CN104695218A - Sterilization softener for pure cotton fabric - Google Patents
Sterilization softener for pure cotton fabric Download PDFInfo
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- CN104695218A CN104695218A CN201510126822.9A CN201510126822A CN104695218A CN 104695218 A CN104695218 A CN 104695218A CN 201510126822 A CN201510126822 A CN 201510126822A CN 104695218 A CN104695218 A CN 104695218A
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Abstract
The invention discloses a sterilization softener for pure cotton fabric. The sterilization softener comprises first components and second components. The first components comprise the component A, the component B and the component C; the component A comprises, by mass, 67-75 parts of stearic acid, 21-23 parts of polyamine dien and 11-15 parts of dien; the component B comprises, by mass, 9-11 parts of dimethyl sulfate, 7-9 parts of diethyl sulfate, 6-10 parts of epoxy chloropropane and 5-9 parts of diethyl sulfate; the component C comprises, by mass, 4-8 parts of glycerin monostearate, 7-15 parts of polyoxyethylene sorbitan fatty acid esters and 2-6 parts of fatty alcohol-polyoxyethylene ether. The second components comprise, by mass, 17-21 parts of sorbitan monostearate, 7-13 parts of fatty alcohol-polyoxyethylene ether, 12-16 parts of baking soda, 13-15 parts of sodium tripolyphosphate and 18-22 parts of ethyl alcohol. The sterilization softener is safe, reliable, environmentally friendly and poisonless, harmless and nonirritating to the human body, the manufacturing process is simple and easy to implement, raw materials are easy to obtain, and the manufacturing cost is low.
Description
Technical field
The invention belongs to textile technology field, relate to a kind of pure-cotton fabric sterilization softener.
Background technology
China is the big country of textile production and outlet, china textile industry self is through development for many years, competitive advantage is fairly obvious, possesses most complete industrial chain in the world, the highest process mating level, the capacity of self-regulation of the industry cluster ground reply market risk of numerous prosperity constantly strengthens, and the developing steps keeping sane to industry provide solid guarantee.From international environment, international market still has expands space more greatly and opportunity.Along with 2007 the end of the year Central European textiles limit expire, 2008 the end of the year China-America Textile quota to limit end, China Textile quota-free era is coming, account for the area all-round opening of global piece market more than 60% share, bring huge opportunity will to China Textile trade.And the coming years, World Economics will be in first transition, will promote the growth of international trade, this brings favourable international market to ensure by increasing to China Textile Clothing Export.
Chemical constitution and the aggregated structure of regeneration and native cellulose fibre are different from synthetic fiber, containing more hydrophilic radical (hydroxyl) in their molecular structure, strand and crystal orientation poor, degree of crystallinity is lower, there is more microgap between strand and between fiber, result in excellent hygroscopicity, gas permeability and snugness of fit.But cellulose base fiber fabric easily shrinks deformation when taking and wash, wrinkle resistance, resilience are poor.
The antibiotic finish of fabric is one of method eliminating pathogenic microorganisms on fabric, and antibiotic finish is called as antimicrobial finish in the U.S. etc.; Antibacterial deodourizing processing is called as in Japan; Someone is referred to as hygienic finishing at home.Weaving antiseptic can be divided into natural, organic and inorganic three major types.Every class antiseptic has its pluses and minuses, and organic antiseptic is effective, wide in variety, is a most widely used class antiseptic at present, but there is the problems such as heat-resistant stable difference, is difficult to use in synthetic fiber spinning technique; Natural antimicrobial agent has good security usually, but its range of application is narrow, and majority has a strong impact on the coloured light of fabric; Inorganic antiseptic good heat resistance, but be difficult to obtain durable effect for after-finishing of textile products, and there is the toxicity problem of heavy metal in most of kind.
Summary of the invention
Technical problem to be solved by this invention is, overcomes the shortcoming of prior art, provides a kind of pure-cotton fabric sterilization softener, product safety of the present invention is reliable, and environmental protection, does not stimulate human non-toxic is harmless, and manufacturing technique is simple to operation, raw material easily obtains, cost of manufacture is low.
In order to solve above technical problem, the invention provides a kind of pure-cotton fabric sterilization softener, comprise first, second component, first component comprises A, B and component C, and its composition comprises following component according to the mass fraction:
First component:
Component A: stearic acid 67-75 part, polyamines is diethylenetriamines 21-23 part, diethylenetriamines 11-15 part;
B component: dimethyl suflfate 9-11 part, dithyl sulfate 7-9 part, epoxychloropropane 6-10 part, dithyl sulfate 5-9 part;
Component C: glycerin monostearate 4-8 part, tween 7-15 part, fatty alcohol-polyoxyethylene ether 2-6 part;
Component B:
Span60 17-21 part, fatty alcohol-polyoxyethylene ether 7-13 part, sodium bicarbonate 12-16 part, sodium phosphate trimer 13-15 part, ethanol 18-22 part.
The technical scheme that the present invention limits further is:
The invention provides a kind of preparation method of pure-cotton fabric sterilization softener, comprise following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 45-48 DEG C, stirs 28-30min with the rotating speed of 350-370r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, be heated to 43-45 DEG C, 20-24min is stirred, the B component in obtained first component with the rotating speed of 320-340r/min;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, be heated to 37-39 DEG C, stirs 12-14min with the rotating speed of 380-400r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 58-64 DEG C, 15-17min is stirred with the rotating speed of 430-450r/min, obtained component B, successively toward wherein adding A, B and component C, then at 36-38 DEG C of temperature, stir 30-45min with the rotating speed of 400-420r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
The invention has the beneficial effects as follows:
The product cost of raw material of the present invention is cheap, be easy to obtain, manufacturing cost is lower, can reach better submissive effect, this product is not containing harmful chemical and heavy metal ion, non-stimulated to human body simultaneously, without allergy, without teratogenesis, without mutagenesis, without carcinogenesis, to human non-toxic's side effect, and there is good mobility, and good stability, clothing can be made more soft, smooth, have anlistatig effect concurrently, clothing is in washing process, fiber fines is often wound around, intertwine, even rupture, clothing is after repeatedly washing, the slickness that the alkalescence effect of washing agent more makes fiber intrinsic, extensibility and elasticity are affected, what show is that one integral piece clothing seems to wear, no shape, touch feel stiff especially, more this clothes washing number of times sensation be more obvious, certain fabric is through the conditioning of softener of the present invention, fiber has recovered original form, fold on fabric also considerably reduces, complicated flatiron work is originally made to become simple, easily, time saving and energy saving.
Present invention process reaction temperature is low, and process safety is stablized, and saves time and the energy; This product does not contain formaldehyde, containing heavy metal ion, without allergy, without teratogenesis, without mutagenesis, without carcinogenesis, is conducive to environmental protection, and to human non-toxic's side effect, technique is simple, is easy to operate, and low temperature preparation, economize energy.
Detailed description of the invention
embodiment 1
The present embodiment provides a kind of pure-cotton fabric sterilization softener, and comprise first, second component, first component comprises A, B and component C, and its composition comprises following component according to the mass fraction:
First component:
Component A: stearic acid 67 parts, polyamines is diethylenetriamines 21 parts, diethylenetriamines 11 parts;
B component: dimethyl suflfate 9 parts, dithyl sulfate 7 parts, epoxychloropropane 6 parts, dithyl sulfate 5 parts;
Component C: glycerin monostearate 4 parts, tween 7 parts, fatty alcohol-polyoxyethylene ether 2 parts;
Component B:
Span60 17 parts, fatty alcohol-polyoxyethylene ether 7 parts, 12 parts, sodium bicarbonate, sodium phosphate trimer 13 parts, ethanol 18 parts.
The present embodiment provides a kind of preparation method of pure-cotton fabric sterilization softener, comprises following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 45 DEG C, stirs 30min with the rotating speed of 350r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, is heated to 43 DEG C, stirs 24min with the rotating speed of 320r/min, the B component in obtained first component;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, is heated to 37 DEG C, stirs 14min with the rotating speed of 380r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 58 DEG C, 17min is stirred with the rotating speed of 430r/min, obtained component B, successively toward wherein adding A, B and component C, then at 36 DEG C of temperature, stir 45min with the rotating speed of 400r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
embodiment 2
The present embodiment provides a kind of pure-cotton fabric sterilization softener, and comprise first, second component, first component comprises A, B and component C, and its composition comprises following component according to the mass fraction:
First component:
Component A: stearic acid 75 parts, polyamines is diethylenetriamines 23 parts, diethylenetriamines 15 parts;
B component: dimethyl suflfate 11 parts, dithyl sulfate 9 parts, epoxychloropropane 10 parts, dithyl sulfate 9 parts;
Component C: glycerin monostearate 8 parts, tween 15 parts, fatty alcohol-polyoxyethylene ether 6 parts;
Component B:
Span60 21 parts, fatty alcohol-polyoxyethylene ether 13 parts, 16 parts, sodium bicarbonate, sodium phosphate trimer 15 parts, ethanol 22 parts.
The present embodiment provides a kind of preparation method of pure-cotton fabric sterilization softener, comprises following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 48 DEG C, stirs 28min with the rotating speed of 370r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, is heated to 45 DEG C, stirs 20min with the rotating speed of 340r/min, the B component in obtained first component;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, is heated to 39 DEG C, stirs 12min with the rotating speed of 400r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 64 DEG C, 15min is stirred with the rotating speed of 450r/min, obtained component B, successively toward wherein adding A, B and component C, then at 38 DEG C of temperature, stir 30min with the rotating speed of 420r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
embodiment 3
The present embodiment provides a kind of pure-cotton fabric sterilization softener, and comprise first, second component, first component comprises A, B and component C, and its composition comprises following component according to the mass fraction:
First component:
Component A: stearic acid 71 parts, polyamines is diethylenetriamines 22 parts, diethylenetriamines 13 parts;
B component: dimethyl suflfate 10 parts, dithyl sulfate 8 parts, epoxychloropropane 8 parts, dithyl sulfate 7 parts;
Component C: glycerin monostearate 6 parts, tween 11 parts, fatty alcohol-polyoxyethylene ether 4 parts;
Component B:
Span60 19 parts, fatty alcohol-polyoxyethylene ether 10 parts, 14 parts, sodium bicarbonate, sodium phosphate trimer 14 parts, ethanol 20 parts.
The present embodiment provides a kind of preparation method of pure-cotton fabric sterilization softener, comprises following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 46 DEG C, stirs 29min with the rotating speed of 360r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, is heated to 44 DEG C, stirs 22min with the rotating speed of 330r/min, the B component in obtained first component;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, is heated to 38 DEG C, stirs 13min with the rotating speed of 390r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 61 DEG C, 16min is stirred with the rotating speed of 440r/min, obtained component B, successively toward wherein adding A, B and component C, then at 37 DEG C of temperature, stir 38min with the rotating speed of 410r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
Above embodiment is only and technological thought of the present invention is described, can not limit protection scope of the present invention with this, and every technological thought proposed according to the present invention, any change that technical scheme basis is done, all falls within scope.
Claims (5)
1. a pure-cotton fabric sterilization softener, is characterized in that, comprises first, second component, and described first component comprises A, B and component C, and its composition comprises following component according to the mass fraction:
First component:
Component A: stearic acid 67-75 part, polyamines is diethylenetriamines 21-23 part, diethylenetriamines 11-15 part;
B component: dimethyl suflfate 9-11 part, dithyl sulfate 7-9 part, epoxychloropropane 6-10 part, dithyl sulfate 5-9 part;
Component C: glycerin monostearate 4-8 part, tween 7-15 part, fatty alcohol-polyoxyethylene ether 2-6 part;
Component B:
Span60 17-21 part, fatty alcohol-polyoxyethylene ether 7-13 part, sodium bicarbonate 12-16 part, sodium phosphate trimer 13-15 part, ethanol 18-22 part.
2. the preparation method of pure-cotton fabric sterilization softener according to claim 1, is characterized in that, comprise following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 45-48 DEG C, stirs 28-30min with the rotating speed of 350-370r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, be heated to 43-45 DEG C, 20-24min is stirred, the B component in obtained first component with the rotating speed of 320-340r/min;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, be heated to 37-39 DEG C, stirs 12-14min with the rotating speed of 380-400r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 58-64 DEG C, 15-17min is stirred with the rotating speed of 430-450r/min, obtained component B, successively toward wherein adding A, B and component C, then at 36-38 DEG C of temperature, stir 30-45min with the rotating speed of 400-420r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
3. the preparation method of pure-cotton fabric sterilization softener according to claim 2, is characterized in that, comprise following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 45 DEG C, stirs 30min with the rotating speed of 350r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, is heated to 43 DEG C, stirs 24min with the rotating speed of 320r/min, the B component in obtained first component;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, is heated to 37 DEG C, stirs 14min with the rotating speed of 380r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 58 DEG C, 17min is stirred with the rotating speed of 430r/min, obtained component B, successively toward wherein adding A, B and component C, then at 36 DEG C of temperature, stir 45min with the rotating speed of 400r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
4. the preparation method of pure-cotton fabric sterilization softener according to claim 2, is characterized in that, comprise following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 48 DEG C, stirs 28min with the rotating speed of 370r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, is heated to 45 DEG C, stirs 20min with the rotating speed of 340r/min, the B component in obtained first component;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, is heated to 39 DEG C, stirs 12min with the rotating speed of 400r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 64 DEG C, 15min is stirred with the rotating speed of 450r/min, obtained component B, successively toward wherein adding A, B and component C, then at 38 DEG C of temperature, stir 30min with the rotating speed of 420r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
5. the preparation method of pure-cotton fabric sterilization softener according to claim 2, is characterized in that, comprise following concrete steps:
Step (1): be that diethylenetriamines and diethylenetriamines join in reactor by stearic acid, polyamines according to said ratio, is heated to 46 DEG C, stirs 29min with the rotating speed of 360r/min, the component A in obtained first component;
Step (2): dimethyl suflfate, dithyl sulfate, epoxychloropropane and dithyl sulfate are joined in the deionized water of 40 parts according to said ratio, is heated to 44 DEG C, stirs 22min with the rotating speed of 330r/min, the B component in obtained first component;
Step (3): glycerin monostearate, tween and fatty alcohol-polyoxyethylene ether are joined in the deionized water of 25 parts according to said ratio, is heated to 38 DEG C, stirs 13min with the rotating speed of 390r/min, the component C in obtained first component;
Step (4): Span60, fatty alcohol-polyoxyethylene ether, sodium bicarbonate, sodium phosphate trimer and ethanol are joined in reactor according to said ratio, be heated to 61 DEG C, 16min is stirred with the rotating speed of 440r/min, obtained component B, successively toward wherein adding A, B and component C, then at 37 DEG C of temperature, stir 38min with the rotating speed of 410r/min, then leave standstill nature cooling, obtain bamboo charcoal cashmere blended yarn woven fabric softener.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510126822.9A CN104695218B (en) | 2015-03-23 | 2015-03-23 | A kind of pure-cotton fabric sterilization softener |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510126822.9A CN104695218B (en) | 2015-03-23 | 2015-03-23 | A kind of pure-cotton fabric sterilization softener |
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| CN104695218A true CN104695218A (en) | 2015-06-10 |
| CN104695218B CN104695218B (en) | 2016-08-31 |
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| CN201510126822.9A Expired - Fee Related CN104695218B (en) | 2015-03-23 | 2015-03-23 | A kind of pure-cotton fabric sterilization softener |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106087397A (en) * | 2016-06-03 | 2016-11-09 | 湖州宏鑫绸厂 | A kind of rabbit hair fabric moth proofing agent |
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| CN1099824A (en) * | 1993-09-01 | 1995-03-08 | 王玉文 | Textiles softening agent |
| CN102766549A (en) * | 2012-06-29 | 2012-11-07 | 南通永源服饰有限公司 | Antibacterial and disinfectant detergent powder |
| CN102877293A (en) * | 2011-07-11 | 2013-01-16 | 李晓梅 | Softener suitable for plurality of fabrics |
| CN102877312A (en) * | 2012-09-05 | 2013-01-16 | 吴江涵辉纺织有限公司 | Fabric softener |
| CN102995397A (en) * | 2011-09-19 | 2013-03-27 | 孙善家 | High-efficiency biological anti-bacterial washing softener |
| CN103013700A (en) * | 2011-09-26 | 2013-04-03 | 姚水莲 | Liquid disinfecting detergent |
-
2015
- 2015-03-23 CN CN201510126822.9A patent/CN104695218B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1099824A (en) * | 1993-09-01 | 1995-03-08 | 王玉文 | Textiles softening agent |
| CN102877293A (en) * | 2011-07-11 | 2013-01-16 | 李晓梅 | Softener suitable for plurality of fabrics |
| CN102995397A (en) * | 2011-09-19 | 2013-03-27 | 孙善家 | High-efficiency biological anti-bacterial washing softener |
| CN103013700A (en) * | 2011-09-26 | 2013-04-03 | 姚水莲 | Liquid disinfecting detergent |
| CN102766549A (en) * | 2012-06-29 | 2012-11-07 | 南通永源服饰有限公司 | Antibacterial and disinfectant detergent powder |
| CN102877312A (en) * | 2012-09-05 | 2013-01-16 | 吴江涵辉纺织有限公司 | Fabric softener |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106087397A (en) * | 2016-06-03 | 2016-11-09 | 湖州宏鑫绸厂 | A kind of rabbit hair fabric moth proofing agent |
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| CN104695218B (en) | 2016-08-31 |
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Effective date of registration: 20160719 Address after: 215104 Suzhou, Wuzhong District Yue Creek Street, Swan Road, No. 10 Applicant after: Suzhou Jing Yuan oil pressure Machinery Co., Ltd. Address before: Wuzhong District town Suzhou city Jiangsu province 215101 collection of Qin Feng Cun Applicant before: Suzhou Chen Heng weaves Co., Ltd |
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