CN104729312A - Device for improving condensation effect of barrier wall type condenser based on partial reflux circulation - Google Patents

Device for improving condensation effect of barrier wall type condenser based on partial reflux circulation Download PDF

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Publication number
CN104729312A
CN104729312A CN201510092807.7A CN201510092807A CN104729312A CN 104729312 A CN104729312 A CN 104729312A CN 201510092807 A CN201510092807 A CN 201510092807A CN 104729312 A CN104729312 A CN 104729312A
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wall type
type condenser
dividing wall
reflux
gas
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CN201510092807.7A
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CN104729312B (en
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羌宁
羌烨晟
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Environmental Protection Technology Co Ltd Is Won In Nanjing Million
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Environmental Protection Technology Co Ltd Is Won In Nanjing Million
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Abstract

The invention discloses a device for improving a condensation effect of a barrier wall type condenser based on partial reflux circulation. A barrier wall type condenser inlet is formed in one end of the barrier wall type condenser, and a barrier wall type condenser gas outlet provided with a reflux gas branch pipe is formed in the other end of the barrier wall type condenser. A barrier wall type condenser body is connected with cooling media, and the barrier wall type condenser gas outlet provided with the reflux gas branch pipe is connected with a reflux gas power device and a demister through pipelines respectively. The reflux gas power device is connected with a reflux gas inlet through a pipeline, and the reflux gas inlet is located in the barrier wall type condenser and is provided with a reflux mixer. The bottom of the end provided with the barrier wall type condenser gas outlet provided with the reflux gas branch pipe of the barrier wall type condenser is provided with a barrier wall type condenser fluid discharge port. The bottom of the demister is provided with a demister fluid drainage port. The barrier wall type condenser fluid discharge port and the demister fluid drainage port are connected with a main fluid drainage port through pipelines. The demister is provided with a non-condensable gas outlet. The device has the advantage of improving condensation efficiency.

Description

A kind of partial reflux circulation improves the device of dividing wall type condenser condenses effect
Technical field
The invention belongs to technical field of environmental protection in chemical industry, relate to the device that the circulation of a kind of partial reflux improves dividing wall type condenser condenses effect.
Background technology
Condensation is complete the separation of gaseous component and recovery by phase transformation as a kind of common elements operating process, is widely used in chemical industry, the numerous areas such as environmental protection, heat energy.The condensation efficiency how improving dividing wall type condenser is one of power of current technical development.Current technological progress is mainly reflected in dividing wall type condenser condenses face mode and internal gas flow turbulent fluctuation improves mass transfer and heat-transfer capability, comprises fin, inner screen component, a lot of form such as internal helicoid component.Condensation process is that in a gas, constituent part is caught a cold and arrived below dew-point temperature, be liquefied as the process of liquid and particle thereof, according to kelvin's law, the vapour pressure of granule liquid is greater than the vapour pressure on main body of liquid surface, therefore for condensation process, gas phase is in the process of liquid-phase conversion, and particle need be grown up could to stablize after certain particle diameter and be transformed to liquid-phase particle state, is the dynamic balance state being in condensation and evaporation when being less than a certain particle diameter.
Existing dividing wall type condenser is mainly considered to improve condensation efficiency from mass transfer and heat transfer angle, but does not all consider the supersaturation nucleation stage that granule condensation growth process must experience, and condensation efficiency also exists room for promotion.
Summary of the invention
The object of the present invention is to provide a kind of partial reflux to circulate and improve the device of dividing wall type condenser condenses effect, solve existing dividing wall type condenser mainly to consider to improve condensation efficiency from mass transfer and heat transfer angle, but all do not consider the supersaturation nucleation stage that granule condensation growth process must experience, the problem that condensation efficiency is lower.
The technical solution adopted in the present invention comprises dividing wall type condenser, dividing wall type condenser one end is provided with dividing wall type condenser inlet, the other end is provided with the dividing wall type condenser-air outlet of band reflux gas arm, dividing wall type condenser body connects cooling media, cooling media provides refrigerant to dividing wall type condenser, dividing wall type condenser-air outlet with reflux gas arm connects reflux gas power set and demister respectively by pipeline, reflux gas power set connect reflux gas entrance by pipeline, reflux gas entrance is positioned on dividing wall type condenser, make dividing wall type condenser inside and export with the dividing wall type condenser-air of band reflux gas arm, the pipeline that reflux gas entrance connects forms a gas passage, reflux gas porch is provided with adverse current blender, the bottom of the dividing wall type condenser-air exit end of the band reflux gas arm of dividing wall type condenser is provided with dividing wall type condenser liquid outlet, demister bottom is provided with demister leakage fluid dram, dividing wall type condenser liquid outlet is connected total leakage fluid dram with demister leakage fluid dram by pipeline, demister is provided with incoagulable gas outlet.
Further, described reflux gas entrance is between the 10%-90% of the vapor path length of dividing wall type condenser.
Further, the gas flow of the dividing wall type condenser-air outlet return of described band reflux gas arm is the 1%-60% of the gas gross to be condensed at dividing wall type condenser inlet place.
The invention has the beneficial effects as follows raising condensation efficiency.
Accompanying drawing explanation
Fig. 1 is the apparatus structure schematic diagram that a kind of partial reflux circulation of the present invention improves dividing wall type condenser condenses effect.
In figure, 1. dividing wall type condenser, 2. dividing wall type condenser inlet, 3. be with the dividing wall type condenser-air outlet of reflux gas arm, 4. cooling media, 5. reflux gas power set, 6. demister, 7. reflux gas entrance, 8. adverse current blender, 9. dividing wall type condenser liquid outlet, 10. demister leakage fluid dram, 11. total leakage fluid drams, 12. incoagulable gas outlets.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is described in detail.
The present invention as shown in Figure 1, comprise dividing wall type condenser 1, dividing wall type condenser 1 one end is provided with dividing wall type condenser inlet 2, the other end is provided with the dividing wall type condenser-air outlet 3 of band reflux gas arm, dividing wall type condenser 1 body connects cooling media 4, cooling media 4 provides refrigerant to dividing wall type condenser 1, dividing wall type condenser-air outlet 3 with reflux gas arm connects reflux gas power set 5 and demister 6 respectively by pipeline, reflux gas power set 5 connect reflux gas entrance 7 by pipeline, reflux gas entrance 7 is positioned on dividing wall type condenser 1, make dividing wall type condenser 1 inside and export 3 with the dividing wall type condenser-air of band reflux gas arm, the pipeline that reflux gas entrance 7 connects forms a gas passage, reflux gas entrance 7 place is provided with adverse current blender 8, the bottom that the dividing wall type condenser-air of the band reflux gas arm of dividing wall type condenser 1 exports 3 one end is provided with dividing wall type condenser liquid outlet 9, demister leakage fluid dram 10 is provided with bottom demister 6, dividing wall type condenser liquid outlet 9 is connected total leakage fluid dram 11 with demister leakage fluid dram 10 by pipeline, demister 6 is provided with incoagulable gas outlet 12.
Reflux gas entrance 6 is between the 10%-90% of the vapor path length of dividing wall type condenser 1.
It is inner that gas to be condensed enters dividing wall type condenser 1 by condensing gas entrance 2, sent by cooling media 4 refrigerant cooling after in the gas passage of dividing wall type condenser 1, there is condensation, part congeal into bulky grain sedimentation or after being condensed in heat-transfer surface surface because Gravitational sliding is finally discharged from the dividing wall type condenser liquid outlet 9 of bottom.Due to the factor of Kelvin effect, a large amount of fine droplets is also there is in flowing gas, with dividing wall type condenser-air outlet 3 flowing of air-flow to the band reflux gas arm of dividing wall type condenser, now reflux gas power set 5 export 3 from the dividing wall type condenser-air of band reflux gas arm and extract portion gas, (gas of extraction is the 1%-60% of the gas gross to be condensed of input), be back to reflux gas entrance 7 place, fully to be mixed with the gas to be condensed condensing to uniform temperature by adverse current blender 8 and contact, for the gas be in the dividing wall type condenser 1 of hypersaturated state provides the nuclei of condensation, impel in the inner space of dividing wall type condenser 1 and also produce condensation rapidly, thus raising condensation effect.Containing more fine droplets in the gas of being discharged by dividing wall type condenser liquid outlet 9, finally discharged after the trapping of high efficiency demister 6 power by demister leakage fluid dram 10, remaining gas exports 12 by incoagulable gas and discharges.
Empirical tests, the reflux cycle system of the present invention by increasing, can lower 20-50% by the condensate concentration in the emission gases of existing condensing plant.Be particularly useful for the application scenario that in gas to be condensed, incoagulable gas content is greater than 20%.
The present invention will be described to enumerate specific embodiment below:
Embodiment 1: input is containing the condensation of cease of ethyl-acetate gas.The entrance concentration of ethyl acetate is that 540 ~ 1480g/m3, carrier gas is mainly nitrogen.Refrigerant is-5 DEG C of chilled waters, and when not adopting reflux, air exit concentration 198-208g/m3, after adopting reflux, in the reflux ratio situation of 10%, exhaust concentration 128-135g/m3, exhaust ethyl acetate mass flowrate obviously declines.
Embodiment 2: input is containing chloroform waste gas condensation.The entrance concentration of chloroform is that 2582g/m3, carrier gas is mainly nitrogen.Refrigerant is-10 DEG C, when not adopting reflux, and exhaust outlet concentration 936-971g/m3, after adopting retracting device, in the reflux ratio situation of 6%, exhaust concentration 698-712g/m3.
Embodiment 3: input is containing dimethylbenzene condensation of gas.The entrance concentration of dimethylbenzene is that 269g/m3, carrier gas is mainly nitrogen.Refrigerant is 4 DEG C, when not adopting reflux, exhaust outlet concentration 18-19g/m3, after adopting retracting device, in the reflux ratio situation of 10%, and exhaust concentration 12-13g/m3.
Advantage of the present invention is certain end face by the discharge portion of condensation process being looped back condensation process, and then contained in condensation exhaust particle provides steam condensing core as the seed that condensate liquid is formed, thus improves condensation efficiency.A part of gas is shunted from the afterbody of condensing unit, the front end of condensing unit and the gas and vapor permeation to be condensed being cooled to uniform temperature is back to by power set or airflow injection device, for it provides the nuclei of condensation improving condensation effect, high efficiency demister is set in the final outlet of condenser system simultaneously, fully reclaims the drop of condensation.
The above is only to better embodiment of the present invention, not any pro forma restriction is done to the present invention, every any simple modification done above embodiment according to technical spirit of the present invention, equivalent variations and modification, all belong in the scope of technical solution of the present invention.

Claims (3)

1. the device of a partial reflux circulation raising dividing wall type condenser condenses effect, it is characterized in that: comprise dividing wall type condenser (1), dividing wall type condenser (1) one end is provided with dividing wall type condenser inlet (2), the other end is provided with dividing wall type condenser-air outlet (3) of band reflux gas arm, dividing wall type condenser (1) body connects cooling media (4), cooling media (4) provides refrigerant to dividing wall type condenser (1), dividing wall type condenser-air with reflux gas arm exports (3) and connects reflux gas power set (5) and demister (6) respectively by pipeline, reflux gas power set (5) connect reflux gas entrance (7) by pipeline, reflux gas entrance (7) is positioned on dividing wall type condenser (1), make dividing wall type condenser (1) inside and export (3) with the dividing wall type condenser-air of band reflux gas arm, the pipeline that reflux gas entrance (7) connects forms a gas passage, reflux gas entrance (7) place is provided with adverse current blender (8), the bottom of dividing wall type condenser-air outlet (3) one end of the band reflux gas arm of dividing wall type condenser (1) is provided with dividing wall type condenser liquid outlet (9), demister (6) bottom is provided with demister leakage fluid dram (10), dividing wall type condenser liquid outlet (9) is connected total leakage fluid dram (11) with demister leakage fluid dram (10) by pipeline, demister (6) is provided with incoagulable gas outlet (12).
2. improve the device of dividing wall type condenser condenses effect according to partial reflux circulation a kind of described in claim 1, it is characterized in that: described reflux gas entrance (6) is positioned between the 10%-90% of the vapor path length of dividing wall type condenser (1).
3. improve the device of dividing wall type condenser condenses effect according to partial reflux circulation a kind of described in claim 1, it is characterized in that: the dividing wall type condenser-air of described band reflux gas arm exports the 1%-60% that the gas flow (3) refluxed is the gas gross to be condensed at dividing wall type condenser inlet (2) place.
CN201510092807.7A 2015-03-02 2015-03-02 A kind of partial reflux circulation improves the device of dividing wall type condenser condensation effect Active CN104729312B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111495102A (en) * 2020-05-07 2020-08-07 扬州市朝晖环境工程有限公司 Circulation type adjustable exhaust-gas treatment equipment
CN113418405A (en) * 2021-06-01 2021-09-21 中广核工程有限公司 Method and system for preventing nuclear power condenser from freezing

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4996106A (en) * 1972-12-22 1974-09-11
CN1352373A (en) * 2000-10-24 2002-06-05 三菱重工业株式会社 Condenser of refrigerator
CN1846826A (en) * 2006-04-06 2006-10-18 天津大学 Distillation condenser for high solidifying point material and its evaporation and condensation process
CN101050923A (en) * 2007-05-09 2007-10-10 云南云天化股份有限公司 Self cleaning method for condenser
CN203582809U (en) * 2013-11-14 2014-05-07 永胜县益农新能源开发有限公司 Condenser

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4996106A (en) * 1972-12-22 1974-09-11
CN1352373A (en) * 2000-10-24 2002-06-05 三菱重工业株式会社 Condenser of refrigerator
CN1846826A (en) * 2006-04-06 2006-10-18 天津大学 Distillation condenser for high solidifying point material and its evaporation and condensation process
CN101050923A (en) * 2007-05-09 2007-10-10 云南云天化股份有限公司 Self cleaning method for condenser
CN203582809U (en) * 2013-11-14 2014-05-07 永胜县益农新能源开发有限公司 Condenser

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111495102A (en) * 2020-05-07 2020-08-07 扬州市朝晖环境工程有限公司 Circulation type adjustable exhaust-gas treatment equipment
CN111495102B (en) * 2020-05-07 2022-04-05 扬州市朝晖环境工程有限公司 Circulation type adjustable exhaust-gas treatment equipment
CN113418405A (en) * 2021-06-01 2021-09-21 中广核工程有限公司 Method and system for preventing nuclear power condenser from freezing

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