CN104817260B - A kind of edge bonding method of vacuum glass and the production method of vacuum glass - Google Patents
A kind of edge bonding method of vacuum glass and the production method of vacuum glass Download PDFInfo
- Publication number
- CN104817260B CN104817260B CN201510181377.6A CN201510181377A CN104817260B CN 104817260 B CN104817260 B CN 104817260B CN 201510181377 A CN201510181377 A CN 201510181377A CN 104817260 B CN104817260 B CN 104817260B
- Authority
- CN
- China
- Prior art keywords
- glass
- sheet glass
- heating
- sealing
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
Landscapes
- Joining Of Glass To Other Materials (AREA)
Abstract
The invention discloses the production method of the edge bonding method and vacuum glass of a kind of vacuum glass, edge bonding method therein includes the following steps:I)The side of the pre- sealing-in of the vacuum glass is positioned over to the side of heating source, the side of the vacuum glass is heated, wherein, the heating source is hot wind;II)When heating side edges to the molten condition of the pre- sealing-in of the vacuum glass, sealing part implantation glass liquid between the upper sheet glass and lower sheet glass of the vacuum glass simultaneously smoothes out, and cools down, and completes edge sealing;Simple with manufacture craft, the period is short, and yield is high, and heat consumption is small, and occupied space is few, can carry out scale automatic assembly line operation, realizes the advantages that large scale vacuum glass produces.
Description
Technical field
The present invention relates to the field of deep of glass, specifically provide a kind of edge bonding method of vacuum glass and vacuum glass
The production method of glass.
Background technology
Vacuum glass is a kind of novel energy-conserving glass, it is based on vacuum flask principle, two sheet glass are sealed around, middle ware
The thin vacuum layer of 0.1 ~ 0.2mm is divided into, due to not having gas heat-transfer, inner surface has had the transparent low spoke that vacuum flask silverskin acts on again
Film is penetrated, the thermal and insulating performance of vacuum glass is made to be much better than " hollow " glass being widely used at present.
Above-mentioned advantage based on vacuum glass, vacuum glass have been widely used in building trade, and its demand
Day by day it is being incremented by, but complex for the processing technology of vacuum glass, especially edge sealing process at present, is needing vacuum glass
Entirety, which is put into heating furnace, carries out whole heating, and the space occupied is big, consumes a large amount of thermal energy, and fabrication cycle is long, influences
The yield of vacuum glass can not meet demand growing day by day.
Therefore, how the edge sealing and production method of existing vacuum glass are improved, to solve the above problems, become people
Urgent problem to be solved.
Invention content
In consideration of it, the purpose of the present invention is to provide a kind of edge bonding method of vacuum glass and the making sides of vacuum glass
Method, at least to solve in previous vacuum glass edge sealing and manufacturing process, existing space is big, and thermal energy consumption is big, production week
Phase is long, low production efficiency, the problems such as can not realizing the making of large scale vacuum glass.
One aspect of the present invention provides a kind of edge bonding method of vacuum glass, which is characterized in that includes the following steps:
I)The side of the pre- sealing-in of the vacuum glass is positioned over to the side of heating source, to the side of the vacuum glass into
Row heating, wherein, the heating source is hot wind;
II)When heating side edges to the molten condition of the pre- sealing-in of the vacuum glass, in upper piece glass of the vacuum glass
Sealing part implantation glass liquid between glass and lower sheet glass simultaneously smoothes out, and cools down, and completes edge sealing.
It is preferred that the step I)Middle heating source is segmented laser heating to the mode of heating of the vacuum glass side.
Further preferably, the segmented laser heating includes:Low-temperature prewarming, medium temperature heating and high-temperature heating three are continuous
Stage, wherein, the temperature of the low-temperature prewarming is 50 ~ 200 DEG C, the temperature of medium temperature heating is 200 ~ 600 DEG C, the high temperature
The temperature of heating is 600 ~ 1000 DEG C.
Further preferably, the step I)The position of middle heating source is fixed, and the relatively described heating source of the vacuum glass moves
It is dynamic.
Further preferably, the step II)The glass metal of middle injection heats, and the glass metal for cryogenic glass powder
Temperature less than/be equal to the pre- sealing-in of the vacuum glass side temperatures.
Another aspect of the present invention additionally provides a kind of production method of vacuum glass, which is characterized in that includes the following steps:
1)Upper sheet glass and lower sheet glass are cut, and clean up according to specification, it is spare;
2)Supporter dot matrix is laid in the side of lower sheet glass, and the surrounding of lower sheet glass is provided with glass binder;
3)The upper sheet glass is withheld in the top of the lower sheet glass, by the glass binder by it is described upper piece
The surrounding of glass and the lower sheet glass bonds, and forms one;
4)The side of the upper sheet glass and the pre- sealing-in of lower sheet glass is positioned over to the side of heating source, is added
Heat, wherein, the heating source is hot wind;
5)When heating side edges to the molten condition of the pre- sealing-in, the envelope on described between sheet glass and lower sheet glass
Mouthful place and smoothes out implantation glass liquid, cools down, completion edge sealing;
6)Medical needle, one end of the medical needle and institute are inserted at the edge sealing of sheet glass and lower sheet glass on described
It states the sealing space formed between sheet glass and lower sheet glass to communicate, the other end is connected with vacuum pump, to the sealing space
It is vacuumized;
7)After vacuumizing, the medical needle is blocked using electric arc welding device, solder joint is formed in the truncated position,
It is blocked at the solder joint using the glass of molten condition.
It is preferred that above support is sphere.
Further preferably, the step 2)It is opposite that the height of the relatively upper sheet glass of middle glass binder is more than above support
The height of upper sheet glass.
Further preferably, the step 4)Middle heating source is to the side of the upper sheet glass and the pre- sealing-in of lower sheet glass
Mode of heating is segmented laser heating.
Further preferably, the segmented laser heating includes:Low-temperature prewarming, medium temperature heating and high-temperature heating three are continuous
Stage, wherein, the temperature of the low-temperature prewarming is 50 ~ 200 DEG C, the temperature of medium temperature heating is 200 ~ 600 DEG C, the high temperature
The temperature of heating is 600 ~ 1000 DEG C.
The present invention is provided in the production method of edge bonding method and vacuum glass of vacuum glass, and glass is unexpected in order to prevent
Heat or irregular easy the problem of bursting of being heated, generate, and by using high hot wind as heating source, concentrate to vacuum glass
The side of pre- sealing-in carries out local heating, and to reduce occupied space and the consumption of heat for no reason during its heating, the present invention utilizes
The characteristic of high hot wind, by high hot wind, to vacuum glass, pre- sealing-in side is heated, and can make vacuum glass along pre- sealing-in side
Successively decrease in gradient to center position temperature, so as to fulfill not only local heating was carried out to vacuum glass, but also can prevent glass rupture from showing
The generation of elephant, complete edge sealing work, since method provided by the invention is that pre- sealing-in side is heated, no matter much sizes
Vacuum glass can make production.
The edge bonding method of vacuum glass provided by the invention and the production method of vacuum glass have manufacture craft letter
Single, the period is short, and yield is high, and heat consumption is small, and occupied space is few, can carry out scale automatic assembly line operation, realizes big
The advantages that size vacuum glass production.
Specific embodiment
The present invention is further expalined with specific embodiment below, but the guarantor being not intended to restrict the invention
Protect range.
In the past in vacuum glass making and the edge sealing course of work is carried out, in order to realize the sealing-in between upper and lower sheet glass,
It needs upper and lower sheet glass being placed into heating furnace and carries out whole heating, then the glass by being set on upper and lower sheet glass
After the melting of glass powder, by upper and lower sheet glass sealing-in, the space occupied is big in entire edge sealing work, and consumption of calorie is more, and operates tired
Difficulty, the period is long, low output, can not meet demand growing day by day on the market, and to solve the above-mentioned problems, the present embodiment carries
A kind of edge bonding method of vacuum glass is supplied, in this method, mainly by high hot wind to needing to carry out the vacuum glass side of edge sealing
Side carries out local emphasis heating, specific as follows to reduce the consumption of heat similar to the heating process and principle of Blowing drum:
I)The side of the pre- sealing-in of vacuum glass is positioned over to the side of high hot air source, opens high hot air source, be hot wind via
Pre- sealing-in side is blown away to vacuum glass direction, final to realize to realize that the side to vacuum glass carries out local emphasis heating
Vacuum glass is successively decreased in gradient from pre- sealing-in side to center position elongating temperature, to effectively prevent the phenomenon that glass is by thermal breakage
It generates;
II)When heating side edges to the molten condition of the pre- sealing-in of the vacuum glass, in upper piece glass of the vacuum glass
Sealing part implantation glass liquid between glass and lower sheet glass simultaneously smoothes out, and cools down, and edge sealing is completed, since glass is only in the shape of melting
Can just realize mutual bonding under state, and fastness is high, therefore, it is necessary to by the heating side edges of the pre- sealing-in of vacuum glass to molten
Melt state.
Wherein, the upper sheet glass and lower sheet glass can select simple glass or tempered glass.
If the direct higher hot wind of temperature in use heats the side of vacuum glass, glass rupture can also occur
Phenomenon,, can be by step I as the improvement of technical solution in order to improve yield rate)Middle heating source is to the vacuum glass side
Mode of heating selects segmented laser heating, is specifically divided into:Three low-temperature prewarming, medium temperature heating and high-temperature heating continuous ranks
Section, wherein, the temperature of the low-temperature prewarming is 50 ~ 200 DEG C, the temperature of medium temperature heating is 200 ~ 600 DEG C, the high temperature adds
The temperature of heat is 600 ~ 1000 DEG C.
It, can be by step I in order to realize large-scale production and the flow work)The position of middle heating source is fixed, by vacuum
Glass is moved relative to the heating source, realizes the heating for pre- sealing-in side, can be incited somebody to action in practical production process true
Empty glass is positioned on transmission belt, and the side of conveyer belt or top are provided with heating source, is realized by the transmission of conveyer belt true
Empty glass completes the local heating for vacuum glass relative to the movement of heating source.
In order to further reduce the probability of glass rupture, as the improvement of technical solution, the step II)The glass of middle injection
Glass liquid is heated for cryogenic glass powder, and the temperature of the glass metal is less than/is equal to the side of the pre- sealing-in of the vacuum glass
Temperature, so as to effectively avoid bursting for glass.
Introduce the detailed process that vacuum glass making is carried out using above-mentioned edge bonding method again below, it is specific as follows:
1)Upper sheet glass and lower sheet glass are cut, and clean up according to specification, it is spare;
2)Supporter dot matrix is laid in the side of lower sheet glass, and the surrounding of lower sheet glass is provided with glass binder,
The preferred high-temperature plastic of the binding agent;
3)The upper sheet glass is withheld in the top of the lower sheet glass, by the glass binder by it is described upper piece
The surrounding of glass and the lower sheet glass bonds, and forms one;
4)The side of the upper sheet glass and the pre- sealing-in of lower sheet glass is positioned over to the side of heating source, is added
Heat, wherein, the heating source is hot wind;
5)When heating side edges to the molten condition of the pre- sealing-in, the envelope on described between sheet glass and lower sheet glass
Mouthful place and smoothes out implantation glass liquid, cools down, completion edge sealing;
6)Medical needle, one end of the medical needle and institute are inserted at the edge sealing of sheet glass and lower sheet glass on described
It states the sealing space formed between sheet glass and lower sheet glass to communicate, the other end is connected with vacuum pump, to the sealing space
It is vacuumized;
7)After vacuumizing, the medical needle is blocked using electric arc welding device, and solder joint is formed in the truncated position,
It is blocked at the solder joint using the glass metal of molten condition, the electric arc welding device can select laser electric arc welding device.
Wherein, step 6)In for convenience medical needle insertion, can be in advance in upper sheet glass and the edge sealing of lower sheet glass
Place's drilling, the medical needle at the aperture by being inserted into.
The present embodiment provide to the method that vacuum glass vacuumizes extracted by medical needle, and be
It is inserted into, is blocked after vacuumizing by electric welding machine, then blocked by molten glass metal, in appearance at the sealing-in of upper and lower glass
The position of syringe needle is can't see, and since medical syringe needle is thinner, can avoided to causing the very big hole to cause to leak at sealing-in
The phenomenon that gas, occurs, and ensures the vacuum degree of vacuum glass well, and avoids previous vacuum glass on the glass of side
It stays there are one hole is vacuumized, by metal cap closure on hole, difficulty is brought to transport and construction.
Wherein, it is conducted heat due to vacuum glass centre and is made of radiant heat transfer and supporter heat transfer, in order to further drop
The hot/cold conduction of the low vacuum glass, it is preferable that above support is sphere, is that point connects with upper sheet glass and lower sheet glass
It touches, effectively reduces hot/cold conduction, more preferably, the sphere is micro- steel ball or glass microballoon.
In order to which upper sheet glass and can either can connect with bottom sheet glass bonding with supporter, as technical solution should, make
The step 2)The height of the relatively upper sheet glass of middle glass binder is more than the height of the relatively upper sheet glass of above support, due to
Glass binder has certain elasticity, and when upper sheet glass is withheld above lower sheet glass, the height of glass binder can drop
It is low, the very good quality that can be in contact with supporter, improve vacuum glass of sheet glass is gone up at this time.
It is consistent with edge bonding method, preferably described step 4)Middle heating source seals the upper sheet glass and the lower sheet glass in advance
The heating side edges mode connect is segmented laser heating, specially:Three low-temperature prewarming, medium temperature heating and high-temperature heating continuous ranks
Section, wherein, the temperature of the low-temperature prewarming is 50 ~ 200 DEG C, the temperature of medium temperature heating is 200 ~ 600 DEG C, the high temperature adds
The temperature of heat is 600 ~ 1000 DEG C.
Experimental test
By use the above method make vacuum glass, ordinary insulating glass available on the market, 10 layers of simple glass and
Single-glass carries out practical test, specific as follows:
4 bowls for being loaded with 50 DEG C of hot water are positioned on desk, respectively by above-mentioned vacuum glass, hollow glass, 10
Layer simple glass and individual layer simple glass are sequentially placed after being loaded on the bowl of 50 DEG C of hot water in 4 and carry out temperature survey for the first time,
By carrying out second test again after ten minutes, specific test data is shown in Table 1.
Table 1:Temperature data table
It understands to use vacuum glass made from method provided by the invention by table 1, it is preferable every the performance of hot/cold,
Better than hollow glass, 10 layers of simple glass and single-glass, meet the requirements.
Claims (2)
1. a kind of edge bonding method of vacuum glass, which is characterized in that include the following steps:
I) side of the pre- sealing-in of the vacuum glass is positioned over to the side of heating source, the side of the vacuum glass is added
Heat, wherein, the heating source is hot wind;
II) when heating side edges to the molten condition of the pre- sealing-in of the vacuum glass, the vacuum glass upper sheet glass and
Sealing part implantation glass liquid between lower sheet glass simultaneously smoothes out, and cools down, and completes edge sealing;
The step I) in heating source be segmented laser heating to the mode of heating of the vacuum glass side, and the segmentation
Formula laser heating includes:Three low-temperature prewarming, medium temperature heating and high-temperature heating successive stages, wherein, the temperature of the low-temperature prewarming
It is 200~600 DEG C to spend for the temperature of 50~200 DEG C, medium temperature heating, the temperature of the high-temperature heating is 600~1000 DEG C;
The step I) in the position of heating source fix, the vacuum glass is moved relative to the heating source;
The step II) in the glass metal that injects heat, and the temperature of the glass metal be less than/is equal to for cryogenic glass powder
The side temperatures of the pre- sealing-in of vacuum glass.
2. a kind of production method of vacuum glass, which is characterized in that include the following steps:
1) upper sheet glass and lower sheet glass are cut, and clean up according to specification, it is spare;
2) supporter dot matrix is laid in the side of lower sheet glass, and the surrounding of lower sheet glass is provided with glass binder;
3) the upper sheet glass is withheld in the top of the lower sheet glass, by the glass binder by the upper sheet glass
It is bonded with the surrounding of the lower sheet glass, forms one, the surrounding of sheet glass and the lower sheet glass is respectively formed on described
The side of pre- sealing-in;
4) side of the upper sheet glass and the pre- sealing-in of lower sheet glass is positioned over to the side of heating source, is heated,
In, the heating source is hot wind;
5) when heating side edges to the molten condition of the pre- sealing-in, the sealing part on described between sheet glass and lower sheet glass
Implantation glass liquid simultaneously smoothes out, and edge sealing is completed in cooling;
6) on described at the edge sealing of sheet glass and lower sheet glass be inserted into medical needle, one end of the medical needle with it is described on
The sealing space formed between sheet glass and lower sheet glass communicates, and the other end is connected with vacuum pump, and the sealing space is carried out
It vacuumizes;
7) after vacuumizing, the medical needle is blocked using electric arc welding device, and solder joint is formed in the truncated position, in institute
It states and is blocked at solder joint using the glass of molten condition;
Above support is sphere;
The height of the relatively upper sheet glass of glass binder is more than the height of the relatively upper sheet glass of above support in the step 2);
Heating source is segmentation to the heating side edges mode of the upper sheet glass and the pre- sealing-in of lower sheet glass in the step 4)
Formula laser heating, and the segmented laser heating includes:Three low-temperature prewarming, medium temperature heating and high-temperature heating successive stages,
Wherein, the temperature of the low-temperature prewarming is 50~200 DEG C, the temperature of medium temperature heating is 200~600 DEG C, the high temperature adds
The temperature of heat is 600~1000 DEG C.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510181377.6A CN104817260B (en) | 2015-04-16 | 2015-04-16 | A kind of edge bonding method of vacuum glass and the production method of vacuum glass |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510181377.6A CN104817260B (en) | 2015-04-16 | 2015-04-16 | A kind of edge bonding method of vacuum glass and the production method of vacuum glass |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104817260A CN104817260A (en) | 2015-08-05 |
CN104817260B true CN104817260B (en) | 2018-06-26 |
Family
ID=53727771
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510181377.6A Expired - Fee Related CN104817260B (en) | 2015-04-16 | 2015-04-16 | A kind of edge bonding method of vacuum glass and the production method of vacuum glass |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN104817260B (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105565683B (en) * | 2015-12-15 | 2018-12-07 | 洛阳兰迪玻璃机器股份有限公司 | A kind of production method and its production line of toughened vacuum glass |
CN105541132B (en) * | 2015-12-15 | 2019-01-04 | 洛阳兰迪玻璃机器股份有限公司 | A kind of production method and its production line of toughened vacuum glass |
CN109454356A (en) * | 2018-11-12 | 2019-03-12 | 合肥圣达电子科技实业有限公司 | A kind of method that high frequency assembly encapsulates transition piece and guarantee transition piece welding airtightness |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101314526A (en) * | 2007-05-28 | 2008-12-03 | 王广武 | Sealing apparatus and method for vacuum glass |
CN102020428A (en) * | 2009-09-16 | 2011-04-20 | 东元奈米应材股份有限公司 | Vacuum plane glass structure and manufacture method thereof |
CN102951787A (en) * | 2012-03-21 | 2013-03-06 | 戴长虹 | Vacuum glass edge sealing method by utilizing metal solders and product manufactured by method |
CN102951795A (en) * | 2012-03-21 | 2013-03-06 | 戴长虹 | Vacuum glass without extraction opening and support and preparation method thereof |
-
2015
- 2015-04-16 CN CN201510181377.6A patent/CN104817260B/en not_active Expired - Fee Related
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101314526A (en) * | 2007-05-28 | 2008-12-03 | 王广武 | Sealing apparatus and method for vacuum glass |
CN102020428A (en) * | 2009-09-16 | 2011-04-20 | 东元奈米应材股份有限公司 | Vacuum plane glass structure and manufacture method thereof |
CN102951787A (en) * | 2012-03-21 | 2013-03-06 | 戴长虹 | Vacuum glass edge sealing method by utilizing metal solders and product manufactured by method |
CN102951795A (en) * | 2012-03-21 | 2013-03-06 | 戴长虹 | Vacuum glass without extraction opening and support and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
CN104817260A (en) | 2015-08-05 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104817260B (en) | A kind of edge bonding method of vacuum glass and the production method of vacuum glass | |
CN106392241B (en) | A kind of light wave soldering oven | |
CN101148313B (en) | One-step forming vacuum glass and its manufacturing method and device | |
CN101492255A (en) | Method of quickly manufacturing vacuum glass | |
CN104183666B (en) | A kind of laser welding couples the method for crystal silicon solar energy battery | |
CN102951806A (en) | Convex vacuum glass welded by glass solders in microwave manner and subjected to edge sealing by strip frames, and manufacturing method of glass | |
CN105118790A (en) | Preparation method of high temperature resistant packaging framework of silicon carbide diode | |
CN105008295B (en) | The system and method for forming fused quartz glass | |
US11114581B2 (en) | Method for producing solar cell module | |
CN206666509U (en) | A kind of PCR reaction plates | |
WO2019210563A1 (en) | Tailless thermally insulated bottle liner and method for fabrication thereof | |
CN111302670A (en) | Electric hot-melt welding interlayer vacuum heat-preservation light-transmission toughened glass plate at periphery of toughened glass edge | |
CN1318342C (en) | Glass metal sealing process of vacuum heat-collecting pipe | |
CN101468872B (en) | Energy-saving thermos flask vacuum machine | |
CN102709455B (en) | Flip chip package structure of LED and its manufacture method | |
CN204539683U (en) | A kind of low-melting alloy silicon-base miniature cooler for smart mobile phone heat radiation | |
CN208869720U (en) | A kind of tubular polycrystalline silicon ingot casting graphite field | |
CN207405073U (en) | Laminated mold construction and glass shaping equipment | |
CN204216095U (en) | A kind of laser sintered equipment | |
CN206853735U (en) | A kind of support for auxiliary substrate solvent thermal growth | |
CN202362820U (en) | Combined multifunctional chip encapsulation head for SIM card | |
CN110219041A (en) | A kind of easy device drawing tubular material | |
CN103420580A (en) | Placement structure for getter of double-vacuum layer glass and manufacturing method of placement structure | |
CN102951794A (en) | Vacuum glass edge sealing method by utilizing low-temperature glass solders and product manufactured by method | |
CN201296727Y (en) | Vacuum glass with hemispherical support point |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20160601 Address after: 110000 3-1-1, 39-1 Taipei Road, Heping District, Liaoning, Shenyang Applicant after: Wu Zhi Address before: 110000 4-4-3, 12-5 East Lake street, Yuhong District, Liaoning, Shenyang Applicant before: Wang Xianzhang |
|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180626 |
|
CF01 | Termination of patent right due to non-payment of annual fee |