CN104692980A - Humus acid nitrogen fertilizer granulating device and method thereof - Google Patents

Humus acid nitrogen fertilizer granulating device and method thereof Download PDF

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Publication number
CN104692980A
CN104692980A CN201510131034.9A CN201510131034A CN104692980A CN 104692980 A CN104692980 A CN 104692980A CN 201510131034 A CN201510131034 A CN 201510131034A CN 104692980 A CN104692980 A CN 104692980A
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CN
China
Prior art keywords
pipeline
liquid ejector
urine
buffering filter
humic acid
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510131034.9A
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Chinese (zh)
Inventor
王维超
辛寒晓
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SHANDONG ZOETICLAND BIOTECHNOLOGY Co Ltd
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SHANDONG ZOETICLAND BIOTECHNOLOGY Co Ltd
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Priority to CN201510131034.9A priority Critical patent/CN104692980A/en
Publication of CN104692980A publication Critical patent/CN104692980A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a humus acid nitrogen fertilizer granulating device and a method thereof. The humus acid nitrogen fertilizer granulating device comprises a storage tank, a liquid ejector, a buffering filter and a granulator which are connected through a pipeline in sequence. A material input port is formed in the liquid ejector and connected with a material hopper through a pipeline. The liquid ejectors eject the urine mixed material adsorbing humus acid and other solid materials into the buffering filter along a tangent line with the ultrasonic speed, stirring, mixing, filtering and foam separating are carried out in the buffering filter, and then the urine mixed material is conveyed to the granulator to be granulated in a high tower mode. The staying time of urine, humus acid and other solid materials in the pipelines is shortened, and the amount of generated biuret is reduced. The urine, humus acid and other solid materials are prevented from blocking the pipelines and equipment, and long-period stable running of a granulating device system is achieved.

Description

A kind of granulating equipment of humic acid nitrogenous fertilizer and method thereof
Technical field
The present invention relates to granulating equipment and the method thereof of nitrogenous fertilizer, be specifically related to a kind of granulating equipment and method thereof of humic acid nitrogenous fertilizer.
Background technology
Humic acids to chemical fertilizer particularly urea there is synergism, the reason of its synergy is from the restraining effect of humic acids to soil urease, humic acids not only can prevent urea too quick decomposition, also there is the synergism to urea, to the hormesis of crop growth, improve the anti-adversity of crop, improve crop and fruit quality, reduce Stoma of Leaves opening degree, reduce the resisting drought saving water performance of moisture transpiration, the slow releasing function etc. to agricultural chemicals, therefore effectively improve the utility value of urea.
But due to technical limitation, the equipment that the direct Hybrid Heating granulation of the solid materials such as urea and humic acid is never applicable to and method, reason is because urea fusing point is 132.7 DEG C, after adding the solid materialss such as humic acid, the urine viscosity of the solid materialss such as absorption humic acid will increase, and just must improve temperature to reduce its viscosity, temperature is higher, the biuret generated is more, and temperature height humic acid also easily decomposes.Biuret is the index that urea fertilizer strictly controls, in order to reduce Biuret Content, prilling temperature must be reduced again, such urine viscosity of adsorbing the solid materialss such as humic acid will increase, the solid materials such as urine and humic acid residence time in pipeline is longer, but also easy blocking pipe and equipment, bring difficulty to operation granulating equipment.
Summary of the invention
Technical problem to be solved by this invention is: the granulating equipment and the method thereof that provide a kind of humic acid nitrogenous fertilizer.Use the granulating equipment of this humic acid nitrogenous fertilizer and method thereof can not only shorten the solid materials such as urine and humic acid residence time in pipeline, reduce the generation quantity of biuret, reduce humic acid pyrolytic decomposition, increase fertilizer efficiency; And the solid materials such as urine and humic acid blocking pipe and equipment can also be avoided, the solid materials such as urine and humic acid transport condition is optimized, is conducive to this prilling equipment system long-period stable operation.
The technical scheme that the present invention solves the problems of the technologies described above is: a kind of granulating equipment of humic acid nitrogenous fertilizer, it is characterized in that: comprise hold-up vessel, liquid ejector, buffering filter, tablets press, described liquid ejector liquid inlet be connected with the delivery port of hold-up vessel by pipeline, liquid spraying outlet is connected with the input aperture of buffering filter by pipeline; Described liquid ejector is also provided with material input, and the material input that this liquid ejector is arranged is connected with material hopper by pipeline; The delivery port of described buffering filter is connected with tablets press mixture input aperture by pipeline; The pipeline that described liquid ejector is connected with hold-up vessel is installed with A under meter and force (forcing) pump successively, the pipeline that described liquid ejector is connected with material hopper is installed with B under meter;
As the preferred scheme of one, the pipeline that described buffering filter is connected with liquid ejector is taper, and the diameter of this pipeline near one end of this buffering filter is greater than the diameter of this pipeline near one end of this liquid ejector.
A prilling process for humic acid nitrogenous fertilizer, described humic acid nitrogenous fertilizer, is made up of the raw material of following weight per-cent: urea 70-80%, solid materials 20-30%; It is characterized in that: comprise the steps:
The melting of A, described urea input hold-up vessel is the step of urine, this urea nitrogen content >=46%, moisture < 1%, biuret < 1%; The temperature 135-140 DEG C of this urea input hold-up vessel melting;
B, configuration solid materials input the step of material hopper, described solid materials is made up of the raw material of following weight per-cent: 40-60% humic acid; 15-20% monoammonium phosphate, diammonium phosphate or potassium primary phosphate one or more; One or more in 15-20% Repone K, potassium sulfate or potassium primary phosphate; One or more in 10-20% nitrocalcite, ferric sulfate, zinc sulfate, magnesium sulfate, copper sulfate, manganous sulfate, boric acid, borax or ammonium molybdate; One or both of 0.1-0.5 ‰ DA-6, the alcohol milk powder that rues;
C, described urine are pressurizeed by force (forcing) pump by the delivery port flow ipe of hold-up vessel, send into the liquid inlet of liquid ejector and liquid ejector material input and suck and to be inputted by material hopper and the step of described solid materials through the metering of B under meter after the metering of A under meter; The pressure of described force (forcing) pump pressurization is 1-1.5MPa;
The urine mixture of adsorbent solid material is ejected into the step of buffering filter by D, liquid ejector by ejiction opening;
E, urine mixture are uniformly mixed and filter and after being separated foam, send tablets press to carry out the step of high tower prilling in buffering filter.
The invention has the beneficial effects as follows: urine is pressurizeed by force (forcing) pump by the delivery port flow ipe of hold-up vessel, liquid ejector is sent into after the metering of A under meter, and with the urine after pressurization for power, the solid materialss such as the humic acid after being measured by B under meter by liquid ejector material input are sucked, the urine mixture of the solid materialss such as absorption humic acid tangentially sprays with ultrasonic speed and enters buffering filter by liquid ejector, under urine mixture impulse force is mixed, urine mixes with solid materialss such as humic acid and realizes being separated of foam in very short time, shorten the residence time of the solid materials such as urine and humic acid in pipeline, reduce the quantity of the biuret of generation, also avoid the solid materials such as urine and humic acid blocking pipe and equipment, the solid materials such as urine and humic acid transport condition is optimized, achieves this prilling equipment system long-period stable operation.
Accompanying drawing explanation
Below in conjunction with drawings and Examples, the present invention is further described;
Fig. 1 is structural representation of the present invention;
In accompanying drawing: 1. hold-up vessel, 2. liquid ejector, 3. buffering filter, 4. tablets press, 5. material hopper, 6.A under meter, 7. force (forcing) pump, 8.B under meter.
Embodiment
Below by specific embodiment, the present invention is described in further detail.
Embodiment 1
As shown in Figure 1, a kind of granulating equipment of humic acid nitrogenous fertilizer, it is characterized in that: comprise hold-up vessel 1, liquid ejector 2, buffering filter 3, tablets press 4, described liquid ejector 2 liquid inlet be connected by the delivery port of pipeline with hold-up vessel 1, liquid spraying outlet is connected by the input aperture of pipeline with buffering filter 3; Described liquid ejector 2 is also provided with material input, and the material input that this liquid ejector 2 is arranged is connected with material hopper 5 by pipeline; The delivery port of described buffering filter 3 is connected with tablets press 4 mixture input aperture by pipeline; The pipeline that described liquid ejector 2 is connected with hold-up vessel 1 is installed with A under meter 6 and force (forcing) pump 7 successively, the pipeline that described liquid ejector 2 is connected with material hopper 5 is installed with B under meter 8;
As the preferred scheme of one, the pipeline that described buffering filter 3 is connected with liquid ejector 2 is taper, and the diameter of this pipeline near one end of this buffering filter 3 is greater than the diameter of this pipeline near one end of this liquid ejector 2.
A prilling process for humic acid nitrogenous fertilizer, described humic acid nitrogenous fertilizer, is made up of the raw material of following weight per-cent: urea 70-80%, solid materials 20-30%; It is characterized in that: comprise the steps:
The melting of A, described urea input hold-up vessel 1 is the step of urine, this urea nitrogen content >=46%, moisture < 1%, biuret < 1%; The temperature 135-140 DEG C of this urea input hold-up vessel 1 melting;
B, configuration solid materials input the step of material hopper 5, described solid materials is made up of the raw material of following weight per-cent: 40-60% humic acid; 15-20% monoammonium phosphate, diammonium phosphate or potassium primary phosphate one or more; One or more in 15-20% Repone K, potassium sulfate or potassium primary phosphate; One or more in 10-20% nitrocalcite, ferric sulfate, zinc sulfate, magnesium sulfate, copper sulfate, manganous sulfate, boric acid, borax or ammonium molybdate; One or both of 0.1-0.5 ‰ DA-6, the alcohol milk powder that rues;
C, described urine are pressurizeed by force (forcing) pump 7 by the delivery port flow ipe of hold-up vessel 1, send into the liquid inlet of liquid ejector 2 and liquid ejector 2 material input and suck and to be inputted by material hopper 5 and the step of the described solid materials measured through B under meter 8 after A under meter 6 measures; The pressure that described force (forcing) pump 7 pressurizes is 1-1.5MPa;
The urine mixture of adsorbent solid material is ejected into the step of buffering filter 3 by D, liquid ejector 2 by ejiction opening;
E, urine mixture are uniformly mixed and filter and after being separated foam, send tablets press 4 to carry out the step of high tower prilling in buffering filter 3.
By above-mentioned description, those skilled in the art in the scope not departing from this invention technological thought, can carry out various change and revise within protection scope of the present invention completely.Unaccomplished matter of the present invention, belongs to the common practise of those skilled in the art.

Claims (3)

1. the granulating equipment of a humic acid nitrogenous fertilizer, it is characterized in that: comprise hold-up vessel, liquid ejector, buffering filter, tablets press, described liquid ejector liquid inlet be connected with the delivery port of hold-up vessel by pipeline, liquid spraying outlet is connected with the input aperture of buffering filter by pipeline; Described liquid ejector is also provided with material input, and the material input that this liquid ejector is arranged is connected with material hopper by pipeline; The delivery port of described buffering filter is connected with tablets press mixture input aperture by pipeline; The pipeline that described liquid ejector is connected with hold-up vessel is installed with A under meter and force (forcing) pump successively, the pipeline that described liquid ejector is connected with material hopper is installed with B under meter.
2. the granulating equipment of a kind of humic acid nitrogenous fertilizer according to claim 1, it is characterized in that: the pipeline that described buffering filter is connected with liquid ejector is taper, the diameter of this pipeline near one end of this buffering filter is greater than the diameter of this pipeline near one end of this liquid ejector.
3., as used the prilling process of a kind of humic acid nitrogenous fertilizer granulating equipment as described in claim 1 or 2, described humic acid nitrogenous fertilizer, is made up of the raw material of following weight per-cent: urea 70-80%, solid materials 20-30%; It is characterized in that: comprise the steps:
The melting of A, described urea input hold-up vessel is the step of urine, this urea nitrogen content >=46%, moisture < 1%, biuret < 1%; The temperature 135-140 DEG C of this urea input hold-up vessel melting;
B, configuration solid materials input the step of material hopper, described solid materials is made up of the raw material of following weight per-cent: 40-60% humic acid; 15-20% monoammonium phosphate, diammonium phosphate or potassium primary phosphate one or more; One or more in 15-20% Repone K, potassium sulfate or potassium primary phosphate; One or more in 10-20% nitrocalcite, ferric sulfate, zinc sulfate, magnesium sulfate, copper sulfate, manganous sulfate, boric acid, borax or ammonium molybdate; One or both of 0.1-0.5 ‰ DA-6, the alcohol milk powder that rues;
C, described urine are pressurizeed by force (forcing) pump by the delivery port flow ipe of hold-up vessel, send into the liquid inlet of liquid ejector and liquid ejector material input and suck and to be inputted by material hopper and the step of described solid materials through the metering of B under meter after the metering of A under meter; The pressure of described force (forcing) pump pressurization is 1-1.5MPa;
The urine mixture of adsorbent solid material is ejected into the step of buffering filter by D, liquid ejector by ejiction opening;
E, urine mixture are uniformly mixed and filter and after being separated foam, send tablets press to carry out the step of high tower prilling in buffering filter.
CN201510131034.9A 2015-03-24 2015-03-24 Humus acid nitrogen fertilizer granulating device and method thereof Pending CN104692980A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107500980A (en) * 2017-08-21 2017-12-22 河南心连心化肥有限公司 The dissolver and dissolving method of a kind of potassium fulvate and application
CN107556098A (en) * 2017-08-21 2018-01-09 河南心连心化肥有限公司 One kind increment humic acid urea, process units and its production method
CN108575678A (en) * 2018-03-20 2018-09-28 中国水利水电科学研究院 A kind of metering irrigation rig based on crop water requirement
CN112409060A (en) * 2020-10-27 2021-02-26 广东拉多美化肥有限公司 High-concentration potassium humate compound fertilizer and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN101429063A (en) * 2008-12-02 2009-05-13 王矛 Humic acid urea and method for producing the same
CN101486611A (en) * 2009-02-26 2009-07-22 赵艳芝 High tower spraying granulation humic acid organic and inorganic compound fertilizer and technique for producing the same
CN102267830A (en) * 2010-06-01 2011-12-07 吴绍山 Method for reducing biuret content in high tower melting granulated compound fertilizer
CN102491814A (en) * 2011-11-25 2012-06-13 史丹利化肥股份有限公司 High-concentration humic acid type chelated multi-trace element special fertilizer for wheat and production method thereof
CN102731171A (en) * 2012-06-05 2012-10-17 四川美丰化工股份有限公司 Solid urea fusion guniting granulation system

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Publication number Priority date Publication date Assignee Title
CN101429063A (en) * 2008-12-02 2009-05-13 王矛 Humic acid urea and method for producing the same
CN101486611A (en) * 2009-02-26 2009-07-22 赵艳芝 High tower spraying granulation humic acid organic and inorganic compound fertilizer and technique for producing the same
CN102267830A (en) * 2010-06-01 2011-12-07 吴绍山 Method for reducing biuret content in high tower melting granulated compound fertilizer
CN102491814A (en) * 2011-11-25 2012-06-13 史丹利化肥股份有限公司 High-concentration humic acid type chelated multi-trace element special fertilizer for wheat and production method thereof
CN102731171A (en) * 2012-06-05 2012-10-17 四川美丰化工股份有限公司 Solid urea fusion guniting granulation system

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107500980A (en) * 2017-08-21 2017-12-22 河南心连心化肥有限公司 The dissolver and dissolving method of a kind of potassium fulvate and application
CN107556098A (en) * 2017-08-21 2018-01-09 河南心连心化肥有限公司 One kind increment humic acid urea, process units and its production method
CN108575678A (en) * 2018-03-20 2018-09-28 中国水利水电科学研究院 A kind of metering irrigation rig based on crop water requirement
CN108575678B (en) * 2018-03-20 2023-11-24 中国水利水电科学研究院 Metering irrigation device based on crop water demand
CN112409060A (en) * 2020-10-27 2021-02-26 广东拉多美化肥有限公司 High-concentration potassium humate compound fertilizer and preparation method thereof
CN112409060B (en) * 2020-10-27 2022-05-17 广东拉多美化肥有限公司 High-concentration potassium humate compound fertilizer and preparation method thereof

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