CN104759114A - Water vapor generation and acid absorption device for nicotine extraction - Google Patents
Water vapor generation and acid absorption device for nicotine extraction Download PDFInfo
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- CN104759114A CN104759114A CN201510168087.8A CN201510168087A CN104759114A CN 104759114 A CN104759114 A CN 104759114A CN 201510168087 A CN201510168087 A CN 201510168087A CN 104759114 A CN104759114 A CN 104759114A
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- steam
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- sour
- water vapor
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Abstract
The invention discloses a water vapor generation and acid absorption device for nicotine extraction. The device is provided with a jacket type enamel kettle, wherein a central hole and two side holes are formed in an upper end cover of the jacket type enamel kettle; a liquid drainage pipe is connected at the bottom of the jacket type enamel kettle; the central hole is connected with a pillar enamel tube and a porous baffle is arranged at the connecting part; a temperature control probe sleeve pipe and a nicotine-containing water vapor induction pipe are connected at the two side holes of the jacket type enamel kettle respectively; the pillar enamel tube is filled with porcelain packing; an acid absorption liquid feeding pipe and a water vapor delivery pipe are arranged on the tube cover of the jacket type enamel kettle; one end of the acid absorption liquid feeding pipe is connected with a high level tank containing acid absorption raw liquid and the other end of the acid absorption liquid feeding pipe extends into the pillar enamel tube and is inserted into the inside of the porcelain packing; the water vapor delivery pipe is connected with a water vapor distillation tank. The device is capable of generating water vapor and has the functions of acid absorption and concentration; the resource is saved and the degeneration of solanesol in the residue after extraction can be avoided.
Description
Technical field
the invention belongs to alkaloid extraction equipment technical field, be specifically related to a kind of steam for nicotine extraction and occur and sour absorption plant.
Background technology
Containing very valuable nicotine and Salanesol in Discarded Tobacco, extraction nicotine and Salanesol, have organic solvent extraction-reverse-extraction method, CO 2 supercritical extraction method and carbonization decarboxylation (destructive distillation) method.Organic solvent extraction-reverse-extraction method, not only will consume a large amount of organic solvents, and contaminated environment; Not only equipment needed thereby is expensive but also to mention cost too high for CO 2 supercritical extraction method; Carbonization decarboxylation (destructive distillation) method, because temperature is higher, has part Salanesol to be transformed to enantiomer, causes its biologically active to reduce.Under alkali condition, with steam distillation effective component extracting nicotine from tobacco waste, can effectively other compositions in nicotine and tobacco be separated, and in residue, the biologically active of Salanesol also can remain unchanged.But traditional steam distillation, on the one hand, needs steam evaporator and acid to absorb two devices; On the other hand, a large amount of steam condenses into water in sour absorption plant, not only wastes mass energy, and has rushed sour absorbent solution rare, and cause its aftertreatment technology also must arrange concentrator, economic benefit is not good.Just because of this reason, traditional extraction by steam distillation nicotine is general only for the lab analysis of tobacco sample nicotine content.
Summary of the invention
The object of this invention is to provide a kind of steam extracted for nicotine to occur and sour absorption plant, this device can produce steam and with acid absorption and concentrating function, economize on resources, and can avoid the Salanesol sex change of extracting in rear residue.
The technical solution adopted in the present invention is: a kind of steam for nicotine extraction occurs and sour absorption plant, be provided with the jacket type enamel still that an inside is loaded with sour absorbing liquid, the top of described jacket type enamel still is sealed by upper end cover, upper end cover is provided with centre bore and two side openings, the bottom connected drainage pipe of jacket type enamel still, discharging tube is provided with glass valve, and the centre bore of upper end cover is connected with cylindricality enamel cylinder, and junction is provided with porous barrier; Two side opening places of upper end cover are connected to temperature control probe sleeve and containing nicotine steam ingress pipe, insert in sour absorbing liquid containing nicotine steam ingress pipe through side opening;
Porcelain filler is filled with in described cylindricality enamel cylinder, the top of cylindricality enamel cylinder is sealed by cover, cover is provided with sour absorbing liquid charge pipe and steam delivery line, acid absorbing liquid charge pipe one end connects is equipped with the head tank that acid absorbs stoste, the other end stretches in the porcelain filler of cylindricality enamel cylinder, and described steam delivery line is connected with steam distillation tank.
Further optimization, the outer surface of described jacket type enamel still and cylindricality enamel cylinder is equipped with heat-insulation layer.
Further optimization, on described steam delivery line, along stream of water vapor to being provided with pressure vacuum meter, temp probe, stream of water vapor control valve, bleed blower fan and sample cock successively.
Further optimization, the sidewall of described jacket type enamel still is also respectively equipped with illumination port and viewport.
Further optimization, described is provided with containing nicotine stream of water vapor control valve containing nicotine steam ingress pipe.
Further optimization, described sour absorbing liquid charge pipe is provided with sour absorbing liquid flow control valve.
Further optimization, between described discharging tube with jacket type enamel still and the port that is connected with head tank and sour absorbing liquid charge pipe of sour absorbing liquid flow control valve is equipped with sealing device.
Beneficial effect of the present invention
Compared with prior art, the present invention at least has following advantage and beneficial effect:
1, the present invention collect acid absorb and steam betide one, also eliminate the nicotine sulphate concentrator of subsequent technique, saved the energy significantly, be also conducive to environmental protection, steam distillation can be realized and extract alkaloidal technology commercialization.
2, the present invention can realize extraction nicotine and carries out at a lower temperature, avoid nicotine extract after the sex change of high added value composition Salanesol in residue.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
Reference numeral: 1, acid absorbing liquid, 2, jacket type enamel still, 3, upper end cover, 4, discharging tube, 5, glass valve, 6, cylindricality enamel cylinder, 7, porous barrier, 8, temperature control probe sleeve, 9, containing nicotine steam ingress pipe, 10, porcelain filler, 11, acid absorbing liquid charge pipe, 12, steam delivery line, 13, head tank, 14, pressure vacuum meter, 15, temp probe, 16, stream of water vapor control valve, 17, to bleed blower fan, 18, sample cock, 19, sealing device, 20, acid absorbs stoste, 21, containing nicotine stream of water vapor control valve, 22, acid absorbing liquid flow control valve, 23, heat-insulation layer.
Detailed description of the invention
For making content of the present invention become apparent, below in conjunction with specific embodiment, describe the present invention.
As shown in the figure, a kind of steam for nicotine extraction occurs and sour absorption plant, be provided with the jacket type enamel still 2 that an inside is loaded with sour absorbing liquid 1, the top of described jacket type enamel still 2 is sealed by upper end cover 3, upper end cover 3 is provided with centre bore and two side openings, the bottom connected drainage pipe 4 of jacket type enamel still 2, and discharging tube 4 is provided with glass valve 5, the centre bore of upper end cover 3 is connected with cylindricality enamel cylinder 6, and junction is provided with porous barrier 7; Two side opening places of upper end cover 3 are connected to temperature control probe sleeve 8 and containing nicotine steam ingress pipe 9, insert in sour absorbing liquid 1 containing nicotine steam ingress pipe 9 through side opening;
Porcelain filler 10 is filled with in described cylindricality enamel cylinder 6, the top of cylindricality enamel cylinder 6 is sealed by cover, cover is provided with sour absorbing liquid charge pipe 11 and steam delivery line 12, acid absorbing liquid charge pipe 11 one end connects is equipped with the head tank 13 that acid absorbs stoste 20, the other end stretches in the porcelain filler 10 of cylindricality enamel cylinder 6, described steam delivery line 12 one end is connected with the preformed hole being positioned at cylindricality enamel cylinder upper flanges lid, and steam delivery line 12 other end is connected with steam distillation tank.
In order to make the present invention, there is better result of use, the outer surface of described jacket type enamel still 2 and cylindricality enamel cylinder 6 is equipped with heat-insulation layer 23, the sidewall of jacket type enamel still 2 is also respectively equipped with illumination port and viewport, and illumination port and viewport are oppositely arranged the both sides of jacket type enamel still 2.Described discharging tube 4 is equipped with sealing device 19 with between jacket type the enamel still 2 and port that is connected with head tank 13 and sour absorbing liquid charge pipe 11 of sour absorbing liquid flow control valve 22.
In technical scheme of the present invention, on described steam delivery line 12, along stream of water vapor to being provided with pressure vacuum meter 14, temp probe 15, stream of water vapor control valve 16 successively, bleed blower fan 17 and sample cock 18, the described nicotine steam ingress pipe 9 that contains is provided with containing nicotine stream of water vapor control valve 21, and sour absorbing liquid charge pipe 11 is provided with sour absorbing liquid flow control valve 22.
Using method of the present invention:
The acid of step one, preparation debita spissitudo absorbs stoste 20, joins in head tank 13.
Step 2, open water vapor flow rate control valve 16 and sample cock 18, close glass valve 5 and containing on nicotine steam ingress pipe 9 containing nicotine stream of water vapor control valve 21, the illuminating lamp of opening clamp shell type enamel still 2, open the sour absorbing liquid flow control valve 22 on sour absorbing liquid charge pipe 11, the acid solution of about 1/3rd is put in jacket type enamel still 2, closes sour absorbing liquid flow control valve 22.
Step 3, the control temperature arranging the heating jacket of jacket type enamel still 2 are 110 DEG C, start heating, about 105 DEG C are boiled when the temperature in the kettle of jacket type enamel still 2 reaches micro-, namely sample cock 18 is emerged steam, unlatching is bled blower fan 17 and containing nicotine stream of water vapor control valve 21, close sample cock 18, regulate sour absorbing liquid flow control valve 22 to drip acid with the speed of 1 about per second and absorb stoste 20.
Step 4, detect steam by steam sample cock 18, if pH >=8 of steam and the pH < 3 of sour absorbing liquid 1, then should strengthen the rate of addition of sour absorbing liquid or turn down containing nicotine stream of water vapor control valve 21.
Step 5, absorb the increase of nicotine amount along with sour absorbing liquid 1, it absorbs the decline of the speed of nicotine, vapour pressure reduces, therefore the rate of addition that acid absorbs stoste 20 should be strengthened, and note observing pressure vacuum meter 14, heighten the control temperature of heating jacket or turn stream of water vapor control valve 16 down, maintaining system pressure at 1 atm higher;
Step 6, when sour absorbing liquid 20 quantity not sufficient in head tank, release appropriate amount of acid acid absorbing liquid 1 in jacket type enamel still 2 by glass valve 5 in time and transfer in head tank 13;
Step 7, sampled the pH value detecting sour absorbing liquid 1 in jacket type enamel still 2 by glass valve 5, discharge when the acid of head tank 13 absorbs stoste 20, and the pH=5 of sour absorbing liquid 1 in jacket type enamel still 2, namely obtain the sour absorbing liquid that nicotine is saturated;
Step 8, closedown, containing nicotine stream of water vapor control valve, are opened glass valve 5 and are released the saturated acid solution of nicotine, close it.
A set of steam distillation involved in the present invention, sour absorption equipment, although set forth for extraction nicotine, its application is not limited only to extraction nicotine, and for other alkaloid of resistance to 110 DEG C, suitable adjusting process parameter can use equally.
Technical scheme cited by the present invention and embodiment be not restriction, be equal to the technical scheme cited by the present invention and embodiment or effect same approach all in the scope that the present invention protects.
Claims (7)
1. one kind occurs and sour absorption plant for the steam of nicotine extraction, it is characterized in that: be provided with the jacket type enamel still (2) that an inside is loaded with sour absorbing liquid (1), the top of described jacket type enamel still (2) is by upper end cover (3) sealing, upper end cover (3) is provided with centre bore and two side openings, bottom connected drainage pipe (4) of jacket type enamel still (2), discharging tube (4) is provided with glass valve (5), the centre bore of upper end cover (3) is connected with cylindricality enamel cylinder (6), and junction is provided with porous barrier (7); Two side opening places of upper end cover (3) are connected to temperature control probe sleeve (8) and containing nicotine steam ingress pipe (9), insert in sour absorbing liquid (1) containing nicotine steam ingress pipe (9) through side opening;
Porcelain filler (10) is filled with in described cylindricality enamel cylinder (6), the top of cylindricality enamel cylinder (6) is sealed by cover, cover is provided with sour absorbing liquid charge pipe (11) and steam delivery line (12), acid absorbing liquid charge pipe (11) one end connects is equipped with the head tank (13) that acid absorbs stoste (20), the other end stretches in the porcelain filler (10) of cylindricality enamel cylinder (6), and described steam delivery line (12) is connected with steam distillation tank.
2. a kind of steam for nicotine extraction occurs and sour absorption plant as claimed in claim 1, it is characterized in that: described jacket type enamel still (2) and the outside of cylindricality enamel cylinder (6) are equipped with heat-insulation layer (23).
3. a kind of steam for nicotine extraction occurs and sour absorption plant as claimed in claim 1, it is characterized in that: on described steam delivery line (12), along stream of water vapor to being provided with pressure vacuum meter (14), temp probe (15), stream of water vapor control valve (16), blower fan of bleeding (17) and sample cock (18) successively.
4. a kind of steam for nicotine extraction occurs and sour absorption plant as claimed in claim 1, it is characterized in that: the sidewall of described jacket type enamel still (2) is also respectively equipped with illumination port and viewport.
5. a kind of steam for nicotine extraction occurs and sour absorption plant as claimed in claim 1, it is characterized in that: described is provided with containing nicotine stream of water vapor control valve (21) containing nicotine steam ingress pipe (9).
6. a kind of steam for nicotine extraction occurs and sour absorption plant as claimed in claim 1, it is characterized in that: described sour absorbing liquid charge pipe (11) is provided with sour absorbing liquid flow control valve (22).
7. a kind of steam extracted for nicotine occurs and sour absorption plant as claimed in claim 1, it is characterized in that: described discharging tube (4) is equipped with sealing device (19) with between jacket type enamel still (2) and the port that is connected with head tank (13) and sour absorbing liquid charge pipe (11) of sour absorbing liquid flow control valve (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510168087.8A CN104759114B (en) | 2015-04-10 | 2015-04-10 | A kind of steam for nicotine extraction occurs and sour absorption plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510168087.8A CN104759114B (en) | 2015-04-10 | 2015-04-10 | A kind of steam for nicotine extraction occurs and sour absorption plant |
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| Publication Number | Publication Date |
|---|---|
| CN104759114A true CN104759114A (en) | 2015-07-08 |
| CN104759114B CN104759114B (en) | 2015-12-30 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510168087.8A Expired - Fee Related CN104759114B (en) | 2015-04-10 | 2015-04-10 | A kind of steam for nicotine extraction occurs and sour absorption plant |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108627630A (en) * | 2018-04-03 | 2018-10-09 | 天津出入境检验检疫局化矿金属材料检测中心 | The device and detection method of halogens in mineral products are detected for steam distillation |
| CN115121120A (en) * | 2022-06-29 | 2022-09-30 | 湖北中烟工业有限责任公司 | Device and method for extracting concentrated nicotine |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1146454A (en) * | 1995-09-29 | 1997-04-02 | 吉林市万发实业有限公司 | Technology for extracting nicotine from tobacco leaf |
| US20050263166A1 (en) * | 2004-05-27 | 2005-12-01 | Oh Soo H | Process for manufacturing low nicotine tabacco leaf substitute |
| CN102516226A (en) * | 2011-11-30 | 2012-06-27 | 薛刚 | Method for distilling and refining nicotine circularly and nicotine distilling and absorbing device |
| CN204522371U (en) * | 2015-04-10 | 2015-08-05 | 南阳师范学院 | A kind of steam for nicotine extraction occurs and sour absorption plant |
-
2015
- 2015-04-10 CN CN201510168087.8A patent/CN104759114B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1146454A (en) * | 1995-09-29 | 1997-04-02 | 吉林市万发实业有限公司 | Technology for extracting nicotine from tobacco leaf |
| US20050263166A1 (en) * | 2004-05-27 | 2005-12-01 | Oh Soo H | Process for manufacturing low nicotine tabacco leaf substitute |
| CN102516226A (en) * | 2011-11-30 | 2012-06-27 | 薛刚 | Method for distilling and refining nicotine circularly and nicotine distilling and absorbing device |
| CN204522371U (en) * | 2015-04-10 | 2015-08-05 | 南阳师范学院 | A kind of steam for nicotine extraction occurs and sour absorption plant |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108627630A (en) * | 2018-04-03 | 2018-10-09 | 天津出入境检验检疫局化矿金属材料检测中心 | The device and detection method of halogens in mineral products are detected for steam distillation |
| CN115121120A (en) * | 2022-06-29 | 2022-09-30 | 湖北中烟工业有限责任公司 | Device and method for extracting concentrated nicotine |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104759114B (en) | 2015-12-30 |
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Granted publication date: 20151230 Termination date: 20200410 |