times down, and each 1.5h merges the water extract twice, and being concentrated into residual volume is 1/8～1/10 of amount of water, gets Rhizoma Typhonii water extract, standby;
5. take by weighing the dosage Radix Et Rhizoma Nardostachyos, be crushed to 80～100 orders, conventional steam distillation method extracts volatile oil, gets Radix et Rhizoma Nardostachyos volatile oil, and is standby;
(2) adjuvant preparation
1. take by weighing dosage Oleum Ricini, liquid paraffin, stearic acid and monoglyceride respectively, mixing is heated to fusing, gets substrate mixture 1, and is standby;
2. take by weighing dosage 10% ethyl hydroxybenzoate alcoholic solution and glycerol respectively, mix the back and add the dosage pure water, be heated to molten after even substrate mixture 2, standby;
(3) emulsifiable paste preparation
Substrate mixture 1 is joined in the substrate mixture 2, and mixing is when treating that temperature is reduced to 45 ± 5 ℃, add the Pseudobulbus Bletillae (Rhizoma Bletillae) decoction liquor respectively, Radix Angelicae Dahuricae alcohol extract, Fructus Gleditsia water extract and Rhizoma Typhonii water extract, after stirring evenly, add Radix et Rhizoma Nardostachyos volatile oil and dosage essence again, continue to be stirred to evenly, stablize emulsifiable paste;
(4) quality inspection
Require to carry out quality inspection according to cosmetics, be the traditional Chinese medicine emulsifiable paste of whitening and skin-protecting after product is qualified.
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| CN2009100190170A CN101658472B (en) | 2009-09-24 | 2009-09-24 | Pure traditional Chinese medicine emulsifiable paste for whitening and protecting skin and preparation method thereof |
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| CN2009100190170A CN101658472B (en) | 2009-09-24 | 2009-09-24 | Pure traditional Chinese medicine emulsifiable paste for whitening and protecting skin and preparation method thereof |
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| CN101658472B true CN101658472B (en) | 2011-09-21 |
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| CN104644646A (en) * | 2014-12-26 | 2015-05-27 | 青岛市市立医院 | Dexamethasone sodium phosphate urea cream and preparation method thereof |
| CN104855539A (en) * | 2015-05-07 | 2015-08-26 | 含山县昭关鹰皇油脂有限公司 | Anti-wrinkle beauty maintaining blend oil |
| CN108348562A (en) * | 2015-10-30 | 2018-07-31 | 安卡有限责任公司 | Treatment or the method for reducing skin disorder severity |
| CN117815096B (en) * | 2024-01-31 | 2024-09-24 | 华泽睿孚生物技术(广州)有限公司 | Moisturizing and repairing composition and application thereof |
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