CN104721398A - Traditional Chinese medicine compound tea tree essential oil - Google Patents
Traditional Chinese medicine compound tea tree essential oil Download PDFInfo
- Publication number
- CN104721398A CN104721398A CN201510159572.9A CN201510159572A CN104721398A CN 104721398 A CN104721398 A CN 104721398A CN 201510159572 A CN201510159572 A CN 201510159572A CN 104721398 A CN104721398 A CN 104721398A
- Authority
- CN
- China
- Prior art keywords
- tea tree
- oil
- parts
- tree ethereal
- essential oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses traditional Chinese medicine compound tea tree essential oil. The traditional Chinese medicine compound tea tree essential oil is characterized by being prepared from the following medicinal raw materials in parts by weight: 9-16 parts of wild chrysanthemum flower, 5-10 parts of fructus forsythiae, 6-12 parts of Chinese angelica, 8-16 parts of schizonepeta, 9-15 parts of Chinese tallow tree seeds, 4-9 parts of croton, 6-12 parts of garter snake, 1.1-1.5 parts of lemon essential oil, 1.3-1.7 parts of lavender essential oil, 5.3-7.5 parts of armeniaca dulcis oil, and 1.2-1.6 parts of tea tree essential oil. The traditional Chinese medicine compound tea tree essential oil disclosed by the invention also has the good effects as follows: natural extracted essential oil is used as the raw material; the traditional Chinese medicine compound tea tree essential oil is free from toxic and stimulating substances; after being used, the traditional Chinese medicine compound tea tree essential oil is free from side effect to a human body, safe and effective; the traditional Chinese medicine compound tea tree essential oil has the effect of treating acne by adjusting mitosis of surface cells and prompting epidermal cells to update; and simultaneously, the traditional Chinese medicine compound tea tree essential oil is also capable of inhibiting melanocyte and has the bactericidal activity.
Description
Technical field
The present invention relates to a kind of compound essential Oil, particularly relate to a kind of Chinese crude drug compound recipe tea tree ethereal oil.
Background technology
Comedo, medical name is acne, is a kind of common chronic inflammation hair follicle sebum gland disease, and be one of common disease of department of dermatologry, the non-inflammation skin lesion of acne shows as opening and closed comedones.The typical skin lesion of closed comedones is the colour of skin pimple of about 1 mm in size, without obvious hair follicle opening.Open comedones (also known as blackhead) shows as the hair follicle opening that dome-shaped pimple companion significantly expands.Acne further develop and can develop into various struvite skin lesion, show as inflamed papules, pustule, tuberosity and cyst.Inflamed papules takes on a red color, and diameter 1 ~ 5 millimeter is not etc.; Pustule is in the same size, is wherein filled with white pus; Tuberosity diameter is greater than 5 millimeters, and that touches has scleroma and pain; The position of cyst is darker, is filled with the mixture of pus and blood.These skin lesion also can merge and form large inflammatory speckle and sinus tract etc.Pigmentation, erythema perstans, pitting or hypertrophic cicatrix is usually left over after struvite skin lesion disappears.Be apt to occur in the position that face, the back of the body, breast etc. are rich in sebaceous gland.Be more common in that female of adolescence, have the middle school student of research display nearly 65% to suffer from acne, sickness rate is higher, it is the common facial skin disease of adolescence, if it is improper to treat not in time or prevent and treat, pigmentation even cicatrix can be formed, affect patient's appearance, mental health and quality of life.
Acne belongs in Chinese medicine " rosacea caused by lung-wind " category.Traditional Chinese medical science ancient literature is more about the discussion of primary disease, and Wang Bing is in Plain Questions of Huangdi's Internal Classic annotation Zhong Geng road: " time the moon cold and cool, shape labor sweating; chilly wind is outer thin, the flesh natural fibre line of meat occupies cold, and fat liquid coagulates then; store in Xuan Fu, oozes dry up according to sky, and Zha thorn is longer than in skin; shape is as rice, or as pin, person of a specified duration is upper black; long one point, remaining color Herba Solani Lyrati and thin in profound mansion, and custom says acne; induce sweat, and Xuan Fu meaning antiperspirant sky is also.Cuo, meaning red complexion, accumulates blood pus in fat anger, shape is little and large, as acid thorn Fructus Jujubae, or as by (doubtful " pea ") bean, this all stagnation of YANG QI in the interior to do ， Dai Pliable and attack it, greatly very go out it." this and modern dermatological discuss acne and adolescence androgen increases; sebaceous gland increases sebum secretion and increases; make hair follicle, sebaceous gland duct hyperkeratosis simultaneously; the sebum stasis of blood is amassed and formed fat bolt in hair follicle; simultaneously; sebum is divided Sui by the corynebacterium acnes existed in hair follicle, generates free fatty.The latter's hair follicle stimulating causes inflammation, and causes follicular wall lesion ruptures, and hair follicle content enters corium, thus causes the inflammatory reaction of perifollicolar varying degree, suppurates and forms the pathogenic factor of abscess and pathogenesis is perfectly in harmony.In summary, modern dermatological opinion acne, be increase with androgen, sebum increases, arrange the pathogenesis that fat is obstructed, bacteriological infection is axle center, TCM acne then with phase heated very, stagnation of YANG QI in the interior, burn that Tianjin is expectorant, the stagnation of phlegm-heat pathogenesis that is axle center.For this pathogenesis, its treatment should with clearing ministerial fire, and clearing away heat and eliminating phlegm is principle.
Application publication number CN 104398782 A(application number 201410436147.5) Chinese invention patent document disclose a kind of Chinese medicine for the treatment of comedo, be made up of following component weight: Radix Et Rhizoma Rhei 20g, Radix Angelicae Sinensis 35g, Rhizoma Cimicifugae 40g, Cortex Lycii 50g, Cortex Moutan 30g, Rhizoma Alismatis 50g, Flos Chrysanthemi Indici 50g, Flos Lonicerae 25g and Radix Ophiopogonis 50g.Application publication number CN 103446014 A(application number 201310369914.0) Chinese invention patent document disclose a kind of quintessence oil of effective removal comedo, formed by the preparation of raw material of following weight portion: Salvia japonica Thunb. 2-4 part, Flos Caryophylli 1-2 part, lavandula angustifolia 1-2 part, Flos Pelargonii 1-2 part, Fructus Citri Limoniae 2-3 part, Camellia sinensis 1-2 part, Lignum cinnamomi camphorae 1-2 part, base oil 10-16 part.Application publication number CN 103893059 A(application number 201410065181.6) Chinese invention patent document disclose a kind of pore cleanser preparation, match well than forming by following composition according to certain mass: the medicinal Flos Rosae Rugosae of 30-45 part, the Pericarpium Citri junoris of 12-17 part, the glycerol stearate of 10-15 part, the betanin of 4-8 part, the sea salt of 9-16 part, the Aloe of 1-5 part, the Herba Lysimachiae foenum-graeci quintessence oil of 0.5-1.5 part, the water of 100-150 part.
At present, the chemical composition adding hormones in the product of western medicine acne or skin and health are harmful to, although the effect of fast treating can be reached, but very large infringement is caused to patient skin and health, accelerates the aging, downright bad of patient skin or produce spot, even forming drug resistance, and most drug treatment is not thorough, recurrent exerbation, even cannot cure, and causes great misery to all one's life of patient.Chinese medicine has certain advantage in Acne treatment, and toxic and side effects is little, does not recur more, is subject to the high praise of people, but the course for the treatment of is longer, and curative effect is not obvious.Therefore containing malicious stimulating component and curative effect, product is not imperative rapidly to develop one.
Summary of the invention
For the deficiencies in the prior art, the object of this invention is to provide one prepare simple, easy to use, the property of medicine is gentle does not stimulate, action effect is Chinese crude drug compound recipe tea tree ethereal oil rapidly.This quintessence oil Be very effective, safety have no side effect.
Technical scheme of the present invention is:
A kind of Chinese crude drug compound recipe tea tree ethereal oil, is characterized in that, be prepared from by following bulk drugs, be weight portion: Flos Chrysanthemi Indici 9-16; Fructus Forsythiae 5-10; Radix Angelicae Sinensis 6-12; Herba Schizonepetae 8-16; Chinese tallow seed 9-15; Fructus Crotonis 4-9; Zaocys 6-12; Fructus Citri Limoniae quintessence oil 1.1-1.5; Herba Lysimachiae foenum-graeci quintessence oil 1.3-1.7; Semen pruni armeniacae oil 5.3-7.5; Tea tree ethereal oil 1.2-1.6.
In preferred scheme, Flos Chrysanthemi Indici 11-14; Fructus Forsythiae 6-9; Radix Angelicae Sinensis 8-10; Herba Schizonepetae 10-14; Chinese tallow seed 11-13; Fructus Crotonis 6-7; Zaocys 8-10; Fructus Citri Limoniae quintessence oil 1.2-1.4; Herba Lysimachiae foenum-graeci quintessence oil 1.4-1.6; Semen pruni armeniacae oil 5.8-7.0; Tea tree ethereal oil 1.3-1.5.
Be more preferably, Flos Chrysanthemi Indici 12.5; Fructus Forsythiae 7.5; Radix Angelicae Sinensis 9; Herba Schizonepetae 12; Chinese tallow seed 12; Fructus Crotonis 6.5; Zaocys 9; Fructus Citri Limoniae quintessence oil 1.3; Herba Lysimachiae foenum-graeci quintessence oil 1.5; Semen pruni armeniacae oil 6.4; Tea tree ethereal oil 1.4.
A kind of Chinese crude drug compound recipe tea tree ethereal oil, preparation method is as follows:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, sieve, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 1-2 hour, and second time extracts 40-60 minute, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through microporous filter membrane filtration, add Fructus Citri Limoniae quintessence oil, real Herba Lysimachiae foenum-graeci quintessence oil, Semen pruni armeniacae oil and tea tree ethereal oil while stirring, then add emulsifying agent, stir, sterilizing, encapsulation, to obtain final product.
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil, preferred scheme is, the middle 40-80 mesh sieve excessively of step (2) (preferred 50-70 mesh sieve excessively, mistake 60 mesh sieve be more preferably).
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil, preferred scheme is, in step (3), first time extracts 1.3-1.7 hour (preferably first time extracts 1.5 hours).
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil, preferred scheme is, in step (3), second time is extracted 45-55 minute (preferably second time is extracted 50 minutes).
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil, preferred scheme is, through 0.6-2.0 μm of microporous filter membrane filtration (preferably through 1.0-1.6 μm of microporous filter membrane filtration, be more preferably through 1.3 μm of microporous filter membrane filtrations) in step (4).
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil, preferred scheme is, adds the emulsifying agent (preferably adding the emulsifying agent of 0.3-0.5 times amount, the emulsifying agent adding 0.4 times amount be more preferably) of 0.2-0.6 times amount in step (4).
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil, preferred scheme is, in step (4), added emulsifying agent is polyglycerol stearate.
A kind of Chinese crude drug compound recipe of gained of the present invention tea tree ethereal oil scientific formula, easy to use, be easy to carry.In addition, excellent results of the present invention also shows:
1,the present invention adopts natural extraction quintessence oil to be raw material, not containing malicious pungent, can not have side effects after using to human body, safe and effective;
2,the present invention, by regulating the mitosis of superficial cell and promoting that epidermis cell upgrades, plays the effect of Acne treatment; Also have simultaneously and suppress melanocyte and bactericidal activity;
3,can not produce other dangerous chemicals after quintessence oil mixing contained by the present invention, fragrance is clearly insulted ice-cold, simultaneously and Chinese medicine ingredients generation synergism, reaches good therapeutic effect, and non-relapse after healing.
Effect of the present invention's primary raw material used is as follows:
Flos Chrysanthemi Indici: base is former: be root or the herb of Compositae Dendranthema Flos Chrysanthemi Indici or lavandulaleaf dendranthema herb.The property of medicine: bitter, acrid, cold.Return liver, heart channel.Function cures mainly: heat-clearing and toxic substances removing, improving eyesight.Cure mainly flu, dysentery, carbuncle, furuncle, conjunctival congestion and swelling pain, dizzy, scrofula, eczema.
Fructus Forsythiae: base is former: this product is the dry fruit of Oleaceae plants Fructus Forsythiae.Character: this product is in long avette to avette, slightly flat.There is the fleck of irregular vertical wrinkle and most projection on surface, and respectively there is 1 obvious longitudinal furrow on two sides.The sharp point in top.Nature and flavor: bitter, are slightly cold.Gui Jing: return lung, the heart, small intestine meridian.Effect: heat-clearing and toxic substances removing, dispersing swelling and dissipating binds.Cure mainly: for carbuncle, scrofula, acute mastitis, erysipelas, anemopyretic cold, epidemic febrile disease from the beginning of, warmly join the army, high hot excessive thirst, coma sends out speckle, pyretic stranguria urine retention.
Radix Angelicae Sinensis: base is former: this product is the dry root of umbelliferae angelica.Chemical analysis: root is containing volatile oil, and Minxian County, Gansu product person contains 0.7% containing 0.4%, Si Chuanwen county product person.Volatilization main body of oil has: butylidenephthalide, the positive pentanone of adjacent carboxyl benzene and Δ 2,4-dihydro acid phthalic anhydride.Nature and flavor: sweet, acrid, warm.Gui Jing: return liver, the heart, spleen channel.Effect: enrich blood and invigorate blood circulation, menstruction regulating and pain relieving, loosening bowel to relieve constipation.Cure mainly: for blood deficiency and yellow complexion, dizzy cardiopalmus, menoxenia, amenorrhea dysmenorrhea, asthenia cold abdominalgia, dryness of the intestine constipation, rheumatic arthralgia, injury from falling down, ulcer sores.Radix Angelicae Sinensis (processed with wine) promoting blood circulation to restore menstrual flow.For amenorrhea dysmenorrhea, rheumatic arthralgia, injury from falling down.
Herba Schizonepetae: base is former: be the herb of labiate Herba Schizonepetae.Chemical analysis: containing volatile oil 1.8%, in oil, main constituent is D-menthone, racemization book lotus ketone, a small amount of d-limonen.Pharmacological action: with the rabbit of artificial fever, oral Herba Schizonepetae decoct and preserved material 2 grams (crude drug)/kilogram, nothing very refrigeration function.In vitro, high concentration (1:100) has the effect of anti-mycobacterium tuberculosis.Nature and flavor: pungent, temperature.Gui Jing: enter lung, Liver Channel.Function cures mainly: deliver, and dispels the wind, treating blood disorders; Parch to black stops blooding.Cure cold heating, headache, laryngopharynx swelling and pain, apoplexy locked mouth, and spit blood, epistaxis, has blood in stool; Metrorrhagia, puerperal blood faints; Carbuncle, skin ulcer scabies, scrofula.Herba Schizonepetae effectiveness is identical, and the power of only dispersing is stronger.
Chinese tallow seed: base is former: be the seed of euphorbia plant Cortex Sapii Radicis.Nature and flavor: sweet are cool, poisonous.Function cures mainly: parasite killing, diuretic, relieving constipation.Control scabies, eczema, chapped skin, edema.Constipation.
Fructus Crotonis: base is former: be the seed of euphorbia plant Fructus Crotonis.Chemical analysis: containing Oleum Tiglii, wherein has the glyceride of oleic acid, linoleic acid, crotonic acid, tiglic acid etc.; Still containing crotonoside.Nature and flavor: pungent, heat, poisonous.Gui Jing: enter stomach, large intestine channel.Function cures mainly: rush down cold long-pending, orifice opening, by expectorant, and row water, parasite killing.Control cold long-pending sluggish, distension and fullness of the chest and abdomen shoot, abdominal mass due to blood stasis, accumulation of phlegm in the hypochondrium, dysentery, edema, acute throat trouble is controlled in external, sore throat, malignant boil scabies.
Zaocys: base is former: be the entirety of Colubridae animal Zaocys removing internal organs.Nature and flavor: Gan Xian are flat.Gui Jing: " Thunder God concocts property of medicine solution ": " enter lung, spleen two warp." function cures mainly: wind-damp dispelling, the meridian dredging.Dispelling the wind and dampness pathogens insensitive impediment, numbness of the skin, bone, tuberculosis of joint, rubella scabies, leprosy, tetanus, poliomyelitis.
Fructus Citri Limoniae quintessence oil: main component: limonene, citral, (Niu Biao) gemic acid, citronella oil, lauro lene.Fructus Citri Limoniae quintessence oil can improve circulatory function, comprises blood circulation promoting, to reduce blood pressure, and only nose bleeding.It can strengthen immune system, and purification health, improves digestive system function, the group of reducing fat, treatment dyspepsia and constipation.Fructus Citri Limoniae quintessence oil has consoling and alleviates the effect of headache and migraine, by the acidic materials in general physical, to treatment of arthritis and rheumatism also helpful.Also contribute to clean acne, clean Greasy Skin and hair, and remove dead skin cells.In the hot water of foot bath, instill several Fructus Citri Limoniae quintessence oil, the object of meridians of invigorating blood circulation can be reached, the effect removing beriberi foot odor can also be reached.Physiology curative effect: the excellent tonic of blood circulation, makes unblocked blood flowing, alleviates the pressure at varicosis position; Erythrocytic vigor Fructus Citri Limoniae can be recovered, alleviate the phenomenon of anemia, stimulate leukocyte simultaneously, help the communicable disease of body resistance; The function of facilitating digestion system.Stimulate leukocyte, to all kinds of knife injury or wound all applicable, hemostasis, helps wound healing, adjusts along whole digestive system, has certain curative effect to gastropathy, gastric ulcer etc.Conditioning blood circulation, is particularly suitable for treating varicosis, is also suitable for, preventing cold, brings down a fever, slow down skin aging, help digest, mosquito proof is bitten hypertension, various focusing depths represented, oral ulcer.Psychological effect: when feeling hot agitation, can bring pure and fresh impression, helps the clarification state of mind.
Real Herba Lysimachiae foenum-graeci quintessence oil: be refined by lavandula angustifolia to form, can heat-clearing and toxic substances removing, and cleaning skin, controls oil content, freckle removing and whitening, wrinkle removal skin care, eye haustra-dsipelling black eye, also can promote that damaged tissues regenerates skin-protecting function such as recoverys grade.It can purify, pacify soul, alleviate indignation and used-up sensation, make people can even-tempered and good-humouredly in the face of live.There is sedation effect to heart, hypertension can be reduced, pacify cardiopalmus, helpful for insomnia.
Semen pruni armeniacae oil: composition: vitamin A, B1, B2, B6, E, protein, fatty acid.Effect: 1, easily absorb, containing enriching vitamin, having the magical effect of nourishing with moisturizing, releiving and antianaphylactic effect.2, Semen pruni armeniacae oil can make skin recover smooth soft and fine, if life-time service can eliminate striae gravidarum effectively.3, being effective softening agent, having obvious effect to skin, is the splendid vegetable oil of a kind of skin care and moisturizing effect.4, for the myalgia that hyperkinesia causes, can strengthen cell band oxygen function, allaying tiredness and carbonic acid are accumulated, and have analgesia and abirritant effect.The hypophysis of hormonal system, thymus and adrenal gland can be stimulated, promote cell turnover.
Tea tree ethereal oil: tea tree ethereal oil originates in Australia is the extract of Camellia sinensis.Abnormal smells from the patient: approximate eucalyptus globolus, fresh, slightly pungent wooden class aromatic, has dense flavour of a drug, fresh, pure and fresh, slightly pungent.Volatility: fast.Composition: topmost chemical composition is ethylene, dipentene, limonene, cineol, Oleum sesami brain, anisoxide.Function: 1, psychological effect: make brains pure and fresh, rejuvenate, be particularly useful for frightened situation.2, health curative effect: the most important purposes of Camellia sinensis helps the communicable disease of immune system fight, and instigate leukocyte and form guard wire, to meet head on the organism of invasion, and can shorten the time of falling ill, be potent antibiotic essential oil.3, skin curative effect: clean-up effect is excellent, improves the suppuration phenomenon of wound infection, and furuncle.Remove small pox and unclean position caused by chickenpox and herpes zoster.Can be applicable to burn, skin ulcer, sunburn, tinea, wart, tinea circinata, herpes and tinea pedis.Also scalp overdrying and the dandruff can be treated.4, sterilize master-hand: 5 folk prescription tea tree ethereal oil champignons, with the antibacterial in purifying air, viral expelling mosquito.5, other effects: tea tree ethereal oil effect has bactericidal antiphlogistic, convergence pore, treatment Common Cold, cough, rhinitis, asthma, improve dysmenorrhea, menoxenia and genital infection.Be applicable to oiliness and acne-prone skin, treatment suppurative wound and burn, tan severely, tinea pedis and dandruff.Clear the head, rejuvenate, anti-dejected.6, beauty functions: the research through expert finds, tea tree ethereal oil utilizes the effect of its anti-inflammation, effectively can resist the small pox that propionibacterium acnes causes.
Detailed description of the invention
Describe technical scheme of the present invention in detail below in conjunction with embodiment and experimental example, but protection domain is not limited thereto.
embodiment 1a kind of Chinese crude drug compound recipe tea tree ethereal oil, is prepared from by following bulk drugs, is weight portion (55g/ part): Flos Chrysanthemi Indici 9 parts; Fructus Forsythiae 5 parts; Radix Angelicae Sinensis 6 parts; Herba Schizonepetae 8 parts; Chinese tallow seed 9 parts; Fructus Crotonis 4 parts; Zaocys 6 parts; Fructus Citri Limoniae quintessence oil 1.1 parts; Real Herba Lysimachiae foenum-graeci quintessence oil 1.3 parts; Semen pruni armeniacae oil 5.3 parts; Tea tree ethereal oil 1.2 parts.
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil is:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, cross 40 mesh sieves, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 1 hour, and second time is extracted 40 minutes, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through 0.6 μm of microporous filter membrane filtration, add Fructus Citri Limoniae quintessence oil (commercial city, Guangzhou glad phyllody cosmetic company limited while stirring, model: 56ML-topgel-no cleaning, 50mL/ bottle), real Herba Lysimachiae foenum-graeci quintessence oil (Jishui County, Jiangxi Province Yikang natural perfume material oil refinery, specification: 30mL/ bottle), Semen pruni armeniacae oil (Guangzhou Peng Yuan Chemical Co., Ltd., 50mL/ bottle) and tea tree ethereal oil (the organic unlimited trade Co., Ltd in Shenzhen, specification: 50mL/ bottle), then the emulsifier polyglycerol stearate of 0.2 times amount is added, stir, sterilizing, encapsulation, obtain.
The using method of compound recipe tea tree ethereal oil of the present invention is: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.
embodiment 2a kind of Chinese crude drug compound recipe tea tree ethereal oil, is prepared from by following bulk drugs, is weight portion (35g/ part): Flos Chrysanthemi Indici 16 parts; Fructus Forsythiae 10 parts; Radix Angelicae Sinensis 12 parts; Herba Schizonepetae 16 parts; Chinese tallow seed 15 parts; Fructus Crotonis 9 parts; Zaocys 12 parts; Fructus Citri Limoniae quintessence oil 1.5 parts; Real Herba Lysimachiae foenum-graeci quintessence oil 1.7 parts; Semen pruni armeniacae oil 7.5 parts; Tea tree ethereal oil 1.6 parts.
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil is:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, cross 80 mesh sieves, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 2 hours, and second time is extracted 60 minutes, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through 2.0 μm of microporous filter membrane filtrations, add Fructus Citri Limoniae quintessence oil (commercial city, Guangzhou glad phyllody cosmetic company limited while stirring, model: 56ML-topgel-no cleaning, 50mL/ bottle), real Herba Lysimachiae foenum-graeci quintessence oil (Jishui County, Jiangxi Province Yikang natural perfume material oil refinery, specification: 30mL/ bottle), Semen pruni armeniacae oil (Guangzhou Peng Yuan Chemical Co., Ltd., 50mL/ bottle) and tea tree ethereal oil (the organic unlimited trade Co., Ltd in Shenzhen, specification: 50mL/ bottle), then the emulsifier polyglycerol stearate of 0.6 times amount is added, stir, sterilizing, encapsulation, obtain.
The using method of compound recipe tea tree ethereal oil of the present invention is: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.
Model case: Song XX, female, 19 years old, student.Patient is to our hospital on July 12nd, 2010.Patient's readme: the year before two cheek starts to occur comedo, because the psychology of liking to be beautiful, patient is automatic extruding small pox usually, cause exacerbation of symptoms, buccal is red and swollen, treats afterwards in section hospital, after treating half a year, the state of an illness slightly controls, but buccal occurs a large amount of acne, pimple.Patient is very worried.Classmate introduced my institute and checked treatment afterwards.Check: patient's yellow complexion is dark red, buccal, forehead, a large amount of acne in chin position, pimple, pustule, tuberosity, and color is dark red, exceeds skin, the tenderness touched, pothole cicatrix is obvious; Red tongue, thin fur is few, thready and weak pulse number.Be diagnosed as: acne.
Use a kind of Chinese crude drug compound recipe of the present embodiment gained tea tree ethereal oil, using method: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.After using two courses for the treatment of, patient's yellow complexion secretly disappears thin out, and acne color turns light red, and protrusion pimple, tuberosity disappear substantially; Continue two courses for the treatment of of medication, patient's face is smooth, and the colour of skin is bright in vain, and acne all disappears, and tongue fur turns thick, arteries and veins comparatively before effectively roomy.Follow up a case by regular visits to so far without recurrence.
embodiment 3a kind of Chinese crude drug compound recipe tea tree ethereal oil, is prepared from by following bulk drugs, is weight portion (50g/ part): Flos Chrysanthemi Indici 11 parts; Fructus Forsythiae 6 parts; Radix Angelicae Sinensis 8 parts; Herba Schizonepetae 10 parts; Chinese tallow seed 11 parts; Fructus Crotonis 6 parts; Zaocys 8 parts; Fructus Citri Limoniae quintessence oil 1.2 parts; Real Herba Lysimachiae foenum-graeci quintessence oil 1.4 parts; Semen pruni armeniacae oil 5.8 parts; Tea tree ethereal oil 1.3 parts.
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil is:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, cross 50 mesh sieves, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 1.3 hours, and second time is extracted 45 minutes, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through 1.0 μm of microporous filter membrane filtrations, add Fructus Citri Limoniae quintessence oil (commercial city, Guangzhou glad phyllody cosmetic company limited while stirring, model: 56ML-topgel-no cleaning, 50mL/ bottle), real Herba Lysimachiae foenum-graeci quintessence oil (Jishui County, Jiangxi Province Yikang natural perfume material oil refinery, specification: 30mL/ bottle), Semen pruni armeniacae oil (Guangzhou Peng Yuan Chemical Co., Ltd., 50mL/ bottle) and tea tree ethereal oil (the organic unlimited trade Co., Ltd in Shenzhen, specification: 50mL/ bottle), then the emulsifier polyglycerol stearate of 0.3 times amount is added, stir, sterilizing, encapsulation, obtain.
The using method of compound recipe tea tree ethereal oil of the present invention is: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.
embodiment 4a kind of Chinese crude drug compound recipe tea tree ethereal oil, is prepared from by following bulk drugs, is weight portion (40g/ part): Flos Chrysanthemi Indici 14 parts; Fructus Forsythiae 9 parts; Radix Angelicae Sinensis 10 parts; Herba Schizonepetae 14 parts; Chinese tallow seed 13 parts; Fructus Crotonis 7 parts; Zaocys 10 parts; Fructus Citri Limoniae quintessence oil 1.4 parts; Real Herba Lysimachiae foenum-graeci quintessence oil 1.6 parts; Semen pruni armeniacae oil 7.0 parts; Tea tree ethereal oil 1.5 parts.
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil is:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, cross 70 mesh sieves, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 1.7 hours, and second time is extracted 55 minutes, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through 1.6 μm of microporous filter membrane filtrations, add Fructus Citri Limoniae quintessence oil (commercial city, Guangzhou glad phyllody cosmetic company limited while stirring, model: 56ML-topgel-no cleaning, 50mL/ bottle), real Herba Lysimachiae foenum-graeci quintessence oil (Jishui County, Jiangxi Province Yikang natural perfume material oil refinery, specification: 30mL/ bottle), Semen pruni armeniacae oil (Guangzhou Peng Yuan Chemical Co., Ltd., 50mL/ bottle) and tea tree ethereal oil (the organic unlimited trade Co., Ltd in Shenzhen, specification: 50mL/ bottle), then the emulsifier polyglycerol stearate of 0.5 times amount is added, stir, sterilizing, encapsulation, obtain.
The using method of compound recipe tea tree ethereal oil of the present invention is: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.
Model case a: XX, man, 18 years old.On June 10th, 2011 is to our hospital.Patient's readme: occur comedo (acne) the year before, has just started to occur on back, and Head And Face is little, and half a year, back part comedo disappeared, and face starts to occur, does not treat, and use anti-acne facial milk cleanser to wash one's face, symptom is unchanged always.Before one week, patient has eaten a large amount of pungent irritable food, and cause acne to increase the weight of, buccal is micro-red, the pain touched, and comes my institute upon somebody's introduction and checks treatment.Check: acne is attached most importance to bilateral buccal and side volume, and color is red, micro-protuberance, and mouth Zhou Wei has burn feeling, feel xerocheilia, thirsty, drinking-water is few.Red tongue, thin fur hundred and lacking, while there is indentation, floating pulse.
Use a kind of Chinese crude drug compound recipe of the present embodiment gained tea tree ethereal oil, using method: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.After using two courses for the treatment of, patient's yellow complexion secretly disappears thin out, and acne color turns light red, then disappears gradually; Continue two courses for the treatment of of medication, patient's face is smooth, and the colour of skin is bright in vain, and acne all disappears, and tongue fur turns thick, arteries and veins comparatively before effectively roomy.Follow up a case by regular visits to so far without recurrence.
embodiment 5a kind of Chinese crude drug compound recipe tea tree ethereal oil, is prepared from by following bulk drugs, is weight portion (45g/ part): Flos Chrysanthemi Indici 12.5 parts; Fructus Forsythiae 7.5 parts; Radix Angelicae Sinensis 9 parts; Herba Schizonepetae 12 parts; Chinese tallow seed 12 parts; Fructus Crotonis 6.5 parts; Zaocys 9 parts; Fructus Citri Limoniae quintessence oil 1.3 parts; Real Herba Lysimachiae foenum-graeci quintessence oil 1.5 parts; Semen pruni armeniacae oil 6.4 parts; Tea tree ethereal oil 1.4 parts.
The preparation method of above-mentioned a kind of Chinese crude drug compound recipe tea tree ethereal oil is:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, cross 60 mesh sieves, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 1.5 hours, and second time is extracted 50 minutes, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through 1.3 μm of microporous filter membrane filtrations, add Fructus Citri Limoniae quintessence oil (commercial city, Guangzhou glad phyllody cosmetic company limited while stirring, model: 56ML-topgel-no cleaning, 50mL/ bottle), real Herba Lysimachiae foenum-graeci quintessence oil (Jishui County, Jiangxi Province Yikang natural perfume material oil refinery, specification: 30mL/ bottle), Semen pruni armeniacae oil (Guangzhou Peng Yuan Chemical Co., Ltd., 50mL/ bottle) and tea tree ethereal oil (the organic unlimited trade Co., Ltd in Shenzhen, specification: 50mL/ bottle), then the emulsifier polyglycerol stearate of 0.4 times amount is added, stir, sterilizing, encapsulation, obtain.
The using method of compound recipe tea tree ethereal oil of the present invention is: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.
test example 1the clinical practice of a kind of Chinese crude drug compound recipe tea tree ethereal oil (embodiment 5) of gained of the present invention:
1.1 physical data
In November ,-2013 in March, 2010, choose experimenter's totally 326 examples of voluntary participation test, wherein male 160 example, women 166 example.Age in 16-32 year, 23 years old mean age.
1.2 Therapeutic Method
All experimenters are divided into experimental group and matched group at random.Two groups of personnel are at the age, and the aspects such as sex, through statistical procedures no significant difference (P > 0.05), have comparability.Wherein experimental group uses a kind of Chinese crude drug compound recipe of gained of the present invention tea tree ethereal oil, using method: get appropriate this product and be applied to affected part, every day three times, 7 days courses for the treatment of.Matched group uses other medicines (as conventional medication such as clear pox element, acne ointment and acne ointments).Observe three courses for the treatment of of treatment altogether.
1.3 curative effect judgment criteria
Cure: comedo or blackhead all disappear, and skin becomes smooth, fine and smooth; Effective: comedo obviously disappears, pore shrinks, and blackhead part is eliminated; Invalid: after using, symptom is without significant change.(total effective rate=cure rate+obvious effective rate)
1.4 experimental result
Result is as shown in table 1:
Table 1: the observed and recorded result of experimental group and matched group personnel
Test results: cure 155 examples (70.4%), effective 62 examples (28.2%), invalid 3 examples (1.4%), total effective rate is 98.6%, and treatment group successful is better than matched group.
The present invention by Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed, Fructus Crotonis and Zaocys totally 7 kinds of Chinese herbal medicine and Fructus Citri Limoniae quintessence oil, real Herba Lysimachiae foenum-graeci quintessence oil, Semen pruni armeniacae oil and tea tree ethereal oil totally 4 kinds of pure plant extract quintessence oils adopt the processing method of science formulated.All medicines share, and have effect of antibacterial, antiinflammatory, elimination pox print and blackhead.Experiment shows that products obtained therefrom total effective rate of the present invention is 98.6%, and successful is better than matched group.
It should be pointed out that detailed description of the invention is the more representational example of the present invention, obvious technical scheme of the present invention is not limited to above-described embodiment, can also have a lot of distortion.Those of ordinary skill in the art, with the present invention clear and definite disclosed or according to undoubted the obtaining of the written description of file, the claimed scope of this patent all should be thought.
Claims (10)
1. a Chinese crude drug compound recipe tea tree ethereal oil, is characterized in that, is prepared from by following bulk drugs, is weight portion: Flos Chrysanthemi Indici 9-16; Fructus Forsythiae 5-10; Radix Angelicae Sinensis 6-12; Herba Schizonepetae 8-16; Chinese tallow seed 9-15; Fructus Crotonis 4-9; Zaocys 6-12; Fructus Citri Limoniae quintessence oil 1.1-1.5; Real Herba Lysimachiae foenum-graeci quintessence oil 1.3-1.7; Semen pruni armeniacae oil 5.3-7.5; Tea tree ethereal oil 1.2-1.6.
2. a kind of Chinese crude drug compound recipe tea tree ethereal oil as claimed in claim 1, is characterized in that, be prepared from by following bulk drugs, be weight portion: Flos Chrysanthemi Indici 11-14; Fructus Forsythiae 6-9; Radix Angelicae Sinensis 8-10; Herba Schizonepetae 10-14; Chinese tallow seed 11-13; Fructus Crotonis 6-7; Zaocys 8-10; Fructus Citri Limoniae quintessence oil 1.2-1.4; Real Herba Lysimachiae foenum-graeci quintessence oil 1.4-1.6; Semen pruni armeniacae oil 5.8-7.0; Tea tree ethereal oil 1.3-1.5.
3. a kind of Chinese crude drug compound recipe tea tree ethereal oil as claimed in claim 1, is characterized in that, be prepared from by following bulk drugs, be weight portion: Flos Chrysanthemi Indici 12.5; Fructus Forsythiae 7.5; Radix Angelicae Sinensis 9; Herba Schizonepetae 12; Chinese tallow seed 12; Fructus Crotonis 6.5; Zaocys 9; Fructus Citri Limoniae quintessence oil 1.3; Real Herba Lysimachiae foenum-graeci quintessence oil 1.5; Semen pruni armeniacae oil 6.4; Tea tree ethereal oil 1.4.
4. a kind of Chinese crude drug compound recipe tea tree ethereal oil as described in as arbitrary in claim 1-3, it is characterized in that, preparation method is as follows:
(1) get clean Zaocys yellow wine to soak, take out, put on wire gauze, the roasting heat of slow fire, treats that Serpentis body is buff, has crisp fragrance taste, and discharging the retained water is easily broken is degree, and let cool, levigation is for subsequent use;
(2) Flos Chrysanthemi Indici, Fructus Forsythiae, Radix Angelicae Sinensis, Herba Schizonepetae, Chinese tallow seed fully be dry, pulverize into fine powder with Fructus Crotonis, mix with step (1) gained fine powder, sieve, obtain mixing fine powders for subsequent use;
(3) by step (2) gained mixing fine powders, be placed in Chinese medicament extracting device, add the dehydrated alcohol reflux, extract, twice of 5 times amount, first time extracts 1-2 hour, and second time extracts 40-60 minute, merge extractive liquid, filter, concentrating under reduced pressure obtains pale yellowish oil thick liquid, for subsequent use;
(4) by above-mentioned oily liquids through microporous filter membrane filtration, add Fructus Citri Limoniae quintessence oil, real Herba Lysimachiae foenum-graeci quintessence oil, Semen pruni armeniacae oil and tea tree ethereal oil while stirring, then add emulsifying agent, stir, sterilizing, encapsulation, to obtain final product.
5. the preparation method of a kind of Chinese crude drug compound recipe tea tree ethereal oil according to claim 4, is characterized in that, crosses 40-80 mesh sieve (preferred cross 50-70 mesh sieve, mistake 60 mesh sieve be more preferably) in step (2).
6. the preparation method of a kind of Chinese crude drug compound recipe tea tree ethereal oil according to claim 4, is characterized in that, in step (3), first time extracts 1.3-1.7 hour (preferably first time extracts 1.5 hours).
7. the preparation method of a kind of Chinese crude drug compound recipe tea tree ethereal oil according to claim 4, is characterized in that, in step (3), second time is extracted 45-55 minute (preferably second time is extracted 50 minutes).
8. the preparation method of a kind of Chinese crude drug compound recipe tea tree ethereal oil according to claim 4, it is characterized in that, through 0.6-2.0 μm of microporous filter membrane filtration (preferably through 1.0-1.6 μm of microporous filter membrane filtration, be more preferably through 1.3 μm of microporous filter membrane filtrations) in step (4).
9. the preparation method of a kind of Chinese crude drug compound recipe tea tree ethereal oil according to claim 4, it is characterized in that, the emulsifying agent (preferably adding the emulsifying agent of 0.3-0.5 times amount, the emulsifying agent adding 0.4 times amount be more preferably) of 0.2-0.6 times amount is added in step (4).
10. the preparation method of a kind of Chinese crude drug compound recipe tea tree ethereal oil according to claim 4, is characterized in that, in step (4), added emulsifying agent is polyglycerol stearate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510159572.9A CN104721398A (en) | 2015-04-07 | 2015-04-07 | Traditional Chinese medicine compound tea tree essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510159572.9A CN104721398A (en) | 2015-04-07 | 2015-04-07 | Traditional Chinese medicine compound tea tree essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104721398A true CN104721398A (en) | 2015-06-24 |
Family
ID=53446194
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510159572.9A Withdrawn CN104721398A (en) | 2015-04-07 | 2015-04-07 | Traditional Chinese medicine compound tea tree essential oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104721398A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104055854A (en) * | 2013-03-21 | 2014-09-24 | 梅广浦 | Traditional Chinese medicine composition capable of removing acne |
-
2015
- 2015-04-07 CN CN201510159572.9A patent/CN104721398A/en not_active Withdrawn
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104055854A (en) * | 2013-03-21 | 2014-09-24 | 梅广浦 | Traditional Chinese medicine composition capable of removing acne |
Non-Patent Citations (2)
| Title |
|---|
| 《安徽医科大学学报》 * |
| 《现代中医药》 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103479775B (en) | Scraping liniment and preparation method thereof | |
| CN105213284A (en) | A kind of anti-acne moisturiser and preparation method thereof | |
| CN103751635A (en) | Traditional Chinese medicine mask for treating chloasma and preparation method thereof | |
| CN105125466A (en) | Freckle removing night cream and preparing method thereof | |
| CN104524125B (en) | A kind of traditional Chinese medicine emulsifiable paste for treating eczema and preparation method thereof | |
| CN105326753A (en) | Cheilogramma-fading nourishing lipstick and preparing method thereof | |
| CN105213941A (en) | A kind of Chinese medicine composition being used for the treatment of infantile diarrhea and preparation method thereof | |
| CN103877247A (en) | Medicine for treating bedsore and preparation method thereof | |
| CN105662996A (en) | Traditional Chinese medicine mask for treating menstruation-associated acne | |
| CN105213279A (en) | A kind of body lotion eliminating striae atrophicae and preparation method thereof | |
| CN101164600A (en) | Medicine for treating acne and whelk | |
| CN106421392A (en) | Traditional Chinese medicinal gel for treating bedsore and preparation method of traditional Chinese medicinal gel | |
| CN106039022A (en) | Skin brightening and whitening traditional Chinese medicinal composition, skin brightening and whitening traditional Chinese medicinal preparation, skin brightening and whitening mask and preparation method | |
| CN105561002A (en) | Folium artemisiae argyi health-care foot bath powder and preparation method thereof | |
| CN105709020A (en) | Foot bath powder with folium artemisiae argyi decoction dregs and preparation method thereof | |
| CN104887591A (en) | Composition for controlling oil, removing acne and resurfacing scars | |
| CN105213285A (en) | A kind of anti-acne facial cleanser and preparation method thereof | |
| CN105194487A (en) | Whitening and beautifying traditional Chinese medicine composition and facial mask and preparation method | |
| CN105342954A (en) | Traditional Chinese medicine mask with skin activating, blood stasis removing and yellow and freckle removing functions and preparation method thereof | |
| CN104888152A (en) | Traditional Chinese medicine preparation for treating postpartum depression and preparation method therefor | |
| CN104491596A (en) | Traditional Chinese medicine composition for treating liver-kidney yin deficiency type stroke and application thereof | |
| CN108272986A (en) | A kind of draft is bathed powder | |
| CN105687051A (en) | Bath salt with acne removal effect and preparation method | |
| CN106822300B (en) | Traditional Chinese medicine preparation for removing acne and beautifying face | |
| CN105342923A (en) | Lipstick for preventing lip chapping and its preparation method |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information |
Address after: 638500 Guang'an City, Guang'an Province, Park Street, No. 27, building 1, unit 502, 2 Applicant after: Fan Yongqi Address before: 250000 Ji'nan, central city, Shandong Lang Lang Road, No. 29 Applicant before: Fan Yongqi |
|
| COR | Change of bibliographic data | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20150624 |
|
| WW01 | Invention patent application withdrawn after publication |