CN104739745A - Firming neck cream and preparation method thereof - Google Patents

Firming neck cream and preparation method thereof Download PDF

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Publication number
CN104739745A
CN104739745A CN201310735317.5A CN201310735317A CN104739745A CN 104739745 A CN104739745 A CN 104739745A CN 201310735317 A CN201310735317 A CN 201310735317A CN 104739745 A CN104739745 A CN 104739745A
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China
Prior art keywords
pot
oil
water
temperature
homogenizing
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Pending
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CN201310735317.5A
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Chinese (zh)
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陈冬英
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DALIAN MEILE BIOLOGICAL TECHNOLOGY DEVELOPMENT Co Ltd
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DALIAN MEILE BIOLOGICAL TECHNOLOGY DEVELOPMENT Co Ltd
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Priority to CN201310735317.5A priority Critical patent/CN104739745A/en
Publication of CN104739745A publication Critical patent/CN104739745A/en
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Abstract

A firming neck cream comprises cetyl octadecyl alcohol, stearic acid, glycerin monostearate, mink oil, white oil, an alga extract liquid, rose water, witch hazel water, methylparaben, diazolidinyl urea and deionized water. A preparation method of the firming neck cream comprises the following steps: 1, adding cetyl octadecyl alcohol, stearic acid, glycerin monostearate, dimethicone, mink oil, white oil, potassium hexadecyl phosphate and vitamin E into an oil pot, and heating; 2, adding deionized water into a water pot, adding glycerin, allantoin and methylparaben into the water pot, and heating; 3, adding diazolidinyl urea into propylene glycol; 4, heating an emulsifying pot, and carrying out vacuum pumping; 5, pumping the material in the oil pot into the emulsifying pot; 6, pumping the material in the water pot into the emulsifying pot, and homogenizing; 7, cooling; 8, adding a mixture obtained in step 3 into the emulsifying pot, and adding the alga extract liquid, rose water and witch hazel water; 9, sampling; 10, discharging; and 11, sending a material discharged from the emulsifying pot to a standing room, ageing for 12h, loading, and packaging. The firming neck cream can firm necks.

Description

One is compacted restructuring compound for the neck and preparation method thereof
technical fieldthe present invention relates to a kind of cosmetics, particularly a kind of restructuring compound for the neck.
background technologyexisting restructuring compound for the neck, primarily of Chinese medicine angelica, Radix Ginseng, Radix Codonopsis, astragalus, CHUANSHAO, BAIYOU composition, adds cream base through extraction and obtains.There is the effect of moist cervical region.Its weak point: do not have and have the effect of compacting to cervical region.
summary of the inventionthe object of this invention is to provide a kind ofly has the one of effect of compacting to compact restructuring compound for the neck and preparation method thereof to cervical region.
Technical scheme of the present invention is: one is compacted restructuring compound for the neck, its composition mainly comprises 16,18 alcohol, stearic acid, glyceryl monostearate, dimethicone, ermine oil, white oil, hexadecanyl phosphate potassium salt, vitamin E, glycerol, propylene glycol, allantoin, seaweed extracted liquor, rose wate, Radix Hamamelidis Mollis water, mud pool tortoise beetle ester, two imidazolidinyl urine and deionized water.Wherein, be 1 ultimate unit with deionized water, deionized water and 16, 18 alcohol, stearic acid, glyceryl monostearate, dimethicone, ermine oil, white oil, hexadecanyl phosphate potassium salt, vitamin E, glycerol, propylene glycol, allantoin, seaweed extracted liquor, rose wate, Radix Hamamelidis Mollis water, mud pool tortoise beetle ester, the mass ratio of two imidazolidinyl urine is 1:0.04454 ~ 0.05444, 1:0.04454 ~ 0.05444, 1:0.02969 ~ 0.03629, 1:0.02969 ~ 0.03629, 1:0.06919 ~ 0.09578, 1:0.07908 ~ 0.11887, 1:0.04454 ~ 0.05444, 1:0.00742 ~ 0.00907, 1:0.07908 ~ 0.11887, 1:0.07908 ~ 0.11887, 1:0.04454 ~ 0.05444, 1:0.00223 ~ 0.00272, 1:0.02969 ~ 0.03629, 1:0.00119 ~ 0.00145, 1:0.00223 ~ 0.00272, 1:0.00297 ~ 0.00363.
The manufacture method of restructuring compound for the neck of compacting realizes according to the following steps:
(1) 16,18 alcohol, stearic acid, glyceryl monostearate, dimethicone, ermine oil, white oil, hexadecanyl phosphate potassium salt, vitamin E are put into oil cauldron and are mixed, heating-up temperature 80 DEG C ± 2 DEG C, and constant temperature stirs 10 minutes;
(2) deionized water enters in kettle, opens stirring, glycerol, allantoin, and mud pool tortoise beetle ester puts into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, and constant temperature stirs 10 minutes;
(3) two imidazolidinyl urine puts into propylene glycol, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 3 in emulsifying pot, stirs 2 minutes, adds seaweed extracted liquor respectively, rose wate, Radix Hamamelidis Mollis water, continues to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.
The present invention compared with prior art tool has the following advantages: have to cervical region effect of compacting.
detailed description of the invention
Embodiment 1
The manufacture method of restructuring compound for the neck of compacting realizes according to the following steps:
(1) 16,18 alcohol 0.04454kg, stearic acid 0.04454 kg, glyceryl monostearate 0.02969 kg, dimethicone 0.02969 kg, ermine oil 0.06919 kg, white oil 0.07908 kg, hexadecanyl phosphate potassium salt 0.04454 kg, vitamin E 0.00742 kg put into oil cauldron and mix, heating-up temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(2) deionized water 1.1 kg enters in kettle, opens stirring, glycerol 0.07908 kg, allantoin 0.00445 kg, and mud pool tortoise beetle ester 0.00223 kg puts into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, and constant temperature stirs 10 minutes;
(3) two imidazolidinyl is urinated 0.00297 kg and is put into propylene glycol 0.07908 kg, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, the mixed material of step 3 is added in emulsifying pot, stir 2 minutes, add seaweed extracted liquor 0.00223 kg respectively, rose wate 0.02969 kg, Radix Hamamelidis Mollis water 0.00119 kg, continue to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.
Embodiment 2
The manufacture method of restructuring compound for the neck of compacting realizes according to the following steps:
(1) 16,18 alcohol 0.05444 kg, stearic acid 0.05444 kg, glyceryl monostearate 0.03629 kg, dimethicone 0.03629 kg, ermine oil 0.09578 kg, white oil 0.11887 kg, hexadecanyl phosphate potassium salt 0.05444 kg, vitamin E 0.00907 kg put into oil cauldron and mix, heating-up temperature 80 DEG C ± 2 DEG C, constant temperature stirs 10 minutes;
(2) deionized water 0.9 kg enters in kettle, opens stirring, glycerol 0.11887 kg, allantoin 0.00544 kg, and mud pool tortoise beetle ester 0.00272 kg puts into aqueous phase pot, agitating heating, temperature 80 DEG C ± 2 DEG C, and constant temperature stirs 10 minutes;
(3) two imidazolidinyl is urinated 0.00363 kg and is put into propylene glycol, and stirring and dissolving is even, for subsequent use;
(4) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(5) will meet the requirements of in oil cauldron material suction emulsifying pot, open stirring, mixing speed 300rpm, temperature 80 DEG C ± 1 DEG C;
(6) rapidly by kettle material suction emulsifying pot, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time 6 minutes, and homogenizing terminates, and constant temperature stirs 10 minutes;
(7) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;
(8) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, the mixed material of step 3 is added in emulsifying pot, stir 2 minutes, add seaweed extracted liquor 0.00272 kg respectively, rose wate 0.03629 kg, Radix Hamamelidis Mollis water 0.00145 kg, continue to stir;
(9) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates 10 minutes;
(10) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;
(11) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.

Claims (2)

1. compact a restructuring compound for the neck, it is characterized in that: raw material 16,18 alcohol comprised, stearic acid, glyceryl monostearate, dimethicone, ermine oil, white oil, hexadecanyl phosphate potassium salt, vitamin E, glycerol, propylene glycol, allantoin, seaweed extracted liquor, rose wate, Radix Hamamelidis Mollis water, mud pool tortoise beetle ester, two imidazolidinyl urine and deionized water are 1 ultimate unit with deionized water, deionized water and 16,18 alcohol, stearic acid, glyceryl monostearate, dimethicone, ermine oil, white oil, hexadecanyl phosphate potassium salt, vitamin E, glycerol, propylene glycol, allantoin, seaweed extracted liquor, rose wate, Radix Hamamelidis Mollis water, mud pool tortoise beetle ester, the mass ratio of two imidazolidinyl urine is 1:0.04454 ~ 0.05444, 1:0.04454 ~ 0.05444, 1:0.02969 ~ 0.03629,1:0.02969 ~ 0.03629,1:0.06919 ~ 0.09578, 1:0.07908 ~ 0.11887, 1:0.04454 ~ 0.05444,1:0.00742 ~ 0.00907,1:0.07908 ~ 0.11887, 1:0.07908 ~ 0.11887, 1:0.04454 ~ 0.05444,1:0.00223 ~ 0.00272,1:0.02969 ~ 0.03629, 1:0.00119 ~ 0.00145, 1:0.00223 ~ 0.00272, 1:0.00297 ~ 0.00363.
2. to compact the preparation method of restructuring compound for the neck, it is characterized in that: (1) octyl methoxycinnamate and dibenzoyl methane butyl ester mixed dissolution homogeneous transparent, then benzoate is put into wherein, stir;
(2) by squalane, dimethicone, caprylic capric triglyceride, 16-18 alcohol, stearic acid, monoglyceride, methoxyl group sesquistearate, polyoxyethylene ether methoxyl group sesquistearate, α-bisabolol puts into oil cauldron, heating, and stir, temperature controls at 80 ± 2 DEG C;
(3) deionized water puts into kettle, opens stirring, ethylenediaminetetraacetic acid is put into kettle stirring and dissolving; Put into wherein by HANSHENGJIAO again, stirring and dissolving is even, and start heating, temperature controls at 85 ± 2 DEG C;
(4) zinc oxide, vitamin B3, glycerol, methyl hydroxybenzoate puts into kettle, stirs and dissolves completely, for subsequent use;
(5) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;
(6) then pour into rapidly in oil phase pot by the raw material of step 1, stir, titanium dioxide dispersion pulp is put into oil phase pot and is stirred;
(7) will meet the requirements of in the mixed material suction emulsifying pot of step 6, open stirring, stir fast 200rpm, then by the material suction emulsifying pot of aqueous phase pot, mixing speed brings up to 500rpm, open homogenizer, homogenizing speed 1800rpm, treats that in material whole suction emulsifying pot, homogenizing speed brings up to 2000rpm, homogenizing 6 minutes, constant temperature stirs 10 minutes;
(8) lower the temperature, cooling rate 2 DEG C/3min, temperature drops to 72 DEG C, again homogenizing, homogenizing speed 1800rpm, 3 minutes time;
(9) continue cooling, temperature reduces to 50 DEG C, and essence, two imidazolidinyl urine adds in emulsifying pot, stirs;
(10) temperature reduces to 42 DEG C, sample analysis, and after qualified, temperature reduces to 40 DEG C, takes the dish out of the pot.
CN201310735317.5A 2013-12-28 2013-12-28 Firming neck cream and preparation method thereof Pending CN104739745A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375184A (en) * 2017-08-22 2017-11-24 卢倩 A kind of restructuring compound for the neck formula with soporific function and preparation method thereof
CN107456427A (en) * 2017-08-23 2017-12-12 本蜜(上海)科技有限公司 Lift the tender restructuring compound for the neck that compacts
CN108635297A (en) * 2018-07-03 2018-10-12 广东名辰堂健康产业股份有限公司 A kind of hand lotion and preparation method thereof with moisture retention
CN109223596A (en) * 2018-09-18 2019-01-18 栗丽 A kind of promoting blood circulation maintenance frost and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040185069A1 (en) * 2003-03-22 2004-09-23 Gupta Shyam K. Hydroxycitric acid derivatives for body slimming and tone firming compositions
CN102406581A (en) * 2011-11-28 2012-04-11 天津郁美净集团有限公司 Skin protecting composite with function of tightening skin

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20040185069A1 (en) * 2003-03-22 2004-09-23 Gupta Shyam K. Hydroxycitric acid derivatives for body slimming and tone firming compositions
CN102406581A (en) * 2011-11-28 2012-04-11 天津郁美净集团有限公司 Skin protecting composite with function of tightening skin

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375184A (en) * 2017-08-22 2017-11-24 卢倩 A kind of restructuring compound for the neck formula with soporific function and preparation method thereof
CN107456427A (en) * 2017-08-23 2017-12-12 本蜜(上海)科技有限公司 Lift the tender restructuring compound for the neck that compacts
CN108635297A (en) * 2018-07-03 2018-10-12 广东名辰堂健康产业股份有限公司 A kind of hand lotion and preparation method thereof with moisture retention
CN109223596A (en) * 2018-09-18 2019-01-18 栗丽 A kind of promoting blood circulation maintenance frost and preparation method thereof

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Application publication date: 20150701