CN104739667A - Moisturizing emulsion and preparation method thereof - Google Patents

Abstract

A moisturizing emulsion mainly comprises disodium ethylene diamine tetraacetate, shea butter, dimethicone, isobutyl palmitate, sweet almond oil, bisabolol, vitamin E acetate, 2,6-di-tert-butyl-4-methylphenol, deionized water, propylene glycol, glycerin, allantoin, xanthan gum, mycose, diazolidinyl urea, iodopropynyl butylcarbamate, methylparaben and an essence. A preparation method of the moisturizing emulsion comprises the following steps: 1, heating sweet almond oil and shea butter, and adding 2,6-di-tert-butyl-4-methylphenol and vitamin E acetate; 2, mixing ethylene diamine tetraacetate, dimethicone, isobutyl palmitate and bisabolol in an oil pot; 3, mixing water, xanthan gum and glycerin in a water pot; 4, mixing propylene glycol with diazolidinyl urea, and adding iodopropynyl butylcarbamate; 5, adding allantoin, mycose and methylparaben into the water pot; 6, heating an emulsifying pot; and 7, adding a material obtained in step 1 into the oil pot, pumping the material in the oil pot to the emulsifying pot, cooling, adding a material obtained in step 4 to the emulsifying pot, and adding the essence. The moisturizing emulsion can moisten skins and maintain skins moist.

Description

A kind of moisturizing emulsion and preparation method thereof

technical fieldthe present invention relates to technical field of skin care, particularly a kind of moisturizing emulsion and preparation method thereof.

background technologybecause modern people's rhythm of life is fast, and by various environmental effect, the frequent drying of skin, intensely dark pool.Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) discloses a kind of skincare humectant.It is made up of according to the following number of weight ratio following component: skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.Its weak point: can not help rapidly moist dry skin, makes skin exquisiteness soft and smooth, can not more deeply be diffused into skin depths, be combined with deep water, keeps the moist of skin.

summary of the inventionthe object of this invention is to provide one and can either help rapidly moist dry skin, make skin exquisiteness soft and smooth, can more deeply be diffused into skin depths again, be combined with deep water, moist a kind of moisturizer keeping skin and preparation method thereof.

Technical scheme of the present invention is: a kind of moisturizer, its composition mainly comprises disodiumedetate, shea butter, dimethicone, iso-octyl palmitate, Semen pruni armeniacae oil, bisabolol, Vitamin E acetate, 2,6-di-tert-butyl-4-methy phenols, deionized water, propylene glycol, glycerol, allantoin, HANSHENGJIAO, trehalose, two imidazolidinyl urea, iodo propinyl butyl carbamate, methyl hydroxybenzoate and essence.Wherein, be 1 ultimate unit with deionized water, deionized water and disodiumedetate, shea butter, dimethicone, iso-octyl palmitate, Semen pruni armeniacae oil, bisabolol, Vitamin E acetate, 2,6-di-tert-butyl-4-methy phenol, propylene glycol, glycerol, allantoin, HANSHENGJIAO, trehalose, two imidazolidinyl urea, iodo propinyl butyl carbamate, methyl hydroxybenzoate, the mass ratio of essence is 1:0.01591 ~ 0.05389, 1:0.01197 ~ 0.01463,1:0.01800 ~ 0.02200,1:0.04797 ~ 0.08863,1:0.05866 ~ 0.09826,1:0.00117 ~ 0.00143,1:0.00243 ~ 0.00297,1:0.00027 ~ 0.00033,1:0.05866 ~ 0.0.09826,1:0.01591 ~ 0.04389,1:0.00243 ~ 0.00293,1:0.00243 ~ 0.00293,1:0.01800 ~ 0.02200,1:0.00117 ~ 0.00143,1:0.00009 ~ 0.00011,1:0.00018 ~ 0.00022,1:0.00603 ~ 0.00737.

The manufacture method of moisturizing emulsion realizes according to the following steps:

(1) Semen pruni armeniacae oil mixes with shea butter, heating, and stability contorting, at 45 DEG C, adds 2,6-di-tert-butyl-4-methy phenol, dissolves, stirs, add Vitamin E acetate, stir, stand-by;

(2) by disodiumedetate, dimethicone, iso-octyl palmitate, bisabolol is put into oil cauldron and is mixed, heating-up temperature about 80 DEG C, and constant temperature stirs 10 minutes;

(3) deionized water enters kettle; HANSHENGJIAO is mixed homogeneously with glycerol, adds in kettle and stirs;

(4) propylene glycol mixes with two imidazolidinyl urea, adds iodo propinyl butyl carbamate, stir, be uniformly dissolved completely after dissolving completely, stand-by;

(5) allantoin, trehalose, methyl hydroxybenzoate adds in kettle, heating kettle, and temperature controls at about 85 DEG C, and constant temperature stirs 10 minutes;

(6) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;

(7) material of step 1 is added in oil cauldron, stir 2 minutes.

(8) material in oil cauldron is pumped in emulsifying pot, opens stirring, mixing speed 300rpm, temperature about 80 DEG C;

(9) be pumped in emulsifying pot by kettle material rapidly, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time about 6 minutes, homogenizing terminates, and constant temperature stirs 10 minutes;

(10) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to about 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;

(11) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 4 in emulsifying pot, stirs 2 minutes, adds essence, continues to stir;

(12) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates about 10 minutes;

(13) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;

(14) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.

The present invention compared with prior art tool has the following advantages: can help rapidly moist dry skin, makes skin exquisiteness soft and smooth, can more deeply be diffused into skin depths again, be combined with deep water, keeps the moist of skin.

detailed description of the invention

Embodiment 1

The manufacture method of moisturizing emulsion realizes according to the following steps:

(1) Semen pruni armeniacae oil 0.05866kg mixes with shea butter 0.01197kg, heating, and stability contorting, at 45 DEG C, adds 2,6-di-tert-butyl-4-methy phenol 0.00027kg, dissolves, stirs, add Vitamin E acetate 0.00243kg, stir, stand-by;

(2) by disodiumedetate 0.01591kg, dimethicone 0.018kg, iso-octyl palmitate 0.04797kg, bisabolol 0.00117kg put into oil cauldron and mix, heating-up temperature about 80 DEG C, and constant temperature stirs 10 minutes;

(3) deionized water 1.1kg enters kettle; HANSHENGJIAO 0.00243kg is mixed homogeneously with glycerol 0.01591kg, adds in kettle and stirs;

(4) propylene glycol 0.05866kg mixes with two imidazolidinyl urea 0.00117kg, adds iodo propinyl butyl carbamate 0.00009kg, stir, be uniformly dissolved completely after dissolving completely, stand-by;

(5) allantoin 0.00243kg, trehalose 0.018kg, methyl hydroxybenzoate 0.00018kg adds in kettle, heating kettle, and temperature controls at about 85 DEG C, and constant temperature stirs 10 minutes;

(6) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;

(7) material of step 1 is added in oil cauldron, stir 2 minutes.

(8) material in oil cauldron is pumped in emulsifying pot, opens stirring, mixing speed 300rpm, temperature about 80 DEG C;

(9) be pumped in emulsifying pot by kettle material rapidly, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time about 6 minutes, homogenizing terminates, and constant temperature stirs 10 minutes;

(10) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to about 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;

(11) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 4 in emulsifying pot, stirs 2 minutes, adds essence 0.00603 kg, continues to stir;

(12) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates about 10 minutes;

(13) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;

(14) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.

Embodiment 2

The manufacture method of moisturizing emulsion realizes according to the following steps:

(1) Semen pruni armeniacae oil 0.09826kg mixes with shea butter 0.01463kg, heating, and stability contorting, at 45 DEG C, adds 2,6-di-tert-butyl-4-methy phenol 0.00033kg, dissolves, stirs, add Vitamin E acetate 0.00297kg, stir, stand-by;

(2) by disodiumedetate 0.05389kg, dimethicone 0.022kg, iso-octyl palmitate 0.08863kg, bisabolol 0.00143kg put into oil cauldron and mix, heating-up temperature about 80 DEG C, and constant temperature stirs 10 minutes;

(3) deionized water 0.9kg enters kettle; HANSHENGJIAO 0.00293kg is mixed homogeneously with glycerol 0.04389kg, adds in kettle and stirs;

(4) propylene glycol 0.05866kg mixes with two imidazolidinyl urea 0.00143kg, adds iodo propinyl butyl carbamate 0.00011kg, stir, be uniformly dissolved completely after dissolving completely, stand-by;

(5) allantoin 0.00293kg, trehalose 0.022kg, methyl hydroxybenzoate 0.00022kg adds in kettle, heating kettle, and temperature controls at about 85 DEG C, and constant temperature stirs 10 minutes;

(6) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;

(7) material of step 1 is added in oil cauldron, stir 2 minutes.

(8) material in oil cauldron is pumped in emulsifying pot, opens stirring, mixing speed 300rpm, temperature about 80 DEG C;

(9) be pumped in emulsifying pot by kettle material rapidly, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time about 6 minutes, homogenizing terminates, and constant temperature stirs 10 minutes;

(10) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to about 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;

(11) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 4 in emulsifying pot, stirs 2 minutes, adds essence 0.00737 kg, continues to stir;

(12) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates about 10 minutes;

(13) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;

(14) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.

Claims (2)

1. a moisturizing emulsion, is characterized in that: the raw material comprised, and is 1 ultimate unit with deionized water, deionized water and disodiumedetate, shea butter, dimethicone, iso-octyl palmitate, Semen pruni armeniacae oil, bisabolol, Vitamin E acetate, 2,6-di-tert-butyl-4-methy phenol, propylene glycol, glycerol, allantoin, HANSHENGJIAO, trehalose, two imidazolidinyl urea, iodo propinyl butyl carbamate, methyl hydroxybenzoate, the mass ratio of essence is 1:0.01591 ~ 0.05389, 1:0.01197 ~ 0.01463,1:0.01800 ~ 0.02200,1:0.04797 ~ 0.08863,1:0.05866 ~ 0.09826,1:0.00117 ~ 0.00143,1:0.00243 ~ 0.00297,1:0.00027 ~ 0.00033,1:0.05866 ~ 0.0.09826,1:0.01591 ~ 0.04389,1:0.00243 ~ 0.00293,1:0.00243 ~ 0.00293,1:0.01800 ~ 0.02200,1:0.00117 ~ 0.00143,1:0.00009 ~ 0.00011,1:0.00018 ~ 0.00022,1:0.00603 ~ 0.00737.

2. a preparation method for moisturizing emulsion, is characterized in that: (1) Semen pruni armeniacae oil mixes with shea butter, heating, and stability contorting is at 45 DEG C, add 2,6-di-tert-butyl-4-methy phenol, dissolve, stir, add Vitamin E acetate, stir, stand-by;

(2) by disodiumedetate, dimethicone, iso-octyl palmitate, bisabolol is put into oil cauldron and is mixed, heating-up temperature about 80 DEG C, and constant temperature stirs 10 minutes;

(3) deionized water enters kettle; HANSHENGJIAO is mixed homogeneously with glycerol, adds in kettle and stirs;

(4) propylene glycol mixes with two imidazolidinyl urea, adds iodo propinyl butyl carbamate, stir, be uniformly dissolved completely after dissolving completely, stand-by;

(5) allantoin, trehalose, methyl hydroxybenzoate adds in kettle, heating kettle, and temperature controls at about 85 DEG C, and constant temperature stirs 10 minutes;

(6) heating emulsification pot, about temperature 45 C, evacuation, vacuum remains on 0.05Mpa;

(7) material of step 1 is added in oil cauldron, stir 2 minutes;

(8) material in oil cauldron is pumped in emulsifying pot, opens stirring, mixing speed 300rpm, temperature about 80 DEG C;

(9) be pumped in emulsifying pot by kettle material rapidly, mixing speed brings up to 500rpm, opens homogenizer, homogenizing speed 1800rpm, treats that material all exhausts, and homogenizing speed brings up to 2000rpm, homogenizing time about 6 minutes, homogenizing terminates, and constant temperature stirs 10 minutes;

(10) lower the temperature, open the cooling water of emulsifying pot, cooling rate 3 DEG C/2 minutes, treats that temperature reduces to about 70 DEG C, again opens homogenizer, homogenizing speed 1800rpm, homogenizing time 3 minutes;

(11) treat that temperature reduces to 60 DEG C, mixing speed reduces to 400rpm, and temperature reduces to 45 DEG C, is added by the mixed material of step 4 in emulsifying pot, stirs 2 minutes, adds essence, continues to stir;

(12) sample, analyze, do discharging simultaneously and prepare, sterilization discharge tank, opens uviol lamp, irradiates about 10 minutes;

(13) treat that temperature reduces to 40 DEG C, after sample analysis result is qualified, discharging;

(14) material taken the dish out of the pot pushes rest chamber, ageing fill afterwards in 12 hours, packaging.