CN104690861A - Preparation method of artificial crystal cluster - Google Patents
Preparation method of artificial crystal cluster Download PDFInfo
- Publication number
- CN104690861A CN104690861A CN201510018920.0A CN201510018920A CN104690861A CN 104690861 A CN104690861 A CN 104690861A CN 201510018920 A CN201510018920 A CN 201510018920A CN 104690861 A CN104690861 A CN 104690861A
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- Prior art keywords
- crystal
- mould
- crystal column
- resin
- mixture
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- 239000013078 crystal Substances 0.000 title claims abstract description 113
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 71
- 239000000741 silica gel Substances 0.000 claims abstract description 59
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 59
- 239000011347 resin Substances 0.000 claims abstract description 49
- 229920005989 resin Polymers 0.000 claims abstract description 49
- 229960001866 silicon dioxide Drugs 0.000 claims description 58
- 239000000203 mixture Substances 0.000 claims description 45
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 36
- 239000003795 chemical substances by application Substances 0.000 claims description 20
- WFUGQJXVXHBTEM-UHFFFAOYSA-N 2-hydroperoxy-2-(2-hydroperoxybutan-2-ylperoxy)butane Chemical group CCC(C)(OO)OOC(C)(CC)OO WFUGQJXVXHBTEM-UHFFFAOYSA-N 0.000 claims description 12
- 239000010453 quartz Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 229910017052 cobalt Inorganic materials 0.000 claims description 10
- 239000010941 cobalt Substances 0.000 claims description 10
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical group [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 10
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 10
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 8
- PASHVRUKOFIRIK-UHFFFAOYSA-L calcium sulfate dihydrate Chemical compound O.O.[Ca+2].[O-]S([O-])(=O)=O PASHVRUKOFIRIK-UHFFFAOYSA-L 0.000 claims description 6
- 239000003054 catalyst Substances 0.000 claims description 5
- 229910052697 platinum Inorganic materials 0.000 claims description 5
- 208000034189 Sclerosis Diseases 0.000 claims description 4
- 239000011230 binding agent Substances 0.000 claims description 4
- 210000005056 cell body Anatomy 0.000 claims description 4
- 239000011248 coating agent Substances 0.000 claims description 4
- 238000000576 coating method Methods 0.000 claims description 4
- 239000003599 detergent Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 230000001680 brushing effect Effects 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000005034 decoration Methods 0.000 abstract 2
- 229910052602 gypsum Inorganic materials 0.000 abstract 1
- 239000010440 gypsum Substances 0.000 abstract 1
- 238000007711 solidification Methods 0.000 description 3
- 230000008023 solidification Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 230000008676 import Effects 0.000 description 2
- 239000008239 natural water Substances 0.000 description 2
- 239000002574 poison Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- -1 if do not stirred Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
Abstract
The invention relates to a preparation method of an artificial crystal cluster. The method comprises the following steps: preparing a gypsum crystal column; preparing a silica gel crystal column mold; preparing a resin crystal column; and preparing a simulated crystal cluster. The artificial crystal cluster prepared by the method is applied to decoration and arrangement, and is light in weight, and low in cost; mass production can be realized; the specification and the color can be customized; the price is only about 1/3 of that of a natural crystal cluster; and meanwhile, the decoration effect of the natural crystal cluster can be realized.
Description
Technical field
The present invention relates to the preparation method of a kind of synthetic quartz bunch, belong to the making field of decorative display handicraft.
Background technology
Crystal bunch: as the term suggests, be the crystal composition of cluster bunch.Be natural quartz crystals bunch, there is high sight and reserve value.On one group of crystal bunch market, asked price 5000 to 50000 is not etc.; Like this, asked price reaches about 100,000 to single the wide 150mm of crystal column height 500mm, and decorative display market is large to crystal bunch demand, in view of crystal bunch costliness, only has the high-grade place of minority to furnish.
Summary of the invention
Mineral crystal bunch rareness, expensive problem on the market, the invention provides the preparation method of a kind of synthetic quartz bunch, synthetic quartz bunch prepared by the present invention is applied to Hotspring Hotel, museum's karst topography, holiday village, tourist attraction etc.
The technical scheme that the present invention solves the problems of the technologies described above is as follows: the preparation method of a kind of synthetic quartz bunch, comprising:
1) parget water crystal column (formpiston) is made
Long 150-200mm is surrounded with 5mm acrylic board or 5 lis of plates, wide 20-30mm, first square groove of high 20mm-30mm, land plaster adds water mixing, pour in the first square groove, take out after sclerosis, accomplish with cutter six prisms that one end is hexagonal pyramid shape, obtain parget water crystal column, as resin crystal column archetype;
2) silica gel crystal column mould (former) is made
Surround long 200-250mm, wide 30-35mm with 5mm acrylic board or 5 lis of plates, second square groove of high 30-35mm, 1) the parget water crystal column that obtains is coated with the thick releasing agent of 0.2-0.5mm, after coating, parget water crystal column is lain in the center of the second square groove,
Mould silica gel adds curing agent and stirs, obtain mould silica-gel mixture, if do not stirred, silica gel crystal column mould there will be one piece and has cured, one piece of not solidification, mould silica gel there will be the uneven situation of dry solidification, affect the silica gel crystal column mold use life-span and turn over mould number of times, by mould silica-gel mixture indwelling ten minutes automatic froth breakings or vacuumize three minutes, the pumpdown time should not be too of a specified duration, otherwise the solidification at once of mould silica gel, produce cross-linking reaction, make mould silica gel become one piece one piece, cannot carry out brushing or pour into
With brush the mould silica-gel mixture brushing after froth breaking or after vacuumizing or be filled in the second square groove, pour the long-pending half of second party cell body into, get on mould silica-gel mixture that one piece of gauze is put in the second square groove, fill mould silica-gel mixture again, take out in the second square groove after mould silica-gel mixture parches, remove the parget water crystal column be wrapped in the middle of mould silica-gel mixture, obtain silica gel crystal column mould;
3) resin crystal column is made
In crystal resin, add promoter, stir, then add curing agent and stir, leave standstill 2-10 minute automatic froth breaking, obtain crystal resin mixture, crystal resin mixture is poured in silica gel crystal column mould, take out after crystal resin mixture solidifies completely, obtain resin crystal column;
4) artificial water druse is made
The resin crystal column of different size is bonded together by a crystal bunch growthform, obtain synthetic quartz bunch, wherein, binding agent used is the mixture of crystal resin, promoter and curing agent, if need different colours crystal bunch, only need add the mill base mated with crystal resin before crystal resin adds curing agent, addition is held according to sample.
On the basis of technique scheme, the present invention can also do following improvement.
Further, 1) make in parget water crystal column, described one end is six prisms length of hexagonal pyramid shape is 50-180mm, inscribed circle diameter is 10-30mm, the height of hexagonal pyramid accounts for the 1/10-1/5 that one end is six prism length of hexagonal pyramid shape, and the weight ratio of described land plaster and water is (1.2-1.4): 1.
Further, 2) make in silica gel crystal column mould, described releasing agent is liquid detergent, does not need to be watered when being coated with parget water crystal column.
Further, 2) make in silica gel crystal column mould, the weight ratio of described mould silica gel and curing agent is 100:(1-2), described mould silica gel is that Beijing Ding Ye Trade Co., Ltd. produces and commercially available product, described curing agent is platinum catalyst, for Beijing Ding Ye Trade Co., Ltd. produces and commercially available product.
Further, 3) make resin crystal column and 4) make in artificial water druse, the weight ratio of described crystal resin and promoter is 100:(0.3-0.5), the weight ratio of described crystal resin and curing agent is 100:(1.5-3), described crystal resin is the import ZJ-K39DG pebble naval stores that profit Chemical Co., Ltd. of Shenzhen sells, described curing agent is methyl ethyl ketone peroxide (MEKPO), described promoter is cobalt iso-octoate, and methyl ethyl ketone peroxide and cobalt iso-octoate are profit Chemical Co., Ltd. of Shenzhen product sold.
The invention has the beneficial effects as follows:
Synthetic quartz prepared by the present invention is bunch in decorative display, and lightweight, cost is low, can volume production, and specification, color are customizable, and price only has about 1/3 of natural water druse, can reach the decorative effect of natural water druse simultaneously.
Accompanying drawing explanation
Fig. 1 is synthetic quartz bunch figure prepared by the present invention;
Detailed description of the invention
Be described principle of the present invention and feature below, example, only for explaining the present invention, is not intended to limit scope of the present invention.
In embodiment, mould therefor silica gel is reverse mould silica gel special, for Beijing Ding Ye Trade Co., Ltd. manufacturer production and commercially available product.
In embodiment, platinum catalyst used is that Beijing Ding Ye Trade Co., Ltd. produces and commercially available product.
In embodiment, crystal resin used is the import ZJ-K39DG pebble naval stores that profit Chemical Co., Ltd. of Shenzhen sells.
In embodiment, curing agent methyl ethyl ketone peroxide (MEKPO) used is profit Chemical Co., Ltd. of Shenzhen product sold.
In embodiment, promoter cobalt iso-octoate used is profit Chemical Co., Ltd. of Shenzhen product sold.
Weather: fine temperature: 15 degree of environment: anti-poison respirator is worn in half outdoor
Embodiment 1
1) parget water crystal column (formpiston) is made
Long 150mm is surrounded with 5mm acrylic board, first square groove of wide 20mm, high 30mm, land plaster to add water mixing by weight 1.4:1, pour in the first square groove, take out after sclerosis, accomplish with cutter six prisms that one end is hexagonal pyramid shape, obtain parget water crystal column, wherein, one end is six prisms length of hexagonal pyramid shape is 180mm, and inscribed circle diameter is 20mm, hexagonal pyramid height 20mm.
2) silica gel crystal column mould (former) is made
Surround long 200mm with 5mm acrylic board, wide 30mm, second square groove of high 35mm, 1) the parget water crystal column that obtains is coated with the thick liquid detergent of 0.2mm (not being watered), after coating, parget water crystal column is lain in the center of the second square groove,
Mould silica gel adds platinum catalyst by weight 100:1, stir, obtain mould silica-gel mixture, by mould silica-gel mixture indwelling ten minutes automatic froth breakings, with brush, the mould silica-gel mixture after froth breaking is filled in the second square groove, pour the long-pending half of second party cell body into, get on mould silica-gel mixture that one piece of gauze is put in the second square groove, fill mould silica-gel mixture again, take out in the second square groove after mould silica-gel mixture parches, remove the parget water crystal column be wrapped in the middle of mould silica-gel mixture, obtain silica gel crystal column mould;
3) resin crystal column (transparent) is made
Cobalt iso-octoate is added in crystal resin, the weight ratio of crystal resin and cobalt iso-octoate is 100:0.5, stir, add methyl ethyl ketone peroxide again to stir, the weight ratio of crystal resin and methyl ethyl ketone peroxide is 100:1.5, leaves standstill 10 minutes automatic froth breakings, obtain crystal resin mixture, poured into by crystal resin mixture in silica gel crystal column mould, crystal resin mixture solidifies taking-up after 2 hours completely, obtains resin crystal column;
4) artificial water druse (transparent) is made
The resin crystal column of different size is bonded together by a crystal bunch growthform, obtains synthetic quartz bunch, wherein, binding agent used is the mixture of crystal resin, cobalt iso-octoate and methyl ethyl ketone peroxide 100:0.5:1.5 in mass ratio.
Embodiment 2
Weather: fine temperature: 5 degree of environment: anti-poison respirator is worn in outdoor
1) parget water crystal column (formpiston) is made
Long 150mm is surrounded with 5mm acrylic board, first square groove of wide 20mm, high 25mm, land plaster to add water mixing by weight 1.2:1, pour in the first square groove, take out after sclerosis, accomplish with cutter six prisms that one end is hexagonal pyramid shape, obtain parget water crystal column, wherein, one end is six prisms length of hexagonal pyramid shape is 120mm, and inscribed circle diameter is 15mm, hexagonal pyramid height 10mm.
2) silica gel crystal column mould (former) is made
Surround long 150mm with 5mm acrylic board, wide 30mm, second square groove of high 30mm, 1) the parget water crystal column that obtains is coated with the thick liquid detergent of 0.3mm (not being watered), after coating, parget water crystal column is lain in the center of the second square groove,
Mould silica gel adds platinum catalyst by weight 100:1, stir, obtain mould silica-gel mixture, by mould silica-gel mixture indwelling ten minutes automatic froth breakings, with brush, the mould silica-gel mixture after froth breaking is brushed in the second square groove, pour the long-pending half of second party cell body into, get on mould silica-gel mixture that one piece of gauze is put in the second square groove, fill mould silica-gel mixture again, take out in the second square groove after mould silica-gel mixture parches, remove the parget water crystal column be wrapped in the middle of mould silica-gel mixture, obtain silica gel crystal column mould;
3) red resin crystal column is made
Cobalt iso-octoate is added in crystal resin, the weight ratio of crystal resin and cobalt iso-octoate is 100:0.5, stir, add mill base, the weight ratio of crystal resin and mill base is 100:0.01, add methyl ethyl ketone peroxide again to stir, the weight ratio of crystal resin and methyl ethyl ketone peroxide is 100:1.8, leave standstill 10 minutes automatic froth breakings, obtain crystal resin mixture, poured into by crystal resin mixture in silica gel crystal column mould, crystal resin mixture solidifies taking-up after 2 hours completely, obtains resin crystal column;
4) red artificial water druse is made
The red resin crystal column of different size is bonded together by a crystal bunch growthform, obtains artificial red crystal bunch, wherein, binding agent used is the mixture of crystal resin, cobalt iso-octoate and methyl ethyl ketone peroxide 100:0.5:1.5 in mass ratio.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (5)
1. a preparation method for synthetic quartz bunch, is characterized in that, comprising:
1) parget water crystal column is made
Long 150-200mm is surrounded, wide 20mm-30mm, first square groove of high 20-30mm with 5mm acrylic board or 5 lis of plates, land plaster adds water mixing, pours in the first square groove, takes out after sclerosis, accomplish with cutter six prisms that one end is hexagonal pyramid shape, obtain parget water crystal column;
2) silica gel crystal column mould is made
Surround long 200-250mm, wide 30-35mm with 5mm acrylic board or 5 lis of plates, second square groove of high 30-35mm, 1) the parget water crystal column that obtains is coated with the thick releasing agent of 0.2-0.5mm, after coating, parget water crystal column is lain in the center of the second square groove,
Mould silica gel adds curing agent and stirs, obtain mould silica-gel mixture, by mould silica-gel mixture indwelling ten minutes automatic froth breakings or vacuumize three minutes, with brush the mould silica-gel mixture brushing after froth breaking or after vacuumizing or be filled in the second square groove, pour the long-pending half of second party cell body into, get on mould silica-gel mixture that one piece of gauze is put in the second square groove, fill mould silica-gel mixture again, take out in the second square groove after mould silica-gel mixture parches, remove the parget water crystal column be wrapped in the middle of mould silica-gel mixture, obtain silica gel crystal column mould,
3) resin crystal column is made
In crystal resin, add promoter, stir, then add curing agent and stir, leave standstill 2-10 minute automatic froth breaking, obtain crystal resin mixture, crystal resin mixture is poured in silica gel crystal column mould, take out after crystal resin mixture solidifies completely, obtain resin crystal column;
4) artificial water druse is made
The resin crystal column of different size is bonded together by a crystal bunch growthform, obtains synthetic quartz bunch, wherein, binding agent used is the mixture of crystal resin, promoter and curing agent.
2. preparation method according to claim 1, it is characterized in that, 1) make in parget water crystal column, described one end is six prisms length of hexagonal pyramid shape is 50-180mm, inscribed circle diameter is 10-30mm, the height of hexagonal pyramid accounts for the 1/10-1/5 that one end is six prism length of hexagonal pyramid shape, and the weight ratio of described land plaster and water is (1.2-1.4): 1.
3. preparation method according to claim 1 and 2, is characterized in that, 2) make in silica gel crystal column mould, described releasing agent is liquid detergent, does not need to be watered when being coated with parget water crystal column.
4. preparation method according to claim 3, is characterized in that, 2) make in silica gel crystal column mould, the weight ratio of described mould silica gel and curing agent is 100:(1-2), described curing agent is platinum catalyst.
5. preparation method according to claim 4, it is characterized in that, 3) make resin crystal column and 4) make in artificial water druse, the weight ratio of described crystal resin and promoter is 100:(0.3-0.5), the weight ratio of described crystal resin and curing agent is 100:(1.5-3), described curing agent is methyl ethyl ketone peroxide, and described promoter is cobalt iso-octoate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510018920.0A CN104690861B (en) | 2015-01-14 | 2015-01-14 | Preparation method of artificial crystal cluster |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510018920.0A CN104690861B (en) | 2015-01-14 | 2015-01-14 | Preparation method of artificial crystal cluster |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104690861A true CN104690861A (en) | 2015-06-10 |
| CN104690861B CN104690861B (en) | 2017-02-22 |
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| CN201510018920.0A Expired - Fee Related CN104690861B (en) | 2015-01-14 | 2015-01-14 | Preparation method of artificial crystal cluster |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1554525A (en) * | 2003-12-25 | 2004-12-15 | 勇 余 | Method for producing crystal art funniture |
| CN1597360A (en) * | 2004-08-02 | 2005-03-23 | 李翠华 | Manufacturing process of ornament or artificial quartz crystal relief wall painting |
| CN101182386A (en) * | 2006-11-13 | 2008-05-21 | 天津市世纪东方建筑景观雕塑技术开发中心 | Method for making chromatic composite glass embossing |
| CN103895440A (en) * | 2014-03-24 | 2014-07-02 | 东北电力大学 | Fabricating process of sandstone-embossment-imitated large seamless mural |
-
2015
- 2015-01-14 CN CN201510018920.0A patent/CN104690861B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1554525A (en) * | 2003-12-25 | 2004-12-15 | 勇 余 | Method for producing crystal art funniture |
| CN1597360A (en) * | 2004-08-02 | 2005-03-23 | 李翠华 | Manufacturing process of ornament or artificial quartz crystal relief wall painting |
| CN101182386A (en) * | 2006-11-13 | 2008-05-21 | 天津市世纪东方建筑景观雕塑技术开发中心 | Method for making chromatic composite glass embossing |
| CN103895440A (en) * | 2014-03-24 | 2014-07-02 | 东北电力大学 | Fabricating process of sandstone-embossment-imitated large seamless mural |
Non-Patent Citations (2)
| Title |
|---|
| 张军，马丽丽: "《立体构成》", 31 July 2012, 北京大学出版社 * |
| 张玉龙，李长德: "《塑料配方与制备手册》", 31 January 2005, 化学工业出版社 * |
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| CN104690861B (en) | 2017-02-22 |
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Granted publication date: 20170222 |