CN104861768A - Acanthopanax sessiliflorus seem berry anthocyanin edible ink and preparation method - Google Patents
Acanthopanax sessiliflorus seem berry anthocyanin edible ink and preparation method Download PDFInfo
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- CN104861768A CN104861768A CN201510295041.2A CN201510295041A CN104861768A CN 104861768 A CN104861768 A CN 104861768A CN 201510295041 A CN201510295041 A CN 201510295041A CN 104861768 A CN104861768 A CN 104861768A
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- edible ink
- berry anthocyanin
- edible
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/06—Printing inks based on fatty oils
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- Organic Chemistry (AREA)
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- General Chemical & Material Sciences (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to an environment-friendly ink and a preparation method, particularly to an acanthopanax sessiliflorus seem berry anthocyanin edible ink and a preparation method. The acanthopanax sessiliflorus seem berry anthocyanin edible ink is prepared from the following raw materials in percentage by weight: 0.5-5% of acanthopanax sessiliflorus seem berry anthocyanin, 92-99.3% of a connecting material, and 0.2-3% of an auxiliary; the connecting material adopts 15-60% of edible oil, 20-40% of fine white sugar and 15-60% of water. Ingredients in the formula of the acanthopanax sessiliflorus seem berry anthocyanin edible ink are all selected from natural substances, so that the acanthopanax sessiliflorus seem berry anthocyanin edible ink does not contain chemosynthesis additives and volatile organic compounds which are contained in a conventional ink, is pollution-free, has the fruity flavor taste of acanthopanax sessiliflorus seem, has no other peculiar smell, is safe to eat, and is harmless to the health of a human body. The method has the characteristics of being simple in operating technology, short in consumed time, good in emulsifying effect, safe to eat, bright and natural in color, good in printing performance, low in cost, smaller in investment, and the like, and is suitable for industrialized production.
Description
technical field
The present invention relates to a kind of environment-friendly ink and preparation method, especially a kind of Sessileflower Acanthopanax Bark berry anthocyanin edible ink and preparation method.
Background technology
In the prior art, ink plays very important effect in printing, packaging and sales process, and colourful ink printing not only can beautify commodity, and can also attract human consumer, promotion.But containing a large amount of volatile organic matter (Volatile Organic Compounds such as toluene, dimethylbenzene, turps, alcohols, aromatic series compounds in traditional ink, VOCs), in printing and drying process, VOCs is volatile in air, contaminate environment, to be detrimental to health, there is the symptom such as Nausea and vomiting, headache, even cause liver, kidney, brain and neural damage, bring out cancer.Therefore, the content effectively controlling VOCs in ink is the study hotspot of ink industry.In recent years, people turn to goal in research not containing the vegetables oil fundamental mode environment-friendly ink of VOCs, as water color ink, UV curing inks, although this kind of ink meets the standard of environment-friendly ink in VOCs and heavy metal content, but still can not directly be printed in food, healthcare products, drug substance surface or wrapping material, edible requirement cannot be met.
Along with people are to the continuous attention of food safety, the safety issue of ink becomes increasingly conspicuous, if the environment-friendly type edible ink that directly can be printed in food surfaces can be produced, ink not only effectively can be avoided the harm of HUMAN HEALTH and environment, but also the decorative effect of food surfaces, exploitation character product can be increased, attract the eyeball of human consumer.Edible ink without benzene, environmental protection is future development from now on.
Edible ink, as a kind of novel environment-friendlyink ink, not only requires it printing performance possessing traditional ink, chromatic colour, faster rate of drying, preferably sticking power and certain stability, but also need guarantee the edible safety of human consumer.Less for the correlative study of edible ink at present, on the one hand, there is the shortcoming such as length consuming time, emulsifying effectiveness difference in the mode emulsified inks such as the many employing stirrings of existing edible ink, grinding; On the other hand, many auxiliary agents containing more chemical composition in existing edible ink formula, are difficult to reach edible nontoxic requirement, limit it and further apply.
At present, about the preparation method of Sessileflower Acanthopanax Bark berry anthocyanin edible ink has no report.
Summary of the invention
The object of the invention is to provide for above-mentioned deficiency that a kind of environmental protection, printing performance are good, the Sessileflower Acanthopanax Bark berry anthocyanin edible ink of rational technology and preparation method.
Technical solution of the present invention is: Sessileflower Acanthopanax Bark berry anthocyanin edible ink, and it is made up of the raw material of following weight:
Sessileflower Acanthopanax Bark berry anthocyanin 0.5-5%, binder 92-99.3%, auxiliary agent 0.2-3%; Described binder is 15-60% edible oil, 20-40% caster sugar and 15-60% water.Edible oil can be soybean oil, sunflower seed oil, Semen Maydis oil, peanut oil, olive wet goods.Changbaishan area Sessileflower Acanthopanax Bark aboundresources; cultivated area increases year by year; fruit of Acanthopanax sessiliflorus is as new resource for food; be a kind of integration of drinking and medicinal herbs food, Sessileflower Acanthopanax Bark berry anthocyanin has anti-oxidant, anti-mutation, antitumor, radioprotective, protection cardiovascular and cerebrovascular, protects liver, improves the effects such as eyesight.
Described auxiliary agent is emulsifying agent 0.1-1.5% and thickening material 0.1-1.5%.
Described emulsifying agent is Yelkin TTS or soybean protein, and described thickening material is xanthan gum or sodium alginate.
Sessileflower Acanthopanax Bark berry anthocyanin edible ink, is made up of the raw material of following weight: the fruit of Acanthopanax sessiliflorus anthocyanogen of 1%, soybean oil 34.1%, Yelkin TTS 0.5%, caster sugar 30%, water 34.1% and xanthan gum 0.3%.
The preparation method of Sessileflower Acanthopanax Bark berry anthocyanin edible ink, its step is as follows: the edible oil binder of oiliness mixed with emulsifying agent, heat, dissolve and make oil base; Remaining caster sugar, water binder are mixed with thickening material, adds colorant Sessileflower Acanthopanax Bark berry anthocyanin after dissolving, after stirring, add oil base, after emulsification, cooling, obtain product.
Described emulsification method is ultrasonic wave-microwave cooperating emulsification, ultrasonic power 100-900w, microwave power 100-600w, emulsifying temperature 30-60 DEG C, emulsification times 5-30min.The heat effect of hyperacoustic cavitation effect and microwave is acted on Sessileflower Acanthopanax Bark berry anthocyanin edible ink simultaneously, the effect of create coupling, working in coordination with, superposing, the electrostatic double layer at rapid damage water-oily interface, accelerates the emulsifying effect of oil and water, shorten emulsification times, strengthen emulsifying effectiveness.
The preparation method of Sessileflower Acanthopanax Bark berry anthocyanin edible ink, is by the soybean oil of 34.1% and the mixing of 0.5% Yelkin TTS, heating, dissolves and make oil base; The fruit of Acanthopanax sessiliflorus anthocyanogen of 1% is added after getting the caster sugar of 30%, the water of 34.1% and 0.3% xanthan gum mixed dissolution, oil base is added after stirring, ultrasonic-microwave cooperating emulsification 20min under ultrasonic power 200W, microwave power 300W, the condition of 50 DEG C, obtains product after cooling
Advantage of the present invention is: all the components 1, in Sessileflower Acanthopanax Bark berry anthocyanin edible ink formula all derives from crude substance, without the chemosynthesis additive contained by conventional printing ink and volatile organic matter, pollution-free, to have Sessileflower Acanthopanax Bark fruital taste and without other peculiar smell, edible safety, is harmful to human health.2, ultrasonic wave-microwave cooperating emulsification Sessileflower Acanthopanax Bark berry anthocyanin edible ink is adopted, short, emulsify well consuming time.This is because the microwave heating effect that hyperacoustic cavitation effect and waveguide are drawn can be directly acted on Sessileflower Acanthopanax Bark berry anthocyanin edible ink by this method, carry out common coupling, work in coordination with, create the effect of superposition strengthening, in addition, in Sessileflower Acanthopanax Bark berry anthocyanin edible ink system, water can rotate under the effect at microwave as polar molecule, destroy the electrostatic double layer at water-oily interface, the chance that disperse phase is polymerized increases, accelerate the emulsifying effect of oil and water, thus substantially reduce emulsification times.3, adopt the mode of silk screen printing, Sessileflower Acanthopanax Bark berry anthocyanin edible ink has good transitivity, tack and printing effect at food surfaces, clear picture, without wire drawing, dizzy dye phenomenon, the soft nature of color, has certain decorative effect, can realize original copy preferably and reproduce.Sessileflower Acanthopanax Bark berry anthocyanin edible ink can meet the requirement of silk screen printing, not only pattern, word etc. directly can be printed in food, directly edible as food surfaces decoration, solve the safety issue of traditional ink, and can also be attractive attention, improve product specification, meet the pursuit of people to personalized food.4, present method has the advantage such as operating procedure simple, consuming time short, emulsify well, edible safety, bright-colored natural, printing performance good, cost is low, less investment, is applicable to suitability for industrialized production
.
Below in conjunction with embodiment, embodiments of the present invention are described in further detail.
Embodiment
Embodiment 1:
By the soybean oil of 34.1% and the mixing of 0.5% Yelkin TTS, heating, dissolve and make oil base; The fruit of Acanthopanax sessiliflorus anthocyanogen of 1% is added after getting the caster sugar of 30%, the water of 34.1% and 0.3% xanthan gum mixed dissolution, oil base is added after stirring, ultrasonic-microwave cooperating emulsification 20min under ultrasonic power 200W, microwave power 300W, the condition of 50 DEG C, obtains product after cooling.
Embodiment 2:
By the soybean oil of 27% and the mixing of 0.5% soybean protein, heating, dissolve and make oil base; Get the caster sugar of 40%, 3 0% water and 0.5% sodium alginate mixed dissolution after add 2% fruit of Acanthopanax sessiliflorus anthocyanogen, oil base is added after stirring, ultrasonic-microwave cooperating emulsification 10min under ultrasonic power 700W, microwave power 500W, the condition of 55 DEG C, obtains product after cooling.
Experimental example 3:
By the soybean oil of 31.9% and the mixing of 1% Yelkin TTS, heating, dissolve and make oil base; The fruit of Acanthopanax sessiliflorus anthocyanogen of 1.5% is added after getting the caster sugar of 25%, the water of 40% and 0.6% sodium alginate mixed dissolution, oil base is added after stirring, ultrasonic-microwave cooperating emulsification 25min under ultrasonic power 300W, microwave power 200W, the condition of 40 DEG C, obtains product after cooling.
The product of embodiment 1,2,3 is carried out performance measurement, the results are shown in following table, its performance index can meet the requirement of silk screen printing.Adopt silk screen printing to be printed on bread surface, all show good transitivity, tack and printing effect, clear picture, without wire drawing, dizzy dye phenomenon, the soft nature of color, can realize original copy preferably and reproduce.
The performance measurement of Sessileflower Acanthopanax Bark berry anthocyanin edible ink
| Product type | Viscosity/Pas | Degree of mobilization/mm | Fineness/um | L* | a* | b* |
| Embodiment 1 | 0.32 | 37 | ﹤15um | 44.62 | 24.44 | 15.43 |
| Embodiment 2 | 0.41 | 30 | ﹤15um | 50.65 | 46.35 | 35.38 |
| Embodiment 3 | 0.33 | 36 | ﹤15um | 47.96 | 32.21 | 23.08 |
Note: L* is product brightness; A* is that product is red/green; B* is that product is yellow/blue.
Describe above, just the specific embodiment of the present invention, various illustrating is not construed as limiting flesh and blood of the present invention.
Claims (7)
1. a Sessileflower Acanthopanax Bark berry anthocyanin edible ink, is characterized in that being made up of the raw material of following weight:
Sessileflower Acanthopanax Bark berry anthocyanin 0.5-5%, binder 92-99.3%, auxiliary agent 0.2-3%; Described binder is 15-60% edible oil, 20-40% caster sugar and 15-60% water.
2., according to Sessileflower Acanthopanax Bark berry anthocyanin edible ink according to claim 1, it is characterized in that described auxiliary agent is emulsifying agent 0.1-1.5% and thickening material 0.1-1.5%.
3., according to the Sessileflower Acanthopanax Bark berry anthocyanin edible ink described in claim 1 or 2, it is characterized in that described emulsifying agent is Yelkin TTS or soybean protein, described thickening material is xanthan gum or sodium alginate.
4., according to Sessileflower Acanthopanax Bark berry anthocyanin edible ink according to claim 3, it is characterized in that being made up of the raw material of following weight: the fruit of Acanthopanax sessiliflorus anthocyanogen of 1%, soybean oil 34.1%, Yelkin TTS 0.5%, caster sugar 30%, water 34.1% and xanthan gum 0.3%.
5. the preparation method of Sessileflower Acanthopanax Bark berry anthocyanin edible ink as claimed in claim 4, is characterized in that step is as follows: the edible oil binder of oiliness mixed with emulsifying agent, heat, dissolve and make oil base; Remaining caster sugar, water binder are mixed with thickening material, adds colorant Sessileflower Acanthopanax Bark berry anthocyanin after dissolving, after stirring, add oil base, after emulsification, cooling, obtain product.
6. according to the preparation method of Sessileflower Acanthopanax Bark berry anthocyanin edible ink according to claim 5, it is characterized in that described emulsification method is ultrasonic wave-microwave cooperating emulsification, ultrasonic power 100-900w, microwave power 100-600w, emulsifying temperature 30-60 DEG C, emulsification times 5-30min.
7., according to the preparation method of Sessileflower Acanthopanax Bark berry anthocyanin edible ink according to claim 6, it is characterized in that the soybean oil of 34.1% and the mixing of 0.5% Yelkin TTS, heating, dissolve and make oil base; The fruit of Acanthopanax sessiliflorus anthocyanogen of 1% is added after getting the caster sugar of 30%, the water of 34.1% and 0.3% xanthan gum mixed dissolution, oil base is added after stirring, ultrasonic-microwave cooperating emulsification 20min under ultrasonic power 200W, microwave power 300W, the condition of 50 DEG C, obtains product after cooling.
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| CN201510295041.2A CN104861768A (en) | 2015-06-03 | 2015-06-03 | Acanthopanax sessiliflorus seem berry anthocyanin edible ink and preparation method |
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| CN201510295041.2A CN104861768A (en) | 2015-06-03 | 2015-06-03 | Acanthopanax sessiliflorus seem berry anthocyanin edible ink and preparation method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106280705A (en) * | 2016-08-25 | 2017-01-04 | 浙江中域科技股份有限公司 | A kind of edible ink-jet printing-ink and preparation method thereof |
| CN106366766A (en) * | 2016-08-31 | 2017-02-01 | 张文涛 | Anti-counterfeiting waterborne ink for medicine packaging and preparation method of anti-counterfeiting waterborne ink |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102649888A (en) * | 2012-05-07 | 2012-08-29 | 刘方旭 | Edible printing ink and preparation method thereof |
| CN103408617A (en) * | 2013-08-22 | 2013-11-27 | 吉林大学 | Preparation method of acanthopanax sessiliflorus berry anthocyanin with antioxidant activity |
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2015
- 2015-06-03 CN CN201510295041.2A patent/CN104861768A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102649888A (en) * | 2012-05-07 | 2012-08-29 | 刘方旭 | Edible printing ink and preparation method thereof |
| CN103408617A (en) * | 2013-08-22 | 2013-11-27 | 吉林大学 | Preparation method of acanthopanax sessiliflorus berry anthocyanin with antioxidant activity |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106280705A (en) * | 2016-08-25 | 2017-01-04 | 浙江中域科技股份有限公司 | A kind of edible ink-jet printing-ink and preparation method thereof |
| CN106366766A (en) * | 2016-08-31 | 2017-02-01 | 张文涛 | Anti-counterfeiting waterborne ink for medicine packaging and preparation method of anti-counterfeiting waterborne ink |
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Application publication date: 20150826 |