CN104958210A - Heat-removing fire-purging toothpaste and preparing method thereof - Google Patents

Heat-removing fire-purging toothpaste and preparing method thereof Download PDF

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Publication number
CN104958210A
CN104958210A CN201510358360.3A CN201510358360A CN104958210A CN 104958210 A CN104958210 A CN 104958210A CN 201510358360 A CN201510358360 A CN 201510358360A CN 104958210 A CN104958210 A CN 104958210A
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China
Prior art keywords
parts
toothpaste
fire
sodium
clearing away
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CN201510358360.3A
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Chinese (zh)
Inventor
吴克
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Priority to CN201510358360.3A priority Critical patent/CN104958210A/en
Publication of CN104958210A publication Critical patent/CN104958210A/en
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Abstract

The invention relates to heat-removing fire-purging toothpaste and a preparing method thereof. The toothpaste comprises the components, by weight, of 22-37 parts of modified silicon dioxide, 0.5-2.5 parts of sodium carboxymethylcellulose, 0.3-1.1 parts of sodium monofluorophosphate, 44-55 parts of aluminum oxide, 0.2-0.42 part of sodium dihydrogen phosphate, 0.15-0.45 part of trisodium phosphate, 0.01-0.05 part of isomaltose, 0.8-2.2 parts of xanthan gum, 0.03-0.07 part of azulene, 0.2-0.6 part of titanium dioxide, 13-22 parts of water, 10-20 parts of cape jasmine and 10-20 parts of lophatherum gracile. The toothpaste has the effects of tooth cleaning and ozostomia avoiding of common toothpaste and has the effects of heat removing, fire purging, blood cooling and detoxifying, and symptoms such as mouth and tongue sores, thirst and dysphoria can be treated.

Description

A kind of clearing away heat-fire toothpaste and preparation method thereof
Technical field
The present invention relates to body care articles for use technical field, particularly relate to a kind of clearing away heat-fire toothpaste and preparation method thereof.
Background technology
Toothpaste is cleaning supplies conventional in daily life, has very long history.Along with the development of science and technology, technological equipment update and perfect, various types of toothpaste is come out one after another, quality and the class of product improve constantly, present toothpaste variety by single clean type toothpaste, develops into great variety of goods, diverse in function, the Mobyneb toothpaste of up to a hundred brands, meets the needs of different levels level of consumption.
But current existing toothpaste does not have effect of clearing away heat-fire, removing pathogenic heat from blood and toxic substance from the body, treatment aphtha of the mouth and tongue, thirsty can not be used for.Such as Chinese invention patent (the patent No. 201410627907.0, applying date 2014.11.11) disclose one and to dispel halitosis Chinese herbal toothpaste, it is made up of following weight parts proportioning raw materials: Herba Menthae 5-15 part, Herba Eupatorii 10-20 part, Herba Lysimachiae 5-15 part, Bulbus Fritillariae Cirrhosae 15-25 part, Aloe 5-15 part, Borneolum Syntheticum 15-25 part, Flos Chrysanthemi Indici 10-20 part, Radix Rehmanniae 15-25 part.The present invention is scientific and reasonable, cost is low, preparation method is simple, effectively can kill the antibacterial in oral cavity, and can eliminate halitosis and other oral inflammations, clean taste during use, free from extraneous odour.
Summary of the invention
the technical problem solved:not there is for existing toothpaste the shortcoming of clearing away heat-fire, removing pathogenic heat from blood and toxic substance from the body effect, the invention provides a kind of clearing away heat-fire toothpaste and preparation method thereof.
technical scheme:a kind of clearing away heat-fire toothpaste, in mass parts containing following composition: improved silica 22 ~ 37 parts, sodium carboxymethyl cellulose 0.5 ~ 2.5 part, sodium monofluorophosphate 0.3 ~ 1.1 part, aluminium oxide 44 ~ 55 parts, sodium dihydrogen phosphate 0.2 ~ 0.42 part, tertiary sodium phosphate 0.15 ~ 0.45 part, dextrinose 0.01 ~ 0.05 part, HANSHENGJIAO 0.8 ~ 2.2 part, azulenes 0.03 ~ 0.07 part, titanium white 0.2 ~ 0.6 part, 13 ~ 22 parts, water, Fructus Gardeniae 10 ~ 20 parts, Herba Lophatheri 10 ~ 20 parts.
A kind of clearing away heat-fire toothpaste described above, in mass parts containing following composition: improved silica 25 ~ 35 parts, sodium carboxymethyl cellulose 0.8 ~ 2.2 part, sodium monofluorophosphate 0.5 ~ 1 part, aluminium oxide 47 ~ 52 parts, sodium dihydrogen phosphate 0.26 ~ 0.38 part, tertiary sodium phosphate 0.2 ~ 0.4 part, dextrinose 0.02 ~ 0.04 part, HANSHENGJIAO 1.1 ~ 2 parts, azulenes 0.04 ~ 0.065 part, titanium white 0.3 ~ 0.5 part, 15 ~ 21 parts, water, Fructus Gardeniae 12 ~ 19 parts, Herba Lophatheri 12 ~ 18 parts.
A kind of clearing away heat-fire toothpaste described above, in mass parts containing following composition: improved silica 27 parts, sodium carboxymethyl cellulose 1.2 parts, sodium monofluorophosphate 0.6 part, aluminium oxide 49 parts, sodium dihydrogen phosphate 0.29 part, tertiary sodium phosphate 0.25 part, dextrinose 0.028 part, HANSHENGJIAO 1.4 parts, azulenes 0.047 part, titanium white 0.35 part, 17 parts, water, Fructus Gardeniae 13 parts, Herba Lophatheri 14 parts.
A kind of clearing away heat-fire toothpaste described above, in mass parts containing following composition: improved silica 30 parts, sodium carboxymethyl cellulose 1.5 parts, sodium monofluorophosphate 0.8 part, aluminium oxide 50 parts, sodium dihydrogen phosphate 0.32 part, tertiary sodium phosphate 0.3 part, dextrinose 0.03 part, HANSHENGJIAO 1.6 parts, azulenes 0.054 part, titanium white 0.4 part, 18 parts, water, Fructus Gardeniae 15 parts, Herba Lophatheri 15 parts.
The preparation method of a kind of clearing away heat-fire toothpaste described above, the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 50 ~ 70 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 190 ~ 210 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 10 ~ 20min, obtain clearing away heat-fire toothpaste.
60 DEG C are warming up in the first step described above.
In second step described above, Fructus Gardeniae and Herba Lophatheri are crushed to 200 orders respectively.
Vacuum outgas 15min is used in the 3rd step described above.
beneficial effect:a kind of clearing away heat-fire toothpaste provided by the invention and preparation method thereof, this toothpaste except have ordinary toothpaste cleaning teeth, prevent the effect of halitosis except, also there is effect of clearing away heat-fire, removing pathogenic heat from blood and toxic substance from the body, the symptoms such as aphtha of the mouth and tongue, thirsty, vexed gas is hot-tempered can be treated.
Detailed description of the invention
embodiment 1
A kind of clearing away heat-fire toothpaste, in mass parts containing following composition: improved silica 22 parts, sodium carboxymethyl cellulose 0.5 part, sodium monofluorophosphate 0.3 part, aluminium oxide 44 parts, sodium dihydrogen phosphate 0.2 part, tertiary sodium phosphate 0.15 part, dextrinose 0.01 part, HANSHENGJIAO 0.8 part, azulenes 0.03 part, titanium white 0.2 part, 13 parts, water, Fructus Gardeniae 10 parts, Herba Lophatheri 10 parts.
A preparation method for clearing away heat-fire toothpaste, the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 50 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 190 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 10min, obtain clearing away heat-fire toothpaste.
embodiment 2
A kind of clearing away heat-fire toothpaste, in mass parts containing following composition: improved silica 37 parts, sodium carboxymethyl cellulose 2.5 parts, sodium monofluorophosphate 1.1 parts, aluminium oxide 55 parts, sodium dihydrogen phosphate 0.42 part, tertiary sodium phosphate 0.45 part, dextrinose 0.05 part, HANSHENGJIAO 2.2 parts, azulenes 0.07 part, titanium white 0.6 part, 22 parts, water, Fructus Gardeniae 20 parts, Herba Lophatheri 20 parts.
A preparation method for clearing away heat-fire toothpaste, the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 70 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 210 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 20min, obtain clearing away heat-fire toothpaste.
embodiment 3
A kind of clearing away heat-fire toothpaste, in mass parts containing following composition: improved silica 35 parts, sodium carboxymethyl cellulose 2.2 parts, sodium monofluorophosphate 1 part, aluminium oxide 52 parts, sodium dihydrogen phosphate 0.38 part, tertiary sodium phosphate 0.4 part, dextrinose 0.04 part, HANSHENGJIAO 2 parts, azulenes 0.04 ~ 0.065 part, titanium white 0.5 part, 21 parts, water, Fructus Gardeniae 19 parts, Herba Lophatheri 18 parts.
A preparation method for clearing away heat-fire toothpaste, the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 60 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 200 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 15min, obtain clearing away heat-fire toothpaste.
embodiment 4
A kind of clearing away heat-fire toothpaste, in mass parts containing following composition: improved silica 27 parts, sodium carboxymethyl cellulose 1.2 parts, sodium monofluorophosphate 0.6 part, aluminium oxide 49 parts, sodium dihydrogen phosphate 0.29 part, tertiary sodium phosphate 0.25 part, dextrinose 0.028 part, HANSHENGJIAO 1.4 parts, azulenes 0.047 part, titanium white 0.35 part, 17 parts, water, Fructus Gardeniae 13 parts, Herba Lophatheri 14 parts.
A preparation method for clearing away heat-fire toothpaste, the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 60 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 200 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 15min, obtain clearing away heat-fire toothpaste.
embodiment 5
A kind of clearing away heat-fire toothpaste, in mass parts containing following composition: improved silica 30 parts, sodium carboxymethyl cellulose 1.5 parts, sodium monofluorophosphate 0.8 part, aluminium oxide 50 parts, sodium dihydrogen phosphate 0.32 part, tertiary sodium phosphate 0.3 part, dextrinose 0.03 part, HANSHENGJIAO 1.6 parts, azulenes 0.054 part, titanium white 0.4 part, 18 parts, water, Fructus Gardeniae 15 parts, Herba Lophatheri 15 parts.
A preparation method for clearing away heat-fire toothpaste, the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 60 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 200 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 15min, obtain clearing away heat-fire toothpaste.
comparative example 1
Patent of invention publication number is the patent of CN 104288063 A, comprises following content:
One treats chronic otitis media Chinese medicine external liquid, is prepared from (every part of 1g) according to the raw material of weight portion by following component: Herba Menthae 5 parts, Herba Eupatorii 10 parts, Herba Lysimachiae 5 parts, Bulbus Fritillariae Cirrhosae 15 parts, Aloe 5 parts, Borneolum Syntheticum 15 parts, Flos Chrysanthemi Indici 10 parts, Radix Rehmanniae 15 parts.
Above medical material adds water 5-6 doubly by gross weight, and temperature fire decocts 3-4 hour, and collecting decoction after decocting twice filters, is concentrated into the paste that relative density is 1.32-1.40, then dry, pulverize into fine powder below 80 degree, add adjuvant, and mixing, makes ointment.
In 6 mouths, the patient of the long ulcer having degree identical uses the toothpaste of embodiment 1-5 and comparative example 1 respectively, sooner or later each brush tooth, and observation ulcer situation is as follows:
Use embodiment 1 toothpaste patient use after 3 days pain alleviate, fully recover after 5 days.
Use embodiment 1 toothpaste patient use after 3 days pain alleviate, fully recover after 4 days.
Use embodiment 1 toothpaste patient use after 2 days pain alleviate, fully recover after 4 days.
Use embodiment 1 toothpaste patient use after 2 days pain alleviate, fully recover after 4 days.
Use embodiment 1 toothpaste patient use after 2 days pain alleviate, fully recover after 3 days.
The patient of the toothpaste of comparative example 1 is used not act on ulcer after a procedure.
Above the embodiment of the present invention is described in detail, for one of ordinary skill in the art, according to the thought of the embodiment of the present invention, all will change in specific embodiments and applications, in sum, this description should not be construed as limitation of the present invention.

Claims (8)

1. a clearing away heat-fire toothpaste, to is characterized in that in mass parts containing following composition: improved silica 22 ~ 37 parts, sodium carboxymethyl cellulose 0.5 ~ 2.5 part, sodium monofluorophosphate 0.3 ~ 1.1 part, aluminium oxide 44 ~ 55 parts, sodium dihydrogen phosphate 0.2 ~ 0.42 part, tertiary sodium phosphate 0.15 ~ 0.45 part, dextrinose 0.01 ~ 0.05 part, HANSHENGJIAO 0.8 ~ 2.2 part, azulenes 0.03 ~ 0.07 part, titanium white 0.2 ~ 0.6 part, 13 ~ 22 parts, water, Fructus Gardeniae 10 ~ 20 parts, Herba Lophatheri 10 ~ 20 parts.
2. a kind of clearing away heat-fire toothpaste according to claim 1, to it is characterized in that in mass parts containing following composition: improved silica 25 ~ 35 parts, sodium carboxymethyl cellulose 0.8 ~ 2.2 part, sodium monofluorophosphate 0.5 ~ 1 part, aluminium oxide 47 ~ 52 parts, sodium dihydrogen phosphate 0.26 ~ 0.38 part, tertiary sodium phosphate 0.2 ~ 0.4 part, dextrinose 0.02 ~ 0.04 part, HANSHENGJIAO 1.1 ~ 2 parts, azulenes 0.04 ~ 0.065 part, titanium white 0.3 ~ 0.5 part, 15 ~ 21 parts, water, Fructus Gardeniae 12 ~ 19 parts, Herba Lophatheri 12 ~ 18 parts.
3. a kind of clearing away heat-fire toothpaste according to claim 1, to is characterized in that in mass parts containing following composition: improved silica 27 parts, sodium carboxymethyl cellulose 1.2 parts, sodium monofluorophosphate 0.6 part, aluminium oxide 49 parts, sodium dihydrogen phosphate 0.29 part, tertiary sodium phosphate 0.25 part, dextrinose 0.028 part, HANSHENGJIAO 1.4 parts, azulenes 0.047 part, titanium white 0.35 part, 17 parts, water, Fructus Gardeniae 13 parts, Herba Lophatheri 14 parts.
4. a kind of clearing away heat-fire toothpaste according to claim 1, to is characterized in that in mass parts containing following composition: improved silica 30 parts, sodium carboxymethyl cellulose 1.5 parts, sodium monofluorophosphate 0.8 part, aluminium oxide 50 parts, sodium dihydrogen phosphate 0.32 part, tertiary sodium phosphate 0.3 part, dextrinose 0.03 part, HANSHENGJIAO 1.6 parts, azulenes 0.054 part, titanium white 0.4 part, 18 parts, water, Fructus Gardeniae 15 parts, Herba Lophatheri 15 parts.
5. the preparation method of a kind of clearing away heat-fire toothpaste as claimed in claim 1, is characterized in that the preparation process of the method is as follows:
The first step: by improved silica and sodium carboxymethyl cellulose mix homogeneously, be warming up to 50 ~ 70 DEG C, add sodium dihydrogen phosphate, tertiary sodium phosphate, dextrinose, HANSHENGJIAO, azulenes, water again, room temperature is cooled to after mix homogeneously, add sodium monofluorophosphate, aluminium oxide, titanium white, after mix homogeneously, be kneaded into mastic;
Second step: Fructus Gardeniae and Herba Lophatheri are crushed to 190 ~ 210 orders respectively, then joins together and grinds in alms bowl, be ground into slurry like material;
3rd step: grind after mastic obtained above and slurry like material mix homogeneously, then use vacuum outgas 10 ~ 20min, obtain clearing away heat-fire toothpaste.
6. the preparation method of a kind of clearing away heat-fire toothpaste according to claim 5, is characterized in that: be warming up to 60 DEG C in the described first step.
7. the preparation method of a kind of clearing away heat-fire toothpaste according to claim 5, is characterized in that: in described second step, Fructus Gardeniae and Herba Lophatheri are crushed to 200 orders respectively.
8. the preparation method of a kind of clearing away heat-fire toothpaste according to claim 5, is characterized in that: use vacuum outgas 15min in the 3rd described step.
CN201510358360.3A 2015-06-26 2015-06-26 Heat-removing fire-purging toothpaste and preparing method thereof Pending CN104958210A (en)

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CN103054741A (en) * 2011-10-21 2013-04-24 汤治强 Tooth beatifying toothpaste
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101502482A (en) * 2009-03-27 2009-08-12 玉溪健坤生物药业有限公司 Toothpaste containing coenzyme Q10 and preparation method thereof
CN101697942A (en) * 2009-11-03 2010-04-28 广东名臣有限公司 Oral-care toothpaste composition
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CN103054741A (en) * 2011-10-21 2013-04-24 汤治强 Tooth beatifying toothpaste
CN102488849A (en) * 2011-12-28 2012-06-13 张君 Traditional Chinese medicine composition used for treating periodontitis
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