CN104975523A - Preparation method of quick-dry wear-resisting textile fabric printing coating - Google Patents
Preparation method of quick-dry wear-resisting textile fabric printing coating Download PDFInfo
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- CN104975523A CN104975523A CN201510455298.XA CN201510455298A CN104975523A CN 104975523 A CN104975523 A CN 104975523A CN 201510455298 A CN201510455298 A CN 201510455298A CN 104975523 A CN104975523 A CN 104975523A
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- 239000011248 coating agent Substances 0.000 title claims abstract description 20
- 238000000576 coating method Methods 0.000 title claims abstract description 20
- 238000007639 printing Methods 0.000 title claims abstract description 17
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000004744 fabric Substances 0.000 title claims abstract description 8
- 239000004753 textile Substances 0.000 title claims abstract description 7
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 13
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 9
- 229920000180 alkyd Polymers 0.000 claims abstract description 7
- OMNKZBIFPJNNIO-UHFFFAOYSA-N n-(2-methyl-4-oxopentan-2-yl)prop-2-enamide Chemical compound CC(=O)CC(C)(C)NC(=O)C=C OMNKZBIFPJNNIO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 13
- 239000000049 pigment Substances 0.000 claims description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- LELOWRISYMNNSU-UHFFFAOYSA-N hydrogen cyanide Chemical compound N#C LELOWRISYMNNSU-UHFFFAOYSA-N 0.000 claims description 6
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 6
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 5
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 5
- 235000012216 bentonite Nutrition 0.000 claims description 5
- 239000008199 coating composition Substances 0.000 claims description 5
- 239000003085 diluting agent Substances 0.000 claims description 5
- 239000012153 distilled water Substances 0.000 claims description 5
- 229920005610 lignin Polymers 0.000 claims description 5
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 5
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 5
- 235000012239 silicon dioxide Nutrition 0.000 claims description 5
- 239000000377 silicon dioxide Substances 0.000 claims description 5
- 239000002562 thickening agent Substances 0.000 claims description 5
- -1 diacetone acrylamides Chemical class 0.000 claims description 4
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical class OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 3
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical class CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 3
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000006266 etherification reaction Methods 0.000 claims description 3
- 238000009413 insulation Methods 0.000 claims description 3
- JMMWKPVZQRWMSS-UHFFFAOYSA-N isopropyl acetate Chemical class CC(C)OC(C)=O JMMWKPVZQRWMSS-UHFFFAOYSA-N 0.000 claims description 3
- 125000005395 methacrylic acid group Chemical class 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 235000019698 starch Nutrition 0.000 claims description 3
- 238000001035 drying Methods 0.000 abstract description 11
- 230000002349 favourable effect Effects 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 5
- 238000012546 transfer Methods 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000010017 direct printing Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 239000003086 colorant Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000012858 packaging process Methods 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
The invention relates to a preparation method of a quick-dry wear-resisting textile fabric printing coating. For the coating disclosed by the invention, acrylic resin favorable for increasing coating drying rate and prepared by adopting a special process is adopted, and diacetone-acrylamide and alkyd resin are added, so that the drying rate of the coating is further increased.
Description
Technical field
The present invention relates to the preparation method of the wear-resisting printing coating for textile fabrics of a kind of rapid-curing cutback.
background of invention
Be coated with by look containing dyestuff or pigment and directly print to white or dye has on the fabric of ground colour, on dyestuff or pigment, dye is bonded to stamp part, thus obtains the printing method of various floral designs, is direct printing technique.The principle painted on fiber of coating direct printing is different from general dyestuff, and its nationality adhesive by insoluble granules of pigments set on the textile.The environmental protection of COAT PRINTING technique, without the need to washing, little to the restriction of fabric, technique is simple, and colorant match is convenient, and coloured light is easy to adjustment and controls, and the pattern profile of printing is clear, well arranged, be rich in third dimension.Its printing quality directly shows very clear on printing machine, and technical process is comparatively brief, and printing quality easily controls, and is a kind of very ripe and most widely used technique.
Along with the rise of clothes personalized customization cybertimes and e-commerce field are provided and delivered requirement timely, the rapid batch of personalized customization clothes produce and the requirement of packaging deliver goods more and more higher.This just require printing coating within the extremely short time can rapid draing firm, to avoid occurring that adhesion is stained when packing.But current COAT PRINTING its drying time, print after rub resistance in the short time, resistance to washing by rubbing with the hands property, heat-resisting stability poor, have impact on the development of clothes personalized customization.
Summary of the invention
For solving the problems referred to above of printing coating, present invention employs following technical scheme:
A preparation method for the wear-resisting printing coating for textile fabrics of rapid-curing cutback, comprises the steps:
A) following component is taken with weight parts: 10 parts of diacetone acrylamide, 15 parts of alkyd resins, 20 parts of acrylic resins, 40 parts of distilled water, 1 part of levelling agent, 2 parts of thickeners, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.5 parts of diluents etc., add in agitator, with the speed of 350 turns/min, abundant dispersed with stirring 30 minutes, treat that each component mixes, obtained mixed liquor;
B) 50 parts of pigment are taken with weight parts, 10 parts of silicon dioxide powders, 3 parts of bentonites, 10 parts of alumina powders, mix, then mixture is added in the obtained mixed liquor of step 1), add the lignin sulfonic acid of 3 weight portions, 4 parts of etherification starchs, mixer stirs 1 hour with the speed of 400 turns/min, fully grind through grinder again, filter and obtain coating composition;
Described acrylic resin is adopted and is obtained with the following method:
With weight parts, get 20 parts of ethanol, 20 parts of propyl alcohol, 15 parts of isopropyl acetates, add after mixing in reactor, with the ramp to 80 DEG C of about 5-10 DEG C/min, insulation 30min, then add 20 parts of ethyl acrylates, 10 parts of methacrylic acids, 15 parts of hydroxy-ethyl acrylates, 2 parts of diacetone acrylamides, 1 part of azo dicyclohexyl formonitrile HCN successively, be uniformly mixed, isothermal reaction 5 hours, be cooled to 30 DEG C, drip 1.5ml concentrated ammonia liquor, then stir 30min, obtain acrylic resin.
Described levelling agent is organosilicon levelling agent.
beneficial effect:
1) contain water-dispersible acrylic's resin in coating of the present invention, it has good adhesive force, and rate of drying is fast, and one of film-forming components that it can be used as coating, can significantly improve the rate of drying of coating serous coat.
2) also use the diacetone acrylamide being beneficial to and improving rate of drying and alkyd resins in coating of the present invention, itself and acrylic resin are worked in coordination with, and further increase the rate of drying of ink slurry.
3) rate of drying of the present invention water paint faster, obviously can reduce the pattern adhesion produced in the printing and packaging process that water paint rate of drying brings slowly, the quality problems such as stained, reduce production cost, there is actual application value pole.
4) rub resistance after coating of the present invention has good printing in the short time and resistance toly wash fastness by rubbing with the hands.
5) the present invention is not containing harmful substances such as formaldehyde, heavy metal and organotins, environmental protection, health.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described, but the scope of protection of present invention is not limited to the scope that embodiment is expressed.
embodiment 1
The preparation of acrylic resin:
With weight parts, get 20 parts of ethanol, 20 parts of propyl alcohol, 15 parts of isopropyl acetates, add after mixing in reactor, with the ramp to 80 DEG C of about 5-10 DEG C/min, insulation 30min, then add 20 parts of ethyl acrylates, 10 parts of methacrylic acids, 15 parts of hydroxy-ethyl acrylates, 2 parts of diacetone acrylamides, 1 part of azo dicyclohexyl formonitrile HCN successively, be uniformly mixed, isothermal reaction 5 hours, be cooled to 30 DEG C, drip 1.5ml concentrated ammonia liquor, then stir 30min, obtain acrylic resin.
The preparation of coating:
Following component is taken: 10 parts of diacetone acrylamide, 15 parts of alkyd resins, 20 parts of acrylic resins with weight parts, 40 parts of distilled water, 1 part of levelling agent, 2 parts of thickeners, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.5 parts of diluents etc., add in agitator, with the speed of 350 turns/min, abundant dispersed with stirring 30 minutes, treat that each component mixes, obtained mixed liquor;
50 parts of pigment are taken with weight parts, 10 parts of silicon dioxide powders, 3 parts of bentonites, 10 parts of alumina powders, mix, then mixture is added in the obtained mixed liquor of step 1), add the lignin sulfonic acid of 3 weight portions, 4 parts of etherification starchs, mixer stirs 1 hour with the speed of 400 turns/min, fully grind through grinder again, filter and obtain coating composition.
comparative example 1
Following component is taken: 25 parts of diacetone acrylamide with weight parts, 20 parts of alkyd resins, 40 parts of distilled water, 1 part of levelling agent, 1 part of thickener, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.3 parts of diluents, add in agitator, with the speed of 350 turns/min, abundant dispersed with stirring 30 minutes, treats that each component mixes, obtained mixed liquor;
50 parts of pigment are taken with weight parts, 10 parts of silicon dioxide powders, 3 parts of bentonites, 10 parts of alumina powders, mix, and are then added by mixture in aforementioned obtained mixed liquor, add the lignin sulfonic acid of 3 weight portions, mixer stirs 1 hour with the speed of 400 turns/min, more fully grinds through grinder, filters and obtains coating composition.
comparative example 2
Following component is taken: 25 parts of alkyd resins with weight parts, the acrylic resin that 20 parts of embodiments 1 are obtained, 40 parts of distilled water, 1 part of levelling agent, 1 part of thickener, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.3 parts of diluents, add in agitator, with the speed of 350 turns/min, abundant dispersed with stirring 30 minutes, treats that each component mixes, obtained mixed liquor.
50 parts of pigment are taken with weight parts, 10 parts of silicon dioxide powders, 3 parts of bentonites, 10 parts of alumina powders, mix, and are then added by mixture in aforementioned obtained mixed liquor, add the lignin sulfonic acid of 3 weight portions, mixer stirs 1 hour with the speed of 400 turns/min, more fully grinds through grinder, filters and obtains coating composition.
Carry out rate of drying, tack evaluation to above-mentioned each coating, result is as follows:
Drying property evaluation method: each coating is printed place 1 hour after printed matter, then stick covering paper tape and exert pressure, paper tape is opened, measure the pigment transfer amount on paper tape, evaluation is divided into 3 grades:
Good: almost without pigment transfer on paper tape; General: to only have local to have a small amount of pigment transfer on paper tape;
Difference: have many places and a large amount of pigment transfers on paper tape.
Claims (2)
1. a preparation method for the wear-resisting printing coating for textile fabrics of rapid-curing cutback, is characterized in that comprising the steps:
A) following component is taken with weight parts: 10 parts of diacetone acrylamide, 15 parts of alkyd resins, 20 parts of acrylic resins, 40 parts of distilled water, 1 part of levelling agent, 2 parts of thickeners, 0.5 part of fatty alcohol-polyoxyethylene ether, 1.5 parts of diluents etc., add in agitator, with the speed of 350 turns/min, abundant dispersed with stirring 30 minutes, treat that each component mixes, obtained mixed liquor;
B) 50 parts of pigment are taken with weight parts, 10 parts of silicon dioxide powders, 3 parts of bentonites, 10 parts of alumina powders, mix, then mixture is added in the obtained mixed liquor of step 1), add the lignin sulfonic acid of 3 weight portions, 4 parts of etherification starchs, mixer stirs 1 hour with the speed of 400 turns/min, fully grind through grinder again, filter and obtain coating composition;
Described acrylic resin is adopted and is obtained with the following method:
With weight parts, get 20 parts of ethanol, 20 parts of propyl alcohol, 15 parts of isopropyl acetates, add after mixing in reactor, with the ramp to 80 DEG C of about 5-10 DEG C/min, insulation 30min, then add 20 parts of ethyl acrylates, 10 parts of methacrylic acids, 15 parts of hydroxy-ethyl acrylates, 2 parts of diacetone acrylamides, 1 part of azo dicyclohexyl formonitrile HCN successively, be uniformly mixed, isothermal reaction 5 hours, be cooled to 30 DEG C, drip 1.5ml concentrated ammonia liquor, then stir 30min, obtain acrylic resin.
2. preparation method according to claim 1, is characterized in that: described levelling agent is organosilicon levelling agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510455298.XA CN104975523B (en) | 2015-07-30 | 2015-07-30 | Preparation method of quick-dry wear-resisting textile fabric printing coating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510455298.XA CN104975523B (en) | 2015-07-30 | 2015-07-30 | Preparation method of quick-dry wear-resisting textile fabric printing coating |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104975523A true CN104975523A (en) | 2015-10-14 |
| CN104975523B CN104975523B (en) | 2017-01-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510455298.XA Active CN104975523B (en) | 2015-07-30 | 2015-07-30 | Preparation method of quick-dry wear-resisting textile fabric printing coating |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104975523B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005001699A2 (en) * | 2003-06-26 | 2005-01-06 | Endress + Hauser Process Solutions Ag | Field bus distribution unit |
| US20100160496A1 (en) * | 2007-04-27 | 2010-06-24 | Jeong Woo Son | Acrylic acid ester copolymer composition and redispersible powders |
| CN102558989A (en) * | 2010-12-09 | 2012-07-11 | 海洋化工研究院 | Anti-fouling coating material with excellent compatibility and use thereof |
| CN103642305A (en) * | 2013-12-02 | 2014-03-19 | 安徽猛牛彩印包装有限公司 | High-bonding printing ink and preparation method thereof |
| CN104530872A (en) * | 2014-12-30 | 2015-04-22 | 佛山金智节能膜有限公司 | Intelligent temperature controlling coating with oriented structure and preparation method thereof |
-
2015
- 2015-07-30 CN CN201510455298.XA patent/CN104975523B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2005001699A2 (en) * | 2003-06-26 | 2005-01-06 | Endress + Hauser Process Solutions Ag | Field bus distribution unit |
| US20100160496A1 (en) * | 2007-04-27 | 2010-06-24 | Jeong Woo Son | Acrylic acid ester copolymer composition and redispersible powders |
| JP2010522798A (en) * | 2007-04-27 | 2010-07-08 | ヤング−ウー ケミテック カンパニーリミテッド | Acrylic ester copolymer composition and redispersible powder |
| CN102558989A (en) * | 2010-12-09 | 2012-07-11 | 海洋化工研究院 | Anti-fouling coating material with excellent compatibility and use thereof |
| CN103642305A (en) * | 2013-12-02 | 2014-03-19 | 安徽猛牛彩印包装有限公司 | High-bonding printing ink and preparation method thereof |
| CN104530872A (en) * | 2014-12-30 | 2015-04-22 | 佛山金智节能膜有限公司 | Intelligent temperature controlling coating with oriented structure and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN104975523B (en) | 2017-01-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wang Xiaoxia Inventor before: Jin Shuanglei |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20161018 Address after: Zhejiang province Jinhua City Xiguan Street 321000 Wucheng Dong Zhai community Dong Kang Lane 6, Room 203 Applicant after: JINHUA ZHICHAN WUYUAN INFORMATION TECHNOLOGY Co.,Ltd. Address before: 312000 Zhejiang city of Shaoxing province Zhuji city Jiyang street Jin Jin Road No. 9 Applicant before: Jin Shuanglei |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20190515 Address after: 432800 No. 86 Changzheng Road, Chengguan Town, Dawu County, Xiaogan City, Hubei Province Patentee after: DAWU GOLD SOURCE TEXTILES & GARMENTS CORP LTD. OF HUBEI Address before: 321000 Room 203, Dong Kang lane, Tung residence community, Xiguan Street, Wucheng District, Jinhua, Zhejiang, China. Patentee before: JINHUA ZHICHAN WUYUAN INFORMATION TECHNOLOGY Co.,Ltd. |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of fast drying and wear-resistant textile printing coating Effective date of registration: 20230824 Granted publication date: 20170111 Pledgee: Dawu sub branch of Bank of Hubei Co.,Ltd. Pledgor: DAWU GOLD SOURCE TEXTILES & GARMENTS CORP LTD. OF HUBEI Registration number: Y2023420000331 |