CN104746373A - Preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp - Google Patents

Preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp Download PDF

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Publication number
CN104746373A
CN104746373A CN201510097231.3A CN201510097231A CN104746373A CN 104746373 A CN104746373 A CN 104746373A CN 201510097231 A CN201510097231 A CN 201510097231A CN 104746373 A CN104746373 A CN 104746373A
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CN
China
Prior art keywords
pulp
broussonetia papyrifera
preparation process
natural
sectional material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510097231.3A
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Chinese (zh)
Inventor
腾铁生
张跃平
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Xinjiang Guoliyuan Investment Co., Ltd.
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Xinjiang Power Eco Japan Co Ltd Of State
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xinjiang Power Eco Japan Co Ltd Of State filed Critical Xinjiang Power Eco Japan Co Ltd Of State
Priority to CN201510097231.3A priority Critical patent/CN104746373A/en
Publication of CN104746373A publication Critical patent/CN104746373A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/02Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21BFIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT
    • D21B1/00Fibrous raw materials or their mechanical treatment
    • D21B1/04Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres
    • D21B1/12Fibrous raw materials or their mechanical treatment by dividing raw materials into small particles, e.g. fibres by wet methods, by the use of steam
    • D21B1/30Defibrating by other means
    • D21B1/34Kneading or mixing; Pulpers
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C3/00Pulping cellulose-containing materials
    • D21C3/22Other features of pulping processes

Abstract

The invention discloses a preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp. The preparation process comprises the following steps: (1) crushing broussonetia papyrifera into a sectional material with the length of 35-50mm, and removing dust; (2) feeding the sectional material subjected to dust removal into a boiling device, adding 3-5 percent of NaOH and 0.4-0.6 percent of anthraquinone according to the weight of the sectional material, and processing for 3-4 hours under the condition that the steam pressure is 0.3-0.4MPa; (3) sequentially feeding into a pulp extrusion machine, a double-screw thread-rolling device and a pulp grinding machine after the sectional material is processed in the step (2), thus obtaining coarse pulp; and (4) performing latency on the coarse pulp obtained in the step (3) through a hydrapulper to obtain the broussonetia papyrifera natural-color semi-chemimechanical pulp. Compared with an existing broussonetia papyrifera paper pulp chemical pulp-making method, the preparation process provided by the invention has the advantages of capability of obviously reducing black liquid quantity and reducing the environmental pollution and easiness for processing.

Description

The preparation technology of paper mulberry true qualities semichemical mechanical pulping
Technical field
The invention belongs to pulping and paper-making field, be specifically related to the preparation of paper mulberry true qualities semichemical mechanical pulping.
Background technology
Paper mulberry (formal name used at school Broussonetia papyrifera) calls Chu Tao etc., for deciduous tree, high 10-20m is strong positive seeds, have that fast-growing, strong adaptability, strong stress resistance, distribution are wide, feature that easily breeding, the period of felling in turn are short, all have distribution in the temperate zone of China, the torrid zone.
Generally adopt chemical pulping method with paper mulberry paper pulp at present; mainly contain sulfate process and sulphite process; adopt traditional chemical pulping method can produce a large amount of black liquor, and black liquor is also the primary pollution source of paper industry, this traditional pulping process is more and more difficult to the requirement meeting environmental protection.
Summary of the invention
The object of this invention is to provide a kind of preparation technology of paper mulberry true qualities semichemical mechanical pulping of more environmental protection.
It is as follows that the present invention realizes the technical scheme that above-mentioned purpose adopts:
The preparation technology of paper mulberry true qualities semichemical mechanical pulping, comprises the steps:
(1) paper mulberry is broken into the section material of 35-50mm, dedusting;
(2) the section material after dedusting is sent in boiling vessel, with section material weighing scale, add the anthraquinone of NaOH and 0.4-0.6% of 3-5%, under steam pressure is 0.3-0.4MPa, processes 3-4 hour;
(3) section material is after step (2) process, sends into press master, twin-screw thread rolling machine and fiberizer successively, is slightly starched;
(4) the thick slurry that obtains of step (3) is after hydrabrusher disappears and dives, and namely obtains paper mulberry true qualities semichemical mechanical pulping.
Compared with the chemical pulping method of traditional paper mulberry paper pulp, the present invention can obviously reduce black liquor amount, and more easily processes, and alleviates the pollution to environment.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further details.
Embodiment 1
(1) paper mulberry is sent into disintegrating machine, be broken into the section material of 35-50mm, goat's horn deduster sent into by qualified section material belt conveyor, to remove the heavy seeds such as dust, then sends into deposit feed bin;
(2) the section material laid in feed bin is sent in boiling vessel by conveying worm and is carried out sofening treatment, is specially with section material weighing scale, adds the NaOH of 4% and the anthraquinone of 0.5%, sofening treatment 3.5 hours under steam pressure is 0.35MPa;
(3) after step (2) process, discharging, with conveying worm, material is sent into high dense press master (slurry concentration 30-45wt%), extrude alkali lye wherein, slurry sends into twin-screw thread rolling machine by conveying worm again, carry out sub-wire process, send into high-density paste mill (slurry concentration 25-40wt%) through conveying worm again after sub-wire, slightly starched through defibrination;
(4) hydrabrusher sent into by the thick slurry that step (3) obtains, and after disappearing at a high speed and diving, starches concentration 5wt%, time 10-15min, namely obtain paper mulberry true qualities semichemical mechanical pulping when disappearing latent.
Embodiment 2
(1) paper mulberry is sent into disintegrating machine, be broken into the section material of 35-50mm, goat's horn deduster sent into by qualified section material belt conveyor, to remove the heavy seeds such as dust, then sends into deposit feed bin;
(2) the section material laid in feed bin is sent in boiling vessel by conveying worm and is carried out sofening treatment, is specially with section material weighing scale, adds the NaOH of 4.5% and the anthraquinone of 0.4%, sofening treatment 4 hours under steam pressure is 0.4MPa;
(3) after step (2) process, discharging, with conveying worm, material is sent into high dense press master (slurry concentration 30-45wt%), extrude alkali lye wherein, slurry sends into twin-screw thread rolling machine by conveying worm again, carry out sub-wire process, send into high-density paste mill (slurry concentration 25-40wt%) through conveying worm again after sub-wire, slightly starched through defibrination;
(4) hydrabrusher sent into by the thick slurry that step (3) obtains, and after disappearing at a high speed and diving, starches concentration 4wt%, time 10-15min, namely obtain paper mulberry true qualities semichemical mechanical pulping when disappearing latent.
Unless otherwise indicated, device therefor of the present invention is conventional equipment.
Adopt the inventive method, the yield of paper mulberry true qualities semichemical mechanical pulping can reach 75-80%, weight in wet base 3.5-5g.To produce 110g/m 2fluting medium is example, and the corrugated medium circling pressure index that paper mulberry true qualities semichemical mechanical pulping of the present invention is produced can reach 15.4 N.m/g, and double above than state's corrugated medium circling pressure index produced that gives up, fracture length can reach about 5000M.
In addition, industrial chemicals consumption of the present invention is less, and lignin stripping is few, and water wasting process is more simpler than traditional handicraft, and expense is little.

Claims (1)

1. the preparation technology of paper mulberry true qualities semichemical mechanical pulping, comprises the steps:
(1) paper mulberry is broken into the section material of 35-50mm, dedusting;
(2) the section material after dedusting is sent in boiling vessel, with section material weighing scale, add the anthraquinone of NaOH and 0.4-0.6% of 3-5%, under steam pressure is 0.3-0.4MPa, processes 3-4 hour;
(3) section material is after step (2) process, sends into press master, twin-screw thread rolling machine and fiberizer successively, is slightly starched;
(4) the thick slurry that obtains of step (3) is after hydrabrusher disappears and dives, and namely obtains paper mulberry true qualities semichemical mechanical pulping.
CN201510097231.3A 2015-03-05 2015-03-05 Preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp Pending CN104746373A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510097231.3A CN104746373A (en) 2015-03-05 2015-03-05 Preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510097231.3A CN104746373A (en) 2015-03-05 2015-03-05 Preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp

Publications (1)

Publication Number Publication Date
CN104746373A true CN104746373A (en) 2015-07-01

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CN201510097231.3A Pending CN104746373A (en) 2015-03-05 2015-03-05 Preparation process of broussonetia papyrifera natural-color semi-chemimechanical pulp

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CN (1) CN104746373A (en)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105178076A (en) * 2015-09-18 2015-12-23 新疆国力源投资有限公司 Preparing method for third-class linter unbleached pulp
CN105200838A (en) * 2015-09-18 2015-12-30 新疆国力源投资有限公司 Method of preparing bamboo willow bleaching pulp
CN106049147A (en) * 2016-07-07 2016-10-26 湖北工业大学 Semi-chemical pulping method for whole broussonetia papyrifera
CN106120420A (en) * 2016-07-07 2016-11-16 湖北工业大学 Broussonetia papyrifera sets chemical-mechanical pulping method entirely
CN106149435A (en) * 2016-07-07 2016-11-23 湖北工业大学 Broussonetia papyrifera sets chemical pulping method entirely
WO2017166860A1 (en) * 2016-03-28 2017-10-05 新疆国力源投资有限公司 Method for producing brownstock pulp using straws
CN107354790A (en) * 2017-07-14 2017-11-17 贵州册亨现代生态农业综合开发有限公司 A kind of method that paper pulp is prepared using paper mulberry rhizome as raw material
CN112726265A (en) * 2020-12-29 2021-04-30 江西理文造纸有限公司 Semi-chemical pulping method for plant fiber

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993022492A1 (en) * 1992-05-05 1993-11-11 Granit S.A. Production of cellulose by the soda-anthraquinone process (sap) with recovery of the boiling chemicals
CN1385580A (en) * 2001-05-11 2002-12-18 张志芬 Pulping using bark of artificial quickly-grown Common Papermulberry (HAP method) and trunk (APMP method)
CN101451323A (en) * 2007-12-05 2009-06-10 山东泉林纸业有限责任公司 Un-bleaching pulp prepared by alkaline steam cooking wheat straw raw material, preparation method and use thereof
CN101736628A (en) * 2008-11-12 2010-06-16 中国制浆造纸研究院 Explosion pulping method for bamboo or cotton stalks or wood or various twigs
CN101871135A (en) * 2009-04-27 2010-10-27 中国制浆造纸研究院 Method for producing bleaching man-made fiber pulp

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993022492A1 (en) * 1992-05-05 1993-11-11 Granit S.A. Production of cellulose by the soda-anthraquinone process (sap) with recovery of the boiling chemicals
CN1385580A (en) * 2001-05-11 2002-12-18 张志芬 Pulping using bark of artificial quickly-grown Common Papermulberry (HAP method) and trunk (APMP method)
CN101451323A (en) * 2007-12-05 2009-06-10 山东泉林纸业有限责任公司 Un-bleaching pulp prepared by alkaline steam cooking wheat straw raw material, preparation method and use thereof
CN101736628A (en) * 2008-11-12 2010-06-16 中国制浆造纸研究院 Explosion pulping method for bamboo or cotton stalks or wood or various twigs
CN101871135A (en) * 2009-04-27 2010-10-27 中国制浆造纸研究院 Method for producing bleaching man-made fiber pulp

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105178076A (en) * 2015-09-18 2015-12-23 新疆国力源投资有限公司 Preparing method for third-class linter unbleached pulp
CN105200838A (en) * 2015-09-18 2015-12-30 新疆国力源投资有限公司 Method of preparing bamboo willow bleaching pulp
WO2017166860A1 (en) * 2016-03-28 2017-10-05 新疆国力源投资有限公司 Method for producing brownstock pulp using straws
CN106049147A (en) * 2016-07-07 2016-10-26 湖北工业大学 Semi-chemical pulping method for whole broussonetia papyrifera
CN106120420A (en) * 2016-07-07 2016-11-16 湖北工业大学 Broussonetia papyrifera sets chemical-mechanical pulping method entirely
CN106149435A (en) * 2016-07-07 2016-11-23 湖北工业大学 Broussonetia papyrifera sets chemical pulping method entirely
CN106049147B (en) * 2016-07-07 2017-10-27 湖北工业大学 Paper mulberry sets semichemical method pulping process entirely
CN106149435B (en) * 2016-07-07 2017-11-10 湖北工业大学 Paper mulberry sets chemical pulping method entirely
CN107354790A (en) * 2017-07-14 2017-11-17 贵州册亨现代生态农业综合开发有限公司 A kind of method that paper pulp is prepared using paper mulberry rhizome as raw material
CN112726265A (en) * 2020-12-29 2021-04-30 江西理文造纸有限公司 Semi-chemical pulping method for plant fiber

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C41 Transfer of patent application or patent right or utility model
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Effective date of registration: 20161021

Address after: 830000, No. 2, building 6, Nanshan New District office building, the Xinjiang Uygur Autonomous Region, Shihezi

Applicant after: Xinjiang Guoliyuan Investment Co., Ltd.

Address before: 830000, the Xinjiang Uygur Autonomous Region, Urumqi hi tech Development Zone, 21, Yu Xin District, Guilin Road, 3, 4, 2, 402

Applicant before: Xinjiang Power Eco Japan Co., Ltd. of state

RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20150701