CN104800140B - A kind of Jing Mian treatment waxes and preparation method thereof - Google Patents
A kind of Jing Mian treatment waxes and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to daily nursing product technical field, discloses a kind of Jing Mian treatment waxes and preparation method thereof.Suo Shu treatment waxes are made up of the stearates of compound emulsifying agent PEG 20, cetostearyl alcohol and cetostearyl alcohol APEO 25, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, lanolin, hydroxyethyl cellulose, glycerine, methyl-silicone oil, phenyl silicone oil, elastomer silicone compound, polyquaternium, preservative, essence and water.The compound emulsifying agent of the present invention can stablize 25%~90% oil components, greatly improve the stability of product；By the different types of grease of high content, variety classes, the silicone oil of viscosity and specific conditioner carry out mixing compounding so that this invention treatment waxes have excellent glossiness effect.
Description
Technical field
The invention belongs to daily nursing product technical field, and in particular to a kind of Jing Mian treatment waxes and preparation method thereof.
Background technology
Treatment wax, layer protecting film can be formed in hair surface, to completely cut off the extraneous injury to hair, increase the light of hair
Pool, minimizing electrostatic friction, appropriate treatment waxes are smeared in hair surface, the sufficient nutrient of hair can be supplemented, it is necessary to hair
Nourishing, make hair submissive, such hair just can often preserve moisten and rich in gloss.However, due to various greases and silicone oil
Polarity is different, it is a large amount of improve constituent contents such as oil phases and making it keep it is stable turn into restrict bottleneck in Formula Development and
Technical barrier.Impaired, the Dry Hair crossed for dyeing and perm, it will be apparent that improving the glossiness of existing product more turns into a kind of urgent
Social demand.
The content of the invention
In order to solve the shortcomings that above prior art and weak point, primary and foremost purpose of the invention is to provide a kind of minute surface
Treatment wax.
Another object of the present invention is to provide the preparation method of above-mentioned Jing Mian treatment waxes.
The object of the invention is achieved through the following technical solutions：
A kind of Jing Mian treatment waxes, include following components in percentage by weight：
The compound emulsifying agent refers to PEG-20 stearates, cetostearyl alcohol and cetostearyl alcohol APEO -25
Compounding；It is preferred that the mass ratio between PEG-20 stearates, cetostearyl alcohol and cetostearyl alcohol APEO -25 is
1.2：1.2：1.
The parts by weight of said components are preferably：
Described methyl-silicone oil includes the low viscosity poly dimethyl that 2.5%~10.0% viscosity is 0.65~5000mPa.s
Siloxanes and 0.5%~5.0% viscosity are 8000~280 × 104MPa.s high viscosity dimethyl silicone polymer.
The preferred phenyl trimethicone of described phenyl silicone oil.
The described preferred Dimethicone Crosspolymer of elastomer silicone compound and methyl cyclosiloxane and
The compounding of ammonia end dimethyl silicone polymer；The Dimethicone Crosspolymer account for compound gross mass 10%~
30%.
The preferred methyl p-hydroxybenzoate of described preservative, propylparaben, double imidazolidinyl urea and iodine third
More than one or both of alkynylamino butyl formate, it is preferably added to the para hydroxybenzene that percentage composition is 0.05%~0.2%
Methyl formate, 0.05%~0.1% propylparaben and 0.1%~0.5% double imidazolidinyl urea and iodine propine
Aminocarbamic acid butyl ester.
The preparation method of above-mentioned Jing Mian treatment waxes, comprises the following steps：
(1) by compound emulsifying agent, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, lanolin, methyl-silicone oil, phenyl silicone oil,
Dosage according to percentage by weight, which is put into oil phase pot, to be warming up to 75~78 DEG C and is mixed evenly, and obtains oil phase；
(2) it will be well mixed in deionized water, hydroxyethyl cellulose input aqueous phase pot and be warming up to 55 DEG C~60 DEG C, at a high speed
Disperse to be allowed to dissolve to turn into transparency liquid, then glycerine is put into aqueous phase pot and is uniformly mixed and is warming up to 77 DEG C~82
DEG C, obtain aqueous phase；
(3) aqueous phase is pumped into vacuum emulsification pot, reserved part aqueous phase is stand-by in aqueous phase pot；
(4) homogeneous and the stirring in vacuum emulsification pot are opened, oil phase is pumped into emulsification pot, then will be pre- in step (3)
The aqueous phase stayed is pumped into emulsification pot, stops homogeneous；
(5) material of step (4) is cooled to 50 DEG C~55 DEG C under agitation, sequentially adds elastomer silicone compounding
Thing, polyquaternium, essence, preservative simultaneously stir, and obtain Jing Mian treatment waxes.
High speed described in step (2) disperses to refer to disperse 25~30min under conditions of 1200~1500r/min.
The product and preparation method of the present invention has the following advantages that and beneficial effect：
(1) compounding for the emulsifying agent that the present invention passes through different HLB values, solves oil components content between 25%~90%
Ruization Xing treatment waxes product keep the problem of stability for a long time, test result indicates that the Jing Mian treatment waxes of the present invention can be steady
Determine grease of the highest content up to 90% and continual and steady 2 years；
(2) due to inventive formulation, stability is high under conditions of high oiliness component content, therefore is formulated for difference
Species, the oil range of choice of polarity are more loose, are compounded by the mixing of variety classes, the grease of polarity or silicone oil, significantly
The Du Tigao luster performances for the treatment of wax product；
(3) inventive formulation passes through the different types of grease of high content, variety classes, the silicone oil of viscosity and specific conditioning
Agent carries out mixing compounding, and Suo get treatment waxes have the effect of minimizing electrostatic friction, fully supplement hair nutrient in application, especially
Impaired, the Dry Hair crossed for dyeing and perm, nourishes effect is more preferably prominent, makes hair more preferably submissive, retain youth with it is beautiful.
Brief description of the drawings
Fig. 1 is embodiment 1~3 and the stability test result pair of comparative example get Dao treatment waxes and commercially available Pu Tong treatment waxes
Than figure；
Fig. 2 is embodiment 1~3 and the glossiness test result pair of comparative example get Dao treatment waxes and commercially available Pu Tong treatment waxes
Than figure.
Embodiment
With reference to embodiment and accompanying drawing, the present invention is described in further detail, but embodiments of the present invention are unlimited
In this.
Embodiment 1
A kind of Jing Mian treatment waxes of the present embodiment, are prepared by the component of following parts by weight：
Compound emulsifying agent (mass ratio 1.2：1.2：1 PEG-20 stearates, cetostearyl alcohol and whale
Elastomer silicone compound (Dimethicone Crosspolymer and the poly- diformazan of methyl cyclosiloxane and ammonia end
The compounding of radical siloxane, Dimethicone Crosspolymer account for compound gross mass 20%)
The preparation method of the Jing Mian treatment waxes of the present embodiment is as follows：
(1) by compound emulsifying agent, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, low viscosity dimethyl silicone polymer, wool
Fat, phenyl trimethicone, propylparaben, put into oil phase pot and heat up according to the dosage of percentage by weight
It is mixed evenly to 75 DEG C, obtains oil phase；
(2) it will be well mixed in deionized water, hydroxyethyl cellulose input aqueous phase pot and be warming up to 55 DEG C, 1200r/min
Under conditions of disperse 25min be allowed to dissolving turn into transparency liquid, then successively by glycerine, methyl p-hydroxybenzoate input aqueous phase
It is uniformly mixed in pot and is warming up to 77 DEG C, obtains aqueous phase；
(3) aqueous phase is pumped into vacuum emulsification pot, reserved part aqueous phase is stand-by in aqueous phase pot；
(4) homogeneous and the stirring in vacuum emulsification pot are opened, oil phase is pumped into emulsification pot, then will be pre- in step (3)
The aqueous phase stayed is pumped into emulsification pot, stops homogeneous；
(5) material of step (4) is cooled to 50 DEG C under agitation, sequentially add high viscosity dimethyl silicone polymer,
Elastomer silicone compound, polyquaternium, essence, double imidazolidinyl urea, iodine propynylbutylcarbamate simultaneously stir,
Obtain Jing Mian treatment waxes.
Embodiment 2
A kind of Jing Mian treatment waxes of the present embodiment, are prepared by the component of following parts by weight：
Compound emulsifying agent (mass ratio 1.2：1.2：1 PEG-20 stearates and cetostearyl alcohol and whale
Elastomer silicone compound (Dimethicone Crosspolymer and the poly- diformazan of methyl cyclosiloxane and ammonia end
The compounding of radical siloxane, Dimethicone Crosspolymer account for compound gross mass 10%)
The preparation method of the Jing Mian treatment waxes of the present embodiment is as follows：
(1) by compound emulsifying agent, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, low viscosity dimethyl silicone polymer, wool
Fat, phenyl trimethicone, propylparaben, put into oil phase pot and heat up according to the dosage of percentage by weight
It is mixed evenly to 78 DEG C, obtains oil phase；
(2) it will be well mixed in deionized water, hydroxyethyl cellulose input aqueous phase pot and be warming up to 60 DEG C, 1500r/min
Under conditions of disperse 30min be allowed to dissolving turn into transparency liquid, then successively by glycerine, methyl p-hydroxybenzoate input aqueous phase
It is uniformly mixed in pot and is warming up to 80 DEG C, obtains aqueous phase；
(3) aqueous phase is pumped into vacuum emulsification pot, reserved part aqueous phase is stand-by in aqueous phase pot；
(4) homogeneous and the stirring in vacuum emulsification pot are opened, oil phase is pumped into emulsification pot, then will be pre- in step (3)
The aqueous phase stayed is pumped into emulsification pot, stops homogeneous；
(5) material of step (4) is cooled to 55 DEG C under agitation, sequentially add high viscosity dimethyl silicone polymer,
Elastomer silicone compound, polyquaternium, essence, double imidazolidinyl urea, iodine propynylbutylcarbamate simultaneously stir,
Obtain Jing Mian treatment waxes.
Embodiment 3
A kind of Jing Mian treatment waxes of the present embodiment, are prepared by the component of following parts by weight：
Compound emulsifying agent (mass ratio 1.2：1.2：1 PEG-20 stearates and cetostearyl alcohol and whale
Elastomer silicone compound (Dimethicone Crosspolymer and the poly- diformazan of methyl cyclosiloxane and ammonia end
The compounding of radical siloxane, Dimethicone Crosspolymer account for compound gross mass 30%)
The preparation method of the Jing Mian treatment waxes of the present embodiment is as follows：
(1) by compound emulsifying agent, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, low viscosity dimethyl silicone polymer, wool
Fat, phenyl trimethicone, propylparaben, put into oil phase pot and heat up according to the dosage of percentage by weight
It is mixed evenly to 76 DEG C, obtains oil phase；
(2) it will be well mixed in deionized water, hydroxyethyl cellulose input aqueous phase pot and be warming up to 60 DEG C, 1500r/min
Under conditions of disperse 30min be allowed to dissolving turn into transparency liquid, then successively by glycerine, methyl p-hydroxybenzoate input aqueous phase
It is uniformly mixed in pot and is warming up to 80 DEG C, obtains aqueous phase；
(3) aqueous phase is pumped into vacuum emulsification pot, reserved part aqueous phase is stand-by in aqueous phase pot；
(4) homogeneous and the stirring in vacuum emulsification pot are opened, oil phase is pumped into emulsification pot, then will be pre- in step (3)
The aqueous phase stayed is pumped into emulsification pot, stops homogeneous；
(5) material of step (4) is cooled to 52 DEG C under agitation, sequentially add high viscosity dimethyl silicone polymer,
Elastomer silicone compound, polyquaternium, essence, double imidazolidinyl urea, iodine propynylbutylcarbamate simultaneously stir,
Obtain Jing Mian treatment waxes.
Comparative example
The Yi Zhong treatment waxes of this comparative example, are prepared by the component of following parts by weight：
The preparation method of this comparative example treatment waxes is as follows：
(1) by cetearyl alcohol alcohol ether -6 and stearyl alcohol, cetearyl alcohol alcohol ether -25, jojoba oil, olive oil, 18
Alcohol, isopropyl palmitate, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, dimethyl silicone polymer, lanolin, the poly- front three of phenyl
Radical siloxane, propylparaben, put into according to the dosage of percentage by weight in oil phase pot be warming up to 75~78 DEG C it is mixed
Conjunction stirs, and obtains oil phase；
(2) it will be well mixed in deionized water, hydroxyethyl cellulose input aqueous phase pot and be warming up to 60 DEG C, 1500r/min
Under conditions of disperse 30min be allowed to dissolving turn into transparency liquid, then successively by glycerine, methyl p-hydroxybenzoate input aqueous phase
It is uniformly mixed in pot and is warming up to 80 DEG C, obtains aqueous phase；
(3) aqueous phase is pumped into vacuum emulsification pot, reserved part aqueous phase is stand-by in aqueous phase pot；
(4) homogeneous and the stirring in vacuum emulsification pot are opened, oil phase is pumped into emulsification pot, then will be pre- in step (3)
The aqueous phase stayed is pumped into emulsification pot, stops homogeneous；
(5) material of step (4) is cooled to 50 DEG C under agitation, sequentially adds essence, double imidazolidinyl urea and iodine
Propynylbutylcarbamate simultaneously stirs, get Dao treatment wax.
Embodiment 1~3, comparative example get Dao treatment waxes and commercially available Pu Tong treatment waxes stability and glossiness examine contrast：
(1) stability change (degradation) is tested
According to degradation formula, stabilization time=proving period × 4 of product[(heat resisting temperature -21.9)/10], wherein, 21.9 are
Constant, stabilization time that is, shelf life of products, test result is as shown in table 1 and Fig. 1.
The stability test result of table 1
From the point of view of the stabilization time of product, commercially available common oil content content is selected to carry out stability examination for 18% treatment waxes
Test, after 48 DEG C of heat resistant tests, appearance in the 21st day is coarse, and the stabilization time for illustrating the product is about 2 years；Select oil content (whale
Wax tristearin alcohol ether -6 and stearyl alcohol, cetearyl alcohol alcohol ether -25, jojoba oil, olive oil, 18 hexadecanols, isopropyl palmitate,
Straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, lanolin, dimethyl silicone polymer, phenyl trimethicone) content is
After 35% comparative example carries out the test of same type, the stabilization time of product is only 0.6 year, the stability distance of product 2 years
There is quite poor shelf-life away from illustrating that product belongs to unsure state.And the treatment waxes of the embodiment of the present invention 1~3 are in oil content
It is (PEG-20 stearates and cetostearyl alcohol and cetostearyl alcohol APEO -25, straight chained alkyl trimethyl ammonium chloride, white
Dormant oils, lanolin, methyl-silicone oil, phenyl silicone oil, elastomer silicone compound) content be 25%~90% content range in,
The proving period of product can be in 20 days stabilizations maintained above, and the quality guarantee period of calculating more than 2 years, illustrates the present invention's
Compound emulsifying agent (PEG-20 stearates and cetostearyl alcohol and cetostearyl alcohol APEO -25) and straight chained alkyl front three
Under the collective effect of ammonium chloride, there is good stabilization to the oil components of high content and multiple types.
(2) gloss rate of change is tested
Weighing 4g embodiments 1~3, comparative example get Dao treatment waxes and commercially available Pu Tong treatment waxes respectively, to be applied to 20g pre-
First pass through on the hair after processing is dried, hair is laid in the X-Rite love beautiful Judge II standards of color with certain thickness 4mm
Lamphouse light source bottom, a length of 30cm is selected, a width of 20cm fixed pan position, daylight mode is opened, passes through visual observations head
The luster performance of hair, which is given, to score, and the rule of scoring is as follows：
Standards of grading：1 point for it is poor, 2 points be it is poor, 3 points be typically, 4 points be it is good, 5 points be excellent.
Test number：10 people, results averaged
It is comprehensive to obtain hair gloss degrees of data, test result (fraction is averaged) as shown in table 2 below and Fig. 2.
The glossiness test result of table 2
| Glossiness (average value) | Oil content content % | |
| Embodiment 1 | 4.7 | 59.0 |
| Embodiment 2 | 4.3 | 25.0 |
| Embodiment 3 | 4.9 | 90.0 |
| Comparative example | 4.0 | 35.0 |
| Commercially available Pu Tong treatment waxes | 1.9 | 18.0 |
It can be seen that by the contrast of embodiment 1~3：With the increase of oil content dosage, its glossiness also improves therewith；But
When the test result that the oil content content of the present embodiment 2 is 25% than comparative example oil content content is 35%, the glossiness performance that shows
More superior, this explanation passes through the matched combined of different oil components in inventive formulation so that inventive formulation is compared to contrast
Example formula has more preferable glossiness performance；Compared to commercially available Pu Tong treatment waxes, the present invention is by increasing oil content content and different oil
The matched combined of property composition, product glossiness are obviously improved.
Above-described embodiment is the preferable embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment
Limitation, other any Spirit Essences without departing from the present invention with made under principle change, modification, replacement, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (8)
1. a kind of Jing Mian treatment waxes, it is characterised in that include following components in percentage by weight：
The compound emulsifying agent refers to answering for PEG-20 stearates, cetostearyl alcohol and cetostearyl alcohol APEO -25
Match somebody with somebody；Mass ratio between PEG-20 stearates, cetostearyl alcohol and cetostearyl alcohol APEO -25 is 1.2:1.2:1.
A kind of 2. Jing Mian treatment waxes according to claim 1, it is characterised in that：Include following components in percentage by weight：
A kind of 3. Jing Mian treatment waxes according to claim 1 or 2, it is characterised in that：Described methyl-silicone oil includes 2.5%
The low viscosity dimethyl silicone polymer and 0.5%~5.0% viscosity that~10.0% viscosity is 0.65~5000mPa.s be 8000~
280×104MPa.s high viscosity dimethyl silicone polymer.
A kind of 4. Jing Mian treatment waxes according to claim 1 or 2, it is characterised in that：Described phenyl silicone oil refers to phenyl
Poly- trimethicone.
A kind of 5. Jing Mian treatment waxes according to claim 1 or 2, it is characterised in that：Described elastomer silicone compounding
Thing refers to Dimethicone Crosspolymer and methyl cyclosiloxane and the compounding of ammonia end dimethyl silicone polymer；It is described poly-
Dimethicone crosspolymers account for the 10%~30% of compound gross mass.
A kind of 6. Jing Mian treatment waxes according to claim 1 or 2, it is characterised in that：Described preservative includes 0.05%
~0.2% methyl p-hydroxybenzoate, 0.05%~0.1% propylparaben and 0.1%~0.5% double miaows
Oxazolidinyl urea and iodine propynylbutylcarbamate.
A kind of 7. preparation method of Jing Mian treatment waxes described in any one of claim 1~6, it is characterised in that：Including following behaviour
Make step：
(1) by compound emulsifying agent, straight chained alkyl trimethyl ammonium chloride, White Mineral Oil, lanolin, methyl-silicone oil, phenyl silicone oil, according to
The dosage of percentage by weight, which is put into oil phase pot, to be warming up to 75~78 DEG C and is mixed evenly, and obtains oil phase；
(2) it will be well mixed in deionized water, hydroxyethyl cellulose input aqueous phase pot and be warming up to 55 DEG C~60 DEG C, it is scattered at a high speed
Being allowed to dissolving turns into transparency liquid, then puts into aqueous phase pot glycerine and is uniformly mixed and is warming up to 77 DEG C~82 DEG C, obtains
To aqueous phase；
(3) aqueous phase is pumped into vacuum emulsification pot, reserved part aqueous phase is stand-by in aqueous phase pot；
(4) open vacuum emulsification pot in homogeneous and stirring, by oil phase be pumped into emulsification pot in, then by step (3) reserve
Aqueous phase is pumped into emulsification pot, stops homogeneous；
(5) material of step (4) is cooled to 50 DEG C~55 DEG C under agitation, sequentially add elastomer silicone compound,
Polyquaternium, essence, preservative simultaneously stir, and obtain Jing Mian treatment waxes.
A kind of 8. preparation method of Jing Mian treatment waxes according to claim 7, it is characterised in that：Described in step (2)
It is scattered at a high speed to refer to disperse 25~30min under conditions of 1200~1500r/min.
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| CN110448500B (en) * | 2019-08-01 | 2022-07-22 | 广东嘉丹婷日用品有限公司 | Hair treatment essence |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| EP1792640A1 (en) * | 2005-12-02 | 2007-06-06 | Wella Aktiengesellschaft | Hair styling cream |
| CN103462858A (en) * | 2013-09-26 | 2013-12-25 | 北京美丽铺化妆品有限公司 | Oat paste having effects of cleaning and skin care, mask and their preparation methods |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| EP1792640A1 (en) * | 2005-12-02 | 2007-06-06 | Wella Aktiengesellschaft | Hair styling cream |
| CN103462858A (en) * | 2013-09-26 | 2013-12-25 | 北京美丽铺化妆品有限公司 | Oat paste having effects of cleaning and skin care, mask and their preparation methods |
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