CN104856894A - Basil essential oil micro powder and preparation method therefor - Google Patents
Basil essential oil micro powder and preparation method therefor Download PDFInfo
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- CN104856894A CN104856894A CN201410074922.7A CN201410074922A CN104856894A CN 104856894 A CN104856894 A CN 104856894A CN 201410074922 A CN201410074922 A CN 201410074922A CN 104856894 A CN104856894 A CN 104856894A
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- essential oil
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Abstract
The invention discloses basil essential oil micro powder and a preparation method therefor. The micro powder is prepared from Arabic gum, maltodextrin, basil essential oil, methyl cellulose and/or carboxymethylcellulose sodium, sodium alginate, span 80 and/or sucrose fatty acid ester, aerosil and the like. Arabic gum, maltodextrin, methyl cellulose and/or carboxymethylcellulose sodium and sodium alginate are dissolved in water, the mixture is heated and the above ingredients are dissolved completely. Then the mixture is cooled and span 80 and/or sucrose fatty acid ester and basil essential oil are added, then the above mixture is stirred uniformly and allowed to stand for 2h, layering is not generated, or the mixed liquid is subjected to homogenization through a high-pressure homogenizer, and then basil essential oil micro powder particles are processed through spray drying. The preparation technology is simple and practical, the prepared micro powder delays and avoids oxidation of basil essential oil, and the retention time is prolonged. Because basil essential oil is solidified, the basil essential oil is convenient to use.
Description
Technical field
The present invention relates to cosmetics industry, daily necessities field, be specifically related to Basil Essential micropowder and preparation method thereof.
Technical background
Herba Ocimi (Herba Ocimi Pilosi) originates in West Asia and India, is just regarded as honorable " king of Rhizoma et radix valerianae " as far back as Greece's Roman period Herba Ocimi (Herba Ocimi Pilosi).Basil Essential is in international cosmetic raw material catalogue, and Basil Essential is widely used in champignon beauty culture by international market, commercially sells well very much, and the normal and quintessence oil such as bergamot, black pepper is arranged in pairs or groups, for the purposes such as massage and bathing.There is a large amount of effumability compositions in Basil Essential, a large amount of losses can be caused in preservation and use procedure, and also can be oxidized in long-term preservation process, be not easy to storage and use.So take some effective methods to preserve Basil Essential, the storage life extending Basil Essential is necessary.The store method of Basil Essential also mainly preserve or be processed into the forms such as micropowder by stored refrigerated, controlled atmosphere.The present invention relates to a kind of preparation method of Basil Essential micropowder, mainly by adopting some suitable materials, a kind of stable uniform liquid is mixed to form with Basil Essential, micro powder granule is made finally by methods such as spraying dry, like this by Basil Essential micropowder solid state, facilitate the use of Basil Essential like this, also can delay and avoid the oxidation of Basil Essential simultaneously, extend the storage life of Basil Essential.
Summary of the invention
The object of the invention is Basil Essential solidification to become wieldy form, meanwhile, also can make suitable the separating with air of Basil Essential, delay and avoid the oxidation of Basil Essential, can the holding time be extended.
Another object of the present invention is to provide the preparation technology of this Basil Essential micropowder.
Technical scheme of the present invention is: with arabic gum, maltodextrin and Basil Essential for main material, by adding the additives such as methylcellulose, sodium alginate, sorbester p17, sucrose fatty acid ester, micropowder silica gel, add water, stir, through the technical process such as high pressure homogenize, spraying dry, be processed into Basil Essential micropowder.
Object of the present invention can be realized by following measures:
A kind of Basil Essential micropowder, is made up of the formula of following weight percents:
Arabic gum 23 ~ 65% maltodextrin 26 ~ 69% methylcellulose 0.10 ~ 0.42% sodium alginate 0.15 ~ 2.11% Arlacel-80 and/or sucrose fatty acid ester 0.7 ~ 2.9% Basil Essential 9% ~ 33%, micropowder silica gel 1 ~ 5%.Another: the dosage of water accounts for 53 ~ 75% of gross weight
A preparation technology for Basil Essential micropowder, comprises the following steps:
A. arabic gum is got by formula and water puts into container, be heated to 60 ~ 85 DEG C, continuous stirring makes it to dissolve, and then adds maltodextrin, methylcellulose, sodium alginate successively, continues to stop heating after stirring makes it all dissolve, natural cooling, when temperature is down to 35 ~ 50 DEG C, add span Arlacel-80 and/or sucrose fatty acid ester, Basil Essential, continue to stir, make it even, leave standstill 2hr without layering.Also high pressure homogenizer (such as Canadian AVESTIN company, EmusiFlex-C50 type high pressure homogenizer) can be adopted to reach the effect homogenized completely.
B. the mixed liquor stirred is maintained 35 ~ 45 DEG C, then inlet temperature be 150 ~ 180 DEG C, leaving air temp carries out spraying dry under being 70 ~ 90 DEG C of conditions, be processed into micro powder granule, then add micropowder silica gel mix homogeneously.
Object of the present invention can also be realized by following measures:
The water used in described Basil Essential micropowder preparation technology is purified water.
Advantage of the present invention:
Preparation technology provided by the invention is simple, and prepared Basil Essential micropowder is a kind of powder, good fluidity, can delay and avoid the oxidation of Basil Essential, extends the holding time of Basil Essential.In addition, after Basil Essential is become solid micro-powder by volatile liquid state, be more convenient for using.
Detailed description of the invention
The invention will be further elaborated by the following examples.
Embodiment 1,
Arabic gum 320g, maltodextrin 156g methylcellulose 1.5g sodium alginate 2.9g Arlacel-80 5.0g Basil Essential 80g purified water 795g
Get arabic gum 320g and purified water 795g by formula and put into container, be heated to 75 DEG C, continuous stirring makes it to dissolve, and then add methylcellulose 1.5g, sodium alginate 2.9g, maltodextrin 156g successively, continue to stop heating, when naturally cooling to 35 DEG C after stirring makes it all dissolve, add Arlacel-80 5.0g and Basil Essential 80g, continue to stir, make it even, leave standstill 2hr without layering.The mixed liquor stirred is maintained 35 DEG C, then inlet temperature be 160 DEG C, leaving air temp carries out spraying dry under being 75 DEG C of conditions, be processed into micro powder granule, then add micropowder silica gel 11.3g, mix homogeneously.
Embodiment 2,
Arabic gum 283g, maltodextrin 189g methylcellulose 1.2g sodium alginate 3.3g Arlacel-80 3.0g sucrose fatty acid ester 4.0g Basil Essential 100g purified water 820g
Get arabic gum 283g and purified water 820g by formula and put into container, be heated to 70 DEG C, continuous stirring makes it to dissolve, and then add methylcellulose 1.2g, sodium alginate 3.3g, maltodextrin 189g successively, continue to stop heating, when naturally cooling to 40 DEG C after stirring makes it all dissolve, add Arlacel-80 3.0g, sucrose fatty acid ester 4.0g and Basil Essential 100g, continue to stir, make it even, leave standstill 2hr without layering.The mixed liquor stirred is maintained 40 DEG C, then inlet temperature be 155 DEG C, leaving air temp carries out spraying dry under being 75 DEG C of conditions, be processed into micro powder granule, then add micropowder silica gel 17g, mix homogeneously.
Embodiment 3,
Arabic gum 236g, maltodextrin 220g methylcellulose 1.7g sodium alginate 4.0g sucrose fatty acid ester 5.5g Basil Essential 90g purified water 800g
Get arabic gum 236g and purified water 800g by formula and put into container, be heated to 75 DEG C, continuous stirring makes it to dissolve, and then add methylcellulose 1.7g successively, sodium alginate 4.0g, maltodextrin 220g, continue to stop heating after stirring makes it all dissolve, when naturally cooling to 45 DEG C, add Arlacel-80 5.5g and Basil Essential 90g, continue to stir, make it even, then high pressure homogenize equipment (Canadian AVESTIN company is adopted, EmusiFlex-C50 type high pressure homogenizer) above-mentioned material is carried out at ambient temperature, first run once with 5000psi, again with 10000 ~ 25000psi process once.The mixed liquor natural cooling that homogenizing is crossed, then inlet temperature be 160 DEG C, leaving air temp carries out spraying dry under being 80 DEG C of conditions, be processed into micro powder granule, then add micropowder silica gel 13g, mix homogeneously.
Claims (3)
1. a Basil Essential micropowder, is characterized in that being made up of the formula of following weight percents:
Arabic gum 23 ~ 65% maltodextrin 26 ~ 69% methylcellulose 0.10 ~ 0.42% sodium alginate 0.15 ~ 2.11% Arlacel-80 and/or sucrose fatty acid ester 0.7 ~ 2.9% Basil Essential 9% ~ 33%, micropowder silica gel 1 ~ 5%.Another: the dosage of water accounts for 53 ~ 75% of gross weight
A preparation technology for Basil Essential micropowder, comprises the following steps:
A. arabic gum is got by formula and water puts into container, be heated to 60 ~ 85 DEG C, continuous stirring makes it to dissolve, and then adds maltodextrin, methylcellulose, sodium alginate successively, continues to stop heating after stirring makes it all dissolve, natural cooling, when temperature is down to 35 ~ 50 DEG C, add span Arlacel-80 and/or sucrose fatty acid ester, Basil Essential, continue to stir, make it even, leave standstill 2hr without layering.Also high pressure homogenizer (such as Canadian AVESTIN company, EmusiFlex-C50 type high pressure homogenizer) can be adopted to reach the effect homogenized completely.
B. the mixed liquor stirred is maintained 35 ~ 45 DEG C, then inlet temperature be 150 ~ 180 DEG C, leaving air temp carries out spraying dry under being 70 ~ 90 DEG C of conditions, be processed into micro powder granule, then add micropowder silica gel mix homogeneously.
2. the preparation technology of Fructus Alpiniae Oxyphyllae quintessence oil micropowder as claimed in claim 1, is characterized in that comprising the following steps:
A. arabic gum is got by formula and water puts into container, be heated to 60 ~ 85 DEG C, continuous stirring makes it to dissolve, and then adds maltodextrin, methylcellulose, sodium alginate successively, continues to stop heating after stirring makes it all dissolve, natural cooling, when temperature is down to 35 ~ 50 DEG C, add span Arlacel-80 and/or sucrose fatty acid ester, Basil Essential, continue to stir, make it even, leave standstill 2hr without layering.Also high pressure homogenizer (such as Canadian AVESTIN company, EmusiFlex-C50 type high pressure homogenizer) can be adopted to reach the effect homogenized completely.
B. the mixed liquor stirred is maintained 35 ~ 45 DEG C, then inlet temperature be 150 ~ 180 DEG C, leaving air temp carries out spraying dry under being 70 ~ 90 DEG C of conditions, be processed into micro powder granule, then add micropowder silica gel mix homogeneously.
3. Basil Essential micropowder according to claim 1, is characterized in that water used in preparation technology is purified water.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410074922.7A CN104856894A (en) | 2014-02-26 | 2014-02-26 | Basil essential oil micro powder and preparation method therefor |
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| CN201410074922.7A CN104856894A (en) | 2014-02-26 | 2014-02-26 | Basil essential oil micro powder and preparation method therefor |
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| CN104856894A true CN104856894A (en) | 2015-08-26 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110964324A (en) * | 2019-12-20 | 2020-04-07 | 佛山科学技术学院 | Antibacterial aromatic gutta-percha for infants |
| CN111040456A (en) * | 2019-12-18 | 2020-04-21 | 佛山科学技术学院 | Medical antibacterial silica gel material |
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| CN1680519A (en) * | 2004-04-05 | 2005-10-12 | 新疆芳香植物科技开发股份有限公司 | Microcapsules of essential oil from fragrant plants and preparation thereof |
| CN1805784A (en) * | 2003-05-11 | 2006-07-19 | 内盖夫研发局属本古里昂大学 | Encapsulated essential oils |
| CN101028074A (en) * | 2007-03-15 | 2007-09-05 | 李一雯 | Rose essential-oil microcapsule and its production |
| CN101519624A (en) * | 2009-01-20 | 2009-09-02 | 华南农业大学 | Cinnamon essential oil microcapsule and preparation method thereof |
| CN102715154A (en) * | 2012-05-08 | 2012-10-10 | 湖北大学 | Litsea cubeba oil mildew and moth proof slow release microcapsule and preparation method |
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2014
- 2014-02-26 CN CN201410074922.7A patent/CN104856894A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1805784A (en) * | 2003-05-11 | 2006-07-19 | 内盖夫研发局属本古里昂大学 | Encapsulated essential oils |
| CN1680519A (en) * | 2004-04-05 | 2005-10-12 | 新疆芳香植物科技开发股份有限公司 | Microcapsules of essential oil from fragrant plants and preparation thereof |
| CN101028074A (en) * | 2007-03-15 | 2007-09-05 | 李一雯 | Rose essential-oil microcapsule and its production |
| CN101519624A (en) * | 2009-01-20 | 2009-09-02 | 华南农业大学 | Cinnamon essential oil microcapsule and preparation method thereof |
| CN102715154A (en) * | 2012-05-08 | 2012-10-10 | 湖北大学 | Litsea cubeba oil mildew and moth proof slow release microcapsule and preparation method |
Non-Patent Citations (1)
| Title |
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| 吕百龄: "《实用工业助剂全书》", 31 August 2001 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111040456A (en) * | 2019-12-18 | 2020-04-21 | 佛山科学技术学院 | Medical antibacterial silica gel material |
| CN110964324A (en) * | 2019-12-20 | 2020-04-07 | 佛山科学技术学院 | Antibacterial aromatic gutta-percha for infants |
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