CN104817902B - A kind of heat-resisting fluorine carbon anticorrosive paint and preparation method thereof - Google Patents
A kind of heat-resisting fluorine carbon anticorrosive paint and preparation method thereof Download PDFInfo
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- CN104817902B CN104817902B CN201510260930.5A CN201510260930A CN104817902B CN 104817902 B CN104817902 B CN 104817902B CN 201510260930 A CN201510260930 A CN 201510260930A CN 104817902 B CN104817902 B CN 104817902B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D127/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers
- C09D127/02—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment
- C09D127/12—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Coating compositions based on derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention provides a kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component, and the weight portion composition of component A includes：50~60 parts of fluorocarbon resin, 0.3~0.5 part of dispersant, 10~20 parts of solvent, 15~25 parts of pigment, 1~2 part of levelling agent, 10~15 parts of anti-settling agent；The weight portion composition of B component includes：70~75 parts of curing agent, 25~30 parts of nano mica powder；The mass ratio of component A and B component is 5:1.The invention also discloses the preparation method of the heat-resisting fluorine carbon anticorrosive paint.The heat-resisting fluorine carbon anticorrosive paint that the present invention is provided has good heat resistance.
Description
Technical field：
The present invention relates to a kind of anticorrosive paint, more particularly to a kind of heat-resisting fluorine carbon anticorrosive paint and preparation method thereof.
Background technology：
Anticorrosive paint, is essential a kind of coating in paint, and etch-proof work can be played to metal material etc.
With, extend its service life, it is used as ship, container priming paint, vehicle paint base, steel structure, bridge, anticorrosive metal priming paint,
Oil pipe anti-corrosive coating etc..The defect that existing anticorrosive paint is present is not good heat resistance, in summer and various high temperature applicationss
Lower easily failure, limits its range of application.
The content of the invention：
The technical problem to be solved in the present invention is to provide a kind of heat-resisting fluorine carbon anticorrosive paint, with good heat resistance.
In order to solve the above technical problems, the technical scheme is that：
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
70~75 parts of curing agent,
25~30 parts of nano mica powder；
The mass ratio of component A and B component is 5:1.
Preferably, fluorocarbon resin of the present invention is FEVE fluorocarbon resins.
Preferably, dispersant of the present invention is one or both of acrylate copolymer, hydrophobic type polycarboxylate
Mixture.
Preferably, solvent of the present invention is dimethylbenzene, propylene glycol methyl ether acetate, diethylene glycol ether acetic acid esters, vinegar
The mixture of acid butyl ester.
Preferably, pigment of the present invention is titanium dioxide, blanc fixe, calcium carbonate, talcum powder, silica flour, trbasic zinc phosphate, three
One or more mixture in poly aluminium phosphate, calcium chromate, wollastonite, carbon black, aluminium powder.
Preferably, levelling agent of the present invention is dimethyl silicone polymer, polydimethyl phenyl siloxane or polyether-modified
Dimethyl silicone polymer.
Preferably, anti-settling agent of the present invention is aerosil, organobentonite, cellulose esters, thixotropy propylene
One or more in acid resin, polyamide wax.
Preferably, curing agent of the present invention is aliphatic polyisocyante.
Another technical problem to be solved by the present invention is that providing the preparation method of above-mentioned heat-resisting fluorine carbon anticorrosive paint.
In order to solve the above technical problems, technical scheme is：
A kind of preparation method of heat-resisting fluorine carbon anticorrosive paint, comprises the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
Compared with prior art, the invention has the advantages that：
Nano mica powder is lamellar structure, is the non-conductor of heat, external heat can be hindered to enter coating, so as to improve anti-
The heat resistance of rotten coating, in addition nano mica powder in itself have good heat endurance, can also effectively improve anticorrosive paint
Heat resistance；Dispersiveness of the nano mica powder in fluorocarbon resin be not good, therefore the present invention utilizes cetyl trimethyl bromination
Ammonium changes the hydrophily on its surface and is changed into lipophile to going to surface to be modified, and improves its dispersiveness, forms enough
Bridge, strengthen being coupled between nano mica powder and fluorocarbon resin, further improve coating heat resistance, while can have
Effect improves mechanical performance.
Specific embodiment
Describe the present invention in detail below in conjunction with specific embodiment, herein illustrative examples of the invention and explanation
It is for explaining the present invention but not as a limitation of the invention.
Embodiment 1
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
Curing agent 10g,
Nano mica powder 6g；
The mass ratio of component A and B component is 5:1.
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
Embodiment 2
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
Curing agent 15g,
Nano mica powder 5g；
The mass ratio of component A and B component is 5:1.
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
Embodiment 3
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
Curing agent 14.4g,
Nano mica powder 5.6g；
The mass ratio of component A and B component is 5:1.
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
Embodiment 4
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
Curing agent 14.8g,
Nano mica powder 5.2g；
The mass ratio of component A and B component is 5:1.
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
Embodiment 5
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
Curing agent 14.6g,
Nano mica powder 5.4g；
The mass ratio of component A and B component is 5:1.
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
Embodiment 6
A kind of heat-resisting fluorine carbon anticorrosive paint, is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
Curing agent 14.2g,
Nano mica powder 5.8g；
The mass ratio of component A and B component is 5:1.
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl front three
Base ammonium bromide is scattered in deionized water, is added after being uniformly dispersed in the ethanol solution of nano mica powder, continues ultrasonic disperse 1 small
When, filter cake is calcined 4 hours in filtering, washing at 400 DEG C, obtains modified Nano mica powder, and modified Nano mica powder is added
Curing agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained after 1 hour
Component A；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
The above-described embodiments merely illustrate the principles and effects of the present invention, not for the limitation present invention.It is any ripe
The personage for knowing this technology all can carry out modifications and changes under without prejudice to spirit and scope of the invention to above-described embodiment.Cause
This, those of ordinary skill in the art is complete with institute under technological thought without departing from disclosed spirit such as
Into all equivalent modifications or change, should be covered by claim of the invention.
Claims (8)
1. a kind of heat-resisting fluorine carbon anticorrosive paint, it is characterised in that：It is made up of component A and B component,
The weight portion composition of component A includes：
The weight portion composition of B component includes：
70~75 parts of curing agent,
25~30 parts of nano mica powder；
The mass ratio of component A and B component is 5:1；
Its preparation method is comprised the following steps：
(1) by nano mica powder, ultrasonic disperse is uniform in ethanol solution, with ultrasonic cleaner by cetyl trimethyl bromine
Change ammonium to be scattered in deionized water, added after being uniformly dispersed in the ethanol solution of nano mica powder, continue ultrasonic disperse 1 hour,
Filtering, washing, filter cake is calcined 4 hours at 400 DEG C, obtains modified Nano mica powder, modified Nano mica powder is added solid
Agent, is well mixed, and obtains B component；
(2) each component in component A is mixed, is disperseed 40 minutes with the rotating speed of 500rpm, grinding is obtained A groups after 1 hour
Part；
(3) by component A and B component according to 5:1 mass ratio is well mixed, and obtains heat-resisting fluorine carbon anticorrosive paint.
2. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The fluorocarbon resin is FEVE fluorine
Carbon resin.
3. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The dispersant is poly- for acrylic acid
The mixture of one or both of compound, hydrophobic type polycarboxylate.
4. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The solvent is dimethylbenzene, third
Glycol methyl ether acetate, diethylene glycol ether acetic acid esters, the mixture of butyl acetate.
5. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The pigment is titanium dioxide, weight
One kind in spar powder, calcium carbonate, talcum powder, silica flour, trbasic zinc phosphate, aluminium triphosphate, calcium chromate, wollastonite, carbon black, aluminium powder
Or two or more mixtures.
6. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The levelling agent is poly dimethyl
Siloxanes, polydimethyl phenyl siloxane or polyether-modified dimethyl silicone polymer.
7. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The anti-settling agent is gas phase dioxy
One or more in SiClx, organobentonite, cellulose esters, thixotropy acrylic resin, polyamide wax.
8. a kind of heat-resisting fluorine carbon anticorrosive paint according to claim 1, it is characterised in that：The curing agent is that aliphatic is more
Isocyanates.
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| CN201510260930.5A CN104817902B (en) | 2015-05-20 | 2015-05-20 | A kind of heat-resisting fluorine carbon anticorrosive paint and preparation method thereof |
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| CN105295584A (en) * | 2015-11-20 | 2016-02-03 | 天津美士邦涂料化工有限公司 | Heat-resistant anticorrosive coating |
| CN105880344B (en) * | 2016-05-13 | 2018-07-31 | 宿迁市通用机械有限公司 | A kind of processing of high-voltage mutual inductor shell is with pulling out a mouthful machine |
| CN107652792A (en) * | 2016-07-23 | 2018-02-02 | 天津市新丽华色材有限责任公司 | A kind of solar energy reflection mirror mirror-back protective coating |
| CN106318056B (en) * | 2016-09-11 | 2018-11-16 | 中海油常州涂料化工研究院有限公司 | A kind of radiation resistance, easy decontamination coating and preparation method thereof |
| CN107603358A (en) * | 2017-09-18 | 2018-01-19 | 浙江汉邦化工有限公司 | A kind of preparation method of the fluorine carbon anticorrosive paint of composite graphite alkene |
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| CN102965033A (en) * | 2012-11-02 | 2013-03-13 | 铜陵祥云消防科技有限责任公司 | Nano-mica powder modified compound adhesive for packaging |
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| CN103627218A (en) * | 2013-12-11 | 2014-03-12 | 浙江南益生物科技有限公司 | Preparation method of liquid nano mica modifier for PLA (poly lactic acid) |
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| CN101643620A (en) * | 2008-08-06 | 2010-02-10 | 中国科学院金属研究所 | Environmental-friendly polyaniline modified micaceous iron oxide anticorrosive coating and preparation method thereof |
| RU2010132698A (en) * | 2010-08-04 | 2012-02-10 | Открытое акционерное общество Научно-производственное объединение "Наука" (ОАО НПО "Наука") (RU) | METHOD FOR PRODUCING COMPOSITIONS FOR OBTAINING ANTIFRICTION COATINGS ON METAL SURFACES |
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Inventor after: Tian Haoliang Inventor after: Wang Changliang Inventor after: Guo Mengqiu Inventor after: Tang Zhihui Inventor after: Gao Junguo Inventor after: Cui Yongjing Inventor after: Zhang Huanhuan Inventor after: Zhou Zimin Inventor before: Ye Fang |
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Effective date of registration: 20170608 Address after: 100095 Haidian District hot springs town, Beijing Village Applicant after: China Hangfa Beijing Institute of Aerial Materials Address before: 510410 Guangdong, Baiyun District, Huangshi, East Road, Cheung garden, central garden, room B, building, room 702 Applicant before: Ye Fang |
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