CN104857907A - Chitosan reaction kettle - Google Patents
Chitosan reaction kettle Download PDFInfo
- Publication number
- CN104857907A CN104857907A CN201510189782.2A CN201510189782A CN104857907A CN 104857907 A CN104857907 A CN 104857907A CN 201510189782 A CN201510189782 A CN 201510189782A CN 104857907 A CN104857907 A CN 104857907A
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- CN
- China
- Prior art keywords
- reaction kettle
- kettle body
- agitating device
- chitosan
- stirrer paddle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The invention discloses a chitosan reaction kettle comprising a reaction kettle body, a stirring device arranged in the reaction kettle body, a feeding port arranged on the top of the reaction kettle body, and a discharge port arranged at the bottom of the reaction kettle body. A motor is arranged above the reaction kettle body, and drives the stirring device to rotate. The rotation direction and speed of the stirring device are controllable. The stirring device extends into the reaction kettle body. Stirring blades are arranged on the end and on the middle part of the stirring device. Stirring baffles rotationally connected with the stirring blades are arranged at the suspended ends of the stirring blades. A scraper sheet is connected to the upper end of the stirring device. The scraping sheet is vertically positioned close to the inner sidewall of the reaction kettle body, and rotates under the driving of the stirring device. The chitosan reaction kettle provided by the invention has the advantages of reasonable structural design and sufficient stirring. With the reaction kettle, product quality can be effectively improved.
Description
Technical field
The present invention relates to reaction vessel technical field, particularly a kind of chitosan reaction still.
Background technology
The reactor of existing production shitosan, agitating device only has stirrer paddle, easily causes stirring insufficient, causes deacetylation problem of non-uniform, cause product quality not high because chitin easily suspends.And the reactor sidewall of shitosan is easily stained with raw material, cause raw material to be bonded on inwall and cause waste.
Summary of the invention
The technical issues that need to address of the present invention are that the reactor of existing production shitosan stirs insufficient, cause product quality not high, and cause raw-material waste.
For solving the problems of the technologies described above, the invention provides a kind of chitosan reaction still, comprise reaction kettle body, be arranged on the agitating device in reaction kettle body, the charging aperture being arranged on reaction kettle body top and the discharging opening be arranged on bottom reaction kettle body, motor is provided with above described reaction kettle body, described driven by motor agitating device rotates, and described agitating device rotation direction and velocity of rotation controlled, described agitating device stretches in reaction kettle body, and be equipped with stirrer paddle in its end and centre position, end, described stirrer paddle unsettled one end is being provided with the mixing baffle be rotationally connected with described stirrer paddle, described mixing baffle centre position and described stirrer paddle are rotationally connected, and the angular range that described mixing baffle and described stirrer paddle rotate is 45 °-135 °, also scraping blade is connected with in the upper end of described agitating device, the madial wall of described reaction kettle body vertically pressed close to by described scraping blade, and driven by described agitating device and rotate.Chitosan reaction still of the present invention adopts paddle to stir, stirrer paddle arranges rotating mixing baffle, make to stir, improve product quality, the angular range that mixing baffle and stirrer paddle rotate is 45 °-135 °, change with rotation direction and the change of stirring resistance, reduce resistance, increase shear flow and the circulation ability of agitating device.Agitating device rotation direction and velocity of rotation controlled, both can rotate forward and also can rotate backward, and velocity of rotation is adjustable, add the flexibility of production, stirring can be made more abundant, and be also connected with scraping blade in the upper end of agitating device, the madial wall of described reaction kettle body vertically pressed close to by scraping blade, under the rotation of agitating device drives, the bonding raw material on reaction kettle body madial wall can be scraped, avoid waste.
As a further improvement on the present invention, be also evenly provided with 4 hanging feets in the centre position of the lateral wall of described reaction kettle body, described hanging feet is fixedly connected on reaction kettle body by hanging feet backing plate.The suspension that hanging feet is used for equipment is fixed, convenient and practical.
As the preferred technical solution of the present invention, be also provided with steam inlet, drain and hand-hole at described reaction kettle body top, the sidewall of described reaction kettle body be also provided with a steam inlet, bottom described reaction kettle body, be provided with steam (vapor) outlet; Described reaction kettle body comprises kettle barrel and reaction kettle cover, and described reaction kettle cover covers on kettle barrel, outside described kettle barrel, be also provided with jacket cylinder.
Chitosan reaction still of the present invention, reasonable in design, stirs fully, can effectively improve the quality of products.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
Fig. 2 is the top view of Fig. 1;
Fig. 3 is that the A-A of Fig. 1 is to sectional view;
Wherein, 1-reaction kettle body, 2-agitating device, 3-charging aperture, 4-discharging opening, 5-motor, 6-stirrer paddle, 7-mixing baffle, 8-scraping blade, 9-hanging feet, 10-hanging feet backing plate, 11-steam inlet, 12-drain, 13-hand-hole, 14-steam (vapor) outlet, 15-kettle barrel, 16-reacts kettle cover, 17-jacket cylinder.
Detailed description of the invention
The preferred technical solution of the present invention is described in detail below in conjunction with accompanying drawing.
As shown in the figure, chitosan reaction still of the present invention, comprise reaction kettle body 1, be arranged on the agitating device 2 in reaction kettle body 1, be arranged on the charging aperture 3 at reaction kettle body 1 top, steam inlet 11, drain 12, hand-hole 13 and the discharging opening 4 be arranged on bottom reaction kettle body 1, steam (vapor) outlet 11, the sidewall of described reaction kettle body 1 is also provided with a steam inlet 11, motor 5 is provided with above described reaction kettle body 1, described motor 5 drives agitating device 2 to rotate, and described agitating device 2 rotation direction and velocity of rotation controlled, described agitating device 2 stretches in reaction kettle body 1, and be equipped with stirrer paddle 6 in its end and centre position, end, described stirrer paddle 6 unsettled one end is being provided with the mixing baffle 7 be rotationally connected with described stirrer paddle 6, described mixing baffle 7 centre position and described stirrer paddle 6 are rotationally connected, and the angular range that described mixing baffle 7 and described stirrer paddle 6 rotate is 45 °-135 °, scraping blade 8 is also connected with in the upper end of described agitating device 2, the madial wall of described reaction kettle body 1 vertically pressed close to by described scraping blade 8, and drive rotation by described agitating device 2, also evenly be provided with 4 hanging feets 9 in the centre position of the lateral wall of described reaction kettle body 1, described hanging feet 9 is fixedly connected on reaction kettle body 1 by hanging feet backing plate 10, described reaction kettle body 1 comprises kettle barrel 15 and reaction kettle cover 16, and described reaction kettle cover 16 covers on kettle barrel 15, outside described kettle barrel 15, be also provided with jacket cylinder 17.
Chitosan reaction still of the present invention produces the design of highdensity shitosan mainly for chitin, chitin is as the non-water soluble substance of sheet, be immersed in chitosan reaction still in 30% dope alkali, then through 90 DEG C of thermophilic digestion deacetylations, belong to a kind of solid-liquid reaction type.
Chitosan reaction still of the present invention adopts paddle to stir, stirrer paddle arranges rotating mixing baffle, make to stir, improve product quality, the angular range that mixing baffle and stirrer paddle rotate is 45 °-135 °, change with rotation direction and the change of stirring resistance, reduce resistance, increase shear flow and the circulation ability of agitating device.Agitating device rotation direction and velocity of rotation controlled, both can rotate forward and also can rotate backward, and velocity of rotation is adjustable, add the flexibility of production, stirring can be made more abundant, and be also connected with scraping blade in the upper end of agitating device, the madial wall of described reaction kettle body vertically pressed close to by scraping blade, under the rotation of agitating device drives, the bonding raw material on reaction kettle body madial wall can be scraped, avoid waste.The suspension that hanging feet is used for equipment is fixed, convenient and practical.Chitosan reaction still of the present invention, reasonable in design, stirs fully, can effectively improve the quality of products.
Claims (4)
1. a chitosan reaction still, comprise reaction kettle body (1), be arranged on the agitating device (2) in reaction kettle body, be arranged on the charging aperture (3) at reaction kettle body (1) top and be arranged on the discharging opening (4) of reaction kettle body (1) bottom, it is characterized in that: described reaction kettle body (1) top is provided with motor (5), described motor (5) drives agitating device (2) to rotate, and described agitating device (2) rotation direction and velocity of rotation controlled, described agitating device (2) stretches in reaction kettle body (1), and be equipped with stirrer paddle (6) in its end and centre position, end, described stirrer paddle (6) unsettled one end is being provided with the mixing baffle (7) be rotationally connected with described stirrer paddle (6), described mixing baffle (7) centre position and described stirrer paddle (6) are rotationally connected, and the angular range that described mixing baffle (7) and described stirrer paddle (6) rotate is 45 °-135 °, scraping blade (8) is also connected with in the upper end of described agitating device (2), the madial wall of described reaction kettle body (1) vertically pressed close to by described scraping blade, and driven by described agitating device (2) and rotate.
2. chitosan reaction still as claimed in claim 1, it is characterized in that: be also evenly provided with 4 hanging feets (9) in the centre position of the lateral wall of described reaction kettle body (1), described hanging feet (9) is fixedly connected on reaction kettle body (1) by hanging feet backing plate (10).
3. chitosan reaction still as claimed in claim 1 or 2, it is characterized in that: be also provided with steam inlet (11), drain (12) and hand-hole (13) at described reaction kettle body (1) top, the sidewall of described reaction kettle body (1) is also provided with a steam inlet (11), described reaction kettle body (1) bottom is provided with steam (vapor) outlet (14).
4. chitosan reaction still as claimed in claim 3, it is characterized in that: described reaction kettle body (1) comprises kettle barrel (15) and reaction kettle cover (16), described reaction kettle cover (16) is covered on kettle barrel (15), is also provided with jacket cylinder (17) in described kettle barrel (15) outside.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510189782.2A CN104857907A (en) | 2015-04-21 | 2015-04-21 | Chitosan reaction kettle |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201510189782.2A CN104857907A (en) | 2015-04-21 | 2015-04-21 | Chitosan reaction kettle |
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CN104857907A true CN104857907A (en) | 2015-08-26 |
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CN201510189782.2A Pending CN104857907A (en) | 2015-04-21 | 2015-04-21 | Chitosan reaction kettle |
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Citations (11)
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US4366123A (en) * | 1981-09-21 | 1982-12-28 | Mitsui Petrochemical Industries Ltd. | Anchor agitator for gaseous phase polymerization vessel |
JPH06170202A (en) * | 1992-12-09 | 1994-06-21 | Dainippon Ink & Chem Inc | Agitating device |
CN102350289A (en) * | 2011-08-08 | 2012-02-15 | 金发科技股份有限公司 | Reaction kettle for producing static material not easy to flow and use method thereof |
CN203494407U (en) * | 2013-09-02 | 2014-03-26 | 海斯摩尔生物科技有限公司 | Dissolver for pure chitosan spinning solution |
CN103721661A (en) * | 2012-10-10 | 2014-04-16 | 江苏九寿堂生物制品有限公司 | Reaction kettle |
CN203816549U (en) * | 2014-05-20 | 2014-09-10 | 淮北旭日建材有限公司 | Liquid stirrer |
CN203955094U (en) * | 2014-05-20 | 2014-11-26 | 上海斯米克控股股份有限公司 | The energy-conservation agitating device of a kind of abnormity |
CN204051014U (en) * | 2014-07-10 | 2014-12-31 | 江苏华泰重工装备有限公司 | A kind of highly effective evaporimeter |
CN104338506A (en) * | 2013-08-02 | 2015-02-11 | 天津润沃供水安装工程有限公司 | Stirring-controllable reaction kettle |
CN104338448A (en) * | 2013-08-02 | 2015-02-11 | 天津润沃供水安装工程有限公司 | Stirring apparatus with subsidiary rotating shaft |
CN204159339U (en) * | 2014-11-12 | 2015-02-18 | 郑州大学 | A kind of resin batch mixing agitator |
-
2015
- 2015-04-21 CN CN201510189782.2A patent/CN104857907A/en active Pending
Patent Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4366123A (en) * | 1981-09-21 | 1982-12-28 | Mitsui Petrochemical Industries Ltd. | Anchor agitator for gaseous phase polymerization vessel |
JPH06170202A (en) * | 1992-12-09 | 1994-06-21 | Dainippon Ink & Chem Inc | Agitating device |
CN102350289A (en) * | 2011-08-08 | 2012-02-15 | 金发科技股份有限公司 | Reaction kettle for producing static material not easy to flow and use method thereof |
CN103721661A (en) * | 2012-10-10 | 2014-04-16 | 江苏九寿堂生物制品有限公司 | Reaction kettle |
CN104338506A (en) * | 2013-08-02 | 2015-02-11 | 天津润沃供水安装工程有限公司 | Stirring-controllable reaction kettle |
CN104338448A (en) * | 2013-08-02 | 2015-02-11 | 天津润沃供水安装工程有限公司 | Stirring apparatus with subsidiary rotating shaft |
CN203494407U (en) * | 2013-09-02 | 2014-03-26 | 海斯摩尔生物科技有限公司 | Dissolver for pure chitosan spinning solution |
CN203816549U (en) * | 2014-05-20 | 2014-09-10 | 淮北旭日建材有限公司 | Liquid stirrer |
CN203955094U (en) * | 2014-05-20 | 2014-11-26 | 上海斯米克控股股份有限公司 | The energy-conservation agitating device of a kind of abnormity |
CN204051014U (en) * | 2014-07-10 | 2014-12-31 | 江苏华泰重工装备有限公司 | A kind of highly effective evaporimeter |
CN204159339U (en) * | 2014-11-12 | 2015-02-18 | 郑州大学 | A kind of resin batch mixing agitator |
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Application publication date: 20150826 |