CN104693833A - Preparation method of onion skin vegetable dye - Google Patents
Preparation method of onion skin vegetable dye Download PDFInfo
- Publication number
- CN104693833A CN104693833A CN201510140693.9A CN201510140693A CN104693833A CN 104693833 A CN104693833 A CN 104693833A CN 201510140693 A CN201510140693 A CN 201510140693A CN 104693833 A CN104693833 A CN 104693833A
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- CN
- China
- Prior art keywords
- dye
- onion skin
- onion
- powder
- skin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a preparation method of an onion skin vegetable dye. The preparation method of the onion skin vegetable dye comprises the steps that firstly, onion skin is selected, cleaned and dried, and then the onion skin is crushed into plant powder of 30-80 meshes through a medicinal herb grinder; secondly, the plant powder is placed into an extraction pot, absolute ethyl alcohol is added into the extraction pot, the plant powder and the absolute ethyl alcohol are stirred for three hours to extract natural dye liquor, the proportion between the onion skin and the absolute ethyl alcohol is 1 to 10-20, and a dye liquid is obtained after filtering and slag removal are conducted; thirdly, the dye liquid is heated to reach 65-70 DEG C, the dye liquid is concentrated and the dye concentrated liquid with the concentration being 40%-50% is obtained; fourthly, reduction vaporization is conducted on the dye concentrated liquid through a rotary evaporator, and the dye concentrated liquid is volatilized and dried into natural dye powder. Raw materials of the onion skin vegetable dye are conveniently obtained, and the production process is simple. The prepared powder dye is convenient to transport, store and produce and high in production efficiency.
Description
[technical field]
The present invention relates to chemical dyestuff technical field, be specifically related to a kind of preparation method of onion-skin vegetable dye.
[background technology]
Along with the raising of people's living standard, quality of life and living environment are more and more paid attention to, the biological degradation of natural plant dye self energy, do not affect environment, vegetable dye originating species, can expand plantation, continuous production, and it is applied to textile dyeing, there is significant Social benefit and economic benefit.Onion-skin contains pigment, is a kind of well Pure natural dye.
[summary of the invention]
The invention provides a kind of preparation method of onion-skin vegetable dye, make its technique simple, production efficiency is high, easily extracts the natural plant dye with dyeing function.
The technical scheme that the preparation method of a kind of onion-skin of the present invention vegetable dye adopts is: a kind of preparation method of onion-skin vegetable dye, comprise the following steps: step 1: choose onion-skin, clean, dry, then be ground into 30-80 object plant powder with medicinal herb grinder; Step 2: plant powder is placed in extractor, adds dehydrated alcohol, and stir and extract natural dye liquor in 3 hours, onion-skin is 1: 10-20 with the ratio of dehydrated alcohol, namely obtains dye solution after filter and remove residue; Step 3: dye solution is heated to 65-70 DEG C, is concentrated into the dye concentrated solution that concentration is 40%-50%; Step 4: by dye concentrated solution through Rotary Evaporators reduction vaporization, volatile dry makes natural dye powder.
Further, Rotary Evaporators is dry: vacuum tightness 0.085 MPa, drying temperature is 50-60 DEG C.
The invention has the beneficial effects as follows: raw material sources are convenient, and production technique is simple; Be prepared into powder dye, be convenient to transport, store and produce, production efficiency is high.
[embodiment]
Below in conjunction with specific embodiment, the invention will be further described.
The preparation method of a kind of onion-skin vegetable dye of the present invention, comprises the following steps:
Step 1: choose onion-skin, cleans, and dries, then is ground into 30-80 object plant powder with medicinal herb grinder;
Step 2: plant powder is placed in extractor, adds dehydrated alcohol, and stir and extract natural dye liquor in 3 hours, onion-skin is 1: 10-20 with the ratio of dehydrated alcohol, namely obtains dye solution after filter and remove residue;
Step 3: dye solution is heated to 65-70 DEG C, is concentrated into the dye concentrated solution that concentration is 40%-50%;
Step 4: by dye concentrated solution through Rotary Evaporators reduction vaporization, volatile dry makes natural dye powder, wherein, Rotary Evaporators is dry: vacuum tightness 0.085 MPa, drying temperature is 50-60 DEG C.
In sum, the invention has the beneficial effects as follows: raw material sources are convenient, and production technique is simple; Be prepared into powder dye, be convenient to transport, store and produce, production efficiency is high.
Claims (2)
1. a preparation method for onion-skin vegetable dye, is characterized in that comprising the following steps:
Step 1: choose onion-skin, cleans, and dries, then is ground into 30-80 object plant powder with medicinal herb grinder;
Step 2: plant powder is placed in extractor, adds dehydrated alcohol, and stir and extract natural dye liquor in 3 hours, onion-skin is 1: 10-20 with the ratio of dehydrated alcohol, namely obtains dye solution after filter and remove residue;
Step 3: dye solution is heated to 65-70 DEG C, is concentrated into the dye concentrated solution that concentration is 40%-50%;
Step 4: by dye concentrated solution through Rotary Evaporators reduction vaporization, volatile dry makes natural dye powder.
2. the mixed planting method of a kind of cassava as claimed in claim 1 and soya bean, is characterized in that: Rotary Evaporators is dry: vacuum tightness 0.085 MPa, drying temperature is 50-60 DEG C.
Priority Applications (1)
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CN201510140693.9A CN104693833A (en) | 2015-03-30 | 2015-03-30 | Preparation method of onion skin vegetable dye |
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CN201510140693.9A CN104693833A (en) | 2015-03-30 | 2015-03-30 | Preparation method of onion skin vegetable dye |
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CN104693833A true CN104693833A (en) | 2015-06-10 |
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CN201510140693.9A Pending CN104693833A (en) | 2015-03-30 | 2015-03-30 | Preparation method of onion skin vegetable dye |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107312355A (en) * | 2017-06-12 | 2017-11-03 | 暨南大学 | The preparation and its application of purple skin Onion pigment |
PL424683A1 (en) * | 2018-02-26 | 2019-09-09 | Geecs Spółka Akcyjna | Method for obtaining extract from onion peel and the extract from onion peel obtained by this method |
CN110791120A (en) * | 2019-10-09 | 2020-02-14 | 五邑大学 | Extraction method of onion skin dye liquor, onion skin dye liquor and application of onion skin dye liquor in protein textiles |
CN113462192A (en) * | 2021-07-01 | 2021-10-01 | 上海禧蓝纺织品有限公司 | Extraction and dyeing method of plant dye and plant mordant |
Citations (6)
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JPH01179666A (en) * | 1988-01-06 | 1989-07-17 | Binshiyoo:Kk | Use of pigment extracted from onion skin |
JPH01269470A (en) * | 1988-04-21 | 1989-10-26 | San Ei Chem Ind Ltd | Coloring of seasoning and sauce in yellowish brown color |
RU2001072C1 (en) * | 1992-04-21 | 1993-10-15 | Лариса Михайловна Ильина | Method for obtaining dye from onion husks |
CN102119993A (en) * | 2011-03-07 | 2011-07-13 | 天津科技大学 | Preparation method of onion extract, application of onion extract for prolonging life of Caenorhabditis elegans and food containing onion extract |
CN103131207A (en) * | 2011-11-25 | 2013-06-05 | 宋德臣 | Ecological dye |
CN104073022A (en) * | 2014-06-26 | 2014-10-01 | 南通润启时装有限公司 | Preparation and application of onion-skin natural dye |
-
2015
- 2015-03-30 CN CN201510140693.9A patent/CN104693833A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01179666A (en) * | 1988-01-06 | 1989-07-17 | Binshiyoo:Kk | Use of pigment extracted from onion skin |
JPH01269470A (en) * | 1988-04-21 | 1989-10-26 | San Ei Chem Ind Ltd | Coloring of seasoning and sauce in yellowish brown color |
RU2001072C1 (en) * | 1992-04-21 | 1993-10-15 | Лариса Михайловна Ильина | Method for obtaining dye from onion husks |
CN102119993A (en) * | 2011-03-07 | 2011-07-13 | 天津科技大学 | Preparation method of onion extract, application of onion extract for prolonging life of Caenorhabditis elegans and food containing onion extract |
CN103131207A (en) * | 2011-11-25 | 2013-06-05 | 宋德臣 | Ecological dye |
CN104073022A (en) * | 2014-06-26 | 2014-10-01 | 南通润启时装有限公司 | Preparation and application of onion-skin natural dye |
Non-Patent Citations (1)
Title |
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吴素玲等: "洋葱黄酮类物质不同提取工艺的比较研究", 《安徽农业科学》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107312355A (en) * | 2017-06-12 | 2017-11-03 | 暨南大学 | The preparation and its application of purple skin Onion pigment |
PL424683A1 (en) * | 2018-02-26 | 2019-09-09 | Geecs Spółka Akcyjna | Method for obtaining extract from onion peel and the extract from onion peel obtained by this method |
CN110791120A (en) * | 2019-10-09 | 2020-02-14 | 五邑大学 | Extraction method of onion skin dye liquor, onion skin dye liquor and application of onion skin dye liquor in protein textiles |
CN113462192A (en) * | 2021-07-01 | 2021-10-01 | 上海禧蓝纺织品有限公司 | Extraction and dyeing method of plant dye and plant mordant |
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Application publication date: 20150610 |