CN104687904A - Preparation method for sedative and dormitive silk quilt - Google Patents
Preparation method for sedative and dormitive silk quilt Download PDFInfo
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- CN104687904A CN104687904A CN201510133668.8A CN201510133668A CN104687904A CN 104687904 A CN104687904 A CN 104687904A CN 201510133668 A CN201510133668 A CN 201510133668A CN 104687904 A CN104687904 A CN 104687904A
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Abstract
The invention relates to a preparation method for a sedative and dormitive silk quilt. The preparation method comprises the following steps of soaking silk floss by using sedative and dormitive treating agents for 30-55 minutes under the conditions that the temperature is 50-60 DEG C and the bath ratio is 1:8-10; spin-drying the silk floss; drying the silk floss; and making a quilt to obtain the sedative and dormitive silk quilt. Pharmacologically, the microcapsule treating agents have effects of soothing the nerves, treating insomnia, promoting blood circulation, killing ants, mosquitoes, cockroaches and mites, restraining diseases such as hypertension, allergic rhinitis and asthma and improving appetite.
Description
Technical field
The invention belongs to the preparation field of functional silk quilt, particularly a kind of preparation method of calming soporific silk quilt.
Background technology
Silk quilt mainly with natural mulberry silk and (or) tussah silk for raw material processes from strand.Because it is rich in several amino acids, there is good hygroscopicity and warmth retention property simultaneously.Human body uses silk quilt to have effect of care skin, green health, promotion sleep, illness prevention and fitness.According to China silk association statistics, the sales volume of silk quilt just with annual 20% ~ 30% speed sustainable growth.Along with the raising of Living consumption, the parent that silk quilt is more and more subject to consumer looks at.
Silk quilt generally makes of raw materials such as mulberry silk, cassava silkwormsilk, tussah silks.Mulberry silk originates in south mostly, and be the silk extracted out from the cocoon of silkworm knot, this silk color and luster is snow-white, and silk is fine and soft soft, and feel is comfortable.Tussah silk originates in the north mostly, and be that tussah cocoon is produced, tussah belongs to wild silkworm, compares with mulberry silk, and the color of tussah silk is deep, and its primitive color is light brown, and tussah silk silk quality is comparatively hard, and warming I life can be similar with mulberry silk, but price is more cheap.Cassava silkwormsilk gloss does not have mulberry silk white, and in rice white, silk is more fluffy, and silk is short.
Mulberry silk for making silk quilt can be divided into again manual mulberry silk and machine-processed mulberry silk.The former draws cocoon and makes, long service life by hand, but adds man-hour, and waste time and energy, work efficiency is not high, and price is relatively high; The latter is that machine makes, and through specially treated, silk is shorter, and service life is shorter than manual silk, but production cost is low, and efficiency is high, price material benefit, and designer-label store generally will accomplish scale production, the machine-processed mulberry silk of most employing.Draw silk because manual, have the skin of silkworm chrysalis to leave over unavoidably, from the color and luster of silk, manual silk is slightly yellow, has stain; Mechanism silk is relatively white, and machine-processed silk is generally sliding than manual silk feel.From uniformity coefficient, in machine-processed silk production process, there will be a bit thick rib unavoidably, but measure considerably less; And manual silk may have some raw blocks (silkworm cocoon do not boiled extremely individually stays).Due to also uncomfortable at the beginning to new silk quilt, may think that manual silk also can the taste of a little silkworm chrysalis, but can not affect the health of human body, airing will disappear for several days.
Silk quilt on market mainly contains plain edition silk quilt and functional silk quilt by Function Classification.To succeed in developing in recent years and the functional silk quilt kind produced in batches mainly contains: one is exempt from turnover function silk quilt.Silk cocoon is adopted vacuum infiltration, expanded cocoon cooking technology, replace the processing method that the cocoon cooking of tradition soda ash is come unstuck, process continuous for expanded silk through increase elasticity and soft hindlimb unload again, effectively can prevent from not gluing also between silk fiber, tangling, finally realize silk quilt and exempt from turnover function.Two is have antibacterial, deodorization, mildew-resistant, antipruritic health silk quilt.Silk silk floss is carried out anti-bacteria health finishing, make it have high antibacterial, deodorization, mildew-resistant, itching-relieving action, that effectively can improve silk quilt takes wholesomeness, can eliminate and weaken the harm of bacterium to human body skin, has catered to the demand of taking wholesomeness class lifting of people to bedroom cover.Three is the silk quilts having stimulating circulation, improve immune disease-resistance function.Adopt anion and far infrared dual-use function to arrange to silk silk floss, can not only make to produce abundant anion in bedroom, thus keep room air fresh; And owing to carrying out far infrared after-finishing to silk silk floss, and far infrared has very strong penetration power, may penetrate into subcutis, cause resonance cell, thus make to produce thermogenetic effect in body, strengthen blood microcirculation, enhance metabolism, improve the ability that human immunity is disease-resistant.Four is aromatic function silk quilts.Aromatic micro-capsule Final finishing is carried out to silk silk floss, under certain physical action (human body and silk quilt contact friction and stretching), is made the fragrance slow releasing of essence by the wall micropore of microcapsules, make silk quilt give out light, graceful fragrance.The pure and fresh gracefulness of lavender (Lavender) fragrance, character is gentle.Lavender is rich in volatile oil, cumarin, tannin, flavonoids etc., and complete stool can be used, especially bud part, connects stem band leaf by flower fringe cut off at duration of flowering, and can be used for each side such as the cooking, medicinal, beauty treatment, purposes is extremely wide.Namely roman and Persians understand very early and utilize fresh lavender to do aromatic bath, use dispelling fatigue and ache, and get spirit and QI cleaning all over the body in return.Lavender is also often used as beauty treatment and anti-inflammatory articles for use, using steaming face, having effect of cleaning skin, anti-inflammatory and balanced fat secretion as immersed in hot water by fresh lavender; Or fried juice applies spatula wound, lacerated wound etc., can prevent to infect and inflammation.
The stem (defoliation) of the wounded in the battle fringe of lavender is then applied to flower arrangement, bouquet etc., or is bundled into lavender and holds in both hands, and replaces camphor ball to be placed on stacte in cabinet and to hold concurrently expelling parasite.Put into dry lavandulae flos during shower in the hot water, can body warmer be made and help for sleep.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of preparation method of calming soporific silk quilt, the present invention is pharmacologically, this microcapsules inorganic agent has stable nerve, Cure for insomnia, stimulates circulation, except ant, except mosquito, except roach, except the diseases such as mite, suppression hypertension, nose sensitivity, asthma, effect of whetting the appetite.
The preparation method of a kind of calming soporific silk quilt of the present invention, comprising:
Silk floss is flooded calming soporific inorganic agent, dip time 30 ~ 55min, temperature 50 ~ 60 DEG C, bath raio is 1:8-10, dries, and dry, quilt processed, obtains calming soporific silk quilt; Wherein calming soporific inorganic agent component is: Lavender microcapsule 3.5%-5%OWF, adhesive 30-40g/L, penetrating agent JFC 5g/L.
Being prepared as of described silk floss: stripping cocoon, open silk floss, soap, come unstuck, oil removing, dehydration, oven dry, obtain silk floss.
The preparation method of described Lavender microcapsule is:
The preparation of O/w emulsion: lavender is dissolved in organic solvent by (1), adds oil soluble reaction monomer, emulsifying agent, forms oil phase; Water-based reaction monomers will be added in distilled water, form aqueous phase; By aqueous phase and oil phase mixing, obtain emulsion;
Coated: emulsion proceeds in reactor by (2), adds catalyst, to bring out two kinds of monomer reactions, stirring reaction 1-2h, the polymer that monomer reaction generates is coated by active ingredient;
Solidification: (3) add cure-crosslinking agent by step (2), continues to stir 0.5-2h, obtains Lavender microcapsule.
In described step (1), organic solvent is the one in carrene, cyclohexanone, ethyl acetate; The mass ratio of lavender and organic solvent is 1:1.
Described step (1) oil-soluble reaction monomers is the one in 2,4 toluene di-isocyanate(TDI)s, 2,6 toluene di-isocyanate(TDI)s; The mass ratio of oil soluble reaction monomer and lavender is 1:1-1.5.
In described step (1), emulsifying agent is PVAC polyvinylalcohol; The mass ratio of emulsifying agent and lavender is 4-5:1.
In described step (1), water-based reaction monomers is polyethylene glycol PEG, and molecular weight is 400; The mass ratio of water-based reaction monomers and lavender is 4-5:1.
In described step (2), catalyst is dibutyl tin dilaurate, and consumption is 0.02% of oil soluble reaction monomer molar quality; Cure-crosslinking agent is ethylenediamine or benzenediol; The consumption of cure-crosslinking agent is the 5%-10% of oil soluble reaction monomer mass.
Described bake out temperature is 80-95 DEG C, and the time is 15-20min.
Described system by process is: weigh, wire drawing, encapsulation, quilting.
Described penetrating agent JFC is sec-octyl alcohol APEO, and structural formula is C
8h1
7(CH
2cH
2o) nH, n=1 ~ 6.
Described OWF refers to silk quilt weight.
In described calming soporific inorganic agent, adhesive can be chosen any one kind of them commercial polyurethanes low-temperature adhesive.
beneficial effect
Gained calming soporific silk quilt of the present invention it can stabilize mood, so have the effect in front to not normal psychological condition; Can purification, pacify soul, alleviate indignation and beaten sensation, make people can even-tempered and good-humouredly in the face of life because its can centre of equilibrium nerve, so helpful to alarmed and dejected state; Also have significantly tranquil and function of releiving, have goodish easypro putting to console with spirit to insomniac;
Because the finishing agent of silk quilt is microcapsules, its slow release characteristic, it is made to have the effect of long-term treatment and prevention, and there will not be any too lax phenomenon, people's calmness and balance can also be given, make that there is stable and efficient job morale, for pacify hot-tempered enter or moody temper have goodish effect, simultaneously to nervous large, irritated with pressure time the hypertension that causes have the effect of relaxing smooth muscle of releiving;
Pharmacologically, this microcapsules inorganic agent has stable nerve, Cure for insomnia, stimulates circulation, except ant, except mosquito, except roach, except the diseases such as mite, suppression hypertension, nose sensitivity, asthma, effect of whetting the appetite.
Detailed description of the invention
Below in conjunction with specific embodiment, set forth the present invention further.Should be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.In addition should be understood that those skilled in the art can make various changes or modifications the present invention, and these equivalent form of values fall within the application's appended claims limited range equally after the content of having read the present invention's instruction.
Embodiment 1
The preparation process of calming soporific function silk quilt mainly comprises: system is continuous, arrangement, quilt processed.Concrete technology is as follows:
(1) system is continuous: stripping cocoon, open silk floss, soap, come unstuck, oil removing, dehydration, oven dry, obtain silk floss
(2) arrange: silk floss is flooded calming soporific inorganic agent (Lavender microcapsule 3.5%OWF, adhesive 40g/L, penetrating agent JFC 5g/L; bath raio 1:8, dip time 30min, temperature 60 C); dry, dry (80 DEG C, 15min).Wherein, Lavender microcapsule preparation technology is as follows:
1. the preparation of O/w emulsion
By lavender in mass ratio 1:1 be dissolved in carrene; Add 2,4 toluene di-isocyanate(TDI)s (consumption is 1.2 times of lavender quality), polyvinyl alcohol (PVA) (consumption is 4.5 times of lavender quality), form oil phase; Measure 100L distilled water, and add PEG400 (PEG400) (consumption is 4 times of lavender) wherein, form aqueous phase; Water-oil phase is mixed, shakes up;
2. coated
O/w emulsion is proceeded in reaction ax, add catalyst dibutyl tin dilaurate 0.02% (corresponding 2, the molar percentage of 4 toluene di-isocyanate(TDI)s) while stirring, to bring out two kinds of monomer reactions, continue to stir 2h, the polymer that monomer reaction generates is coated by active ingredient;
3. solidify
Add cure-crosslinking agent ethylenediamine (consumption is 5% of isocyanates), continue to stir 1h, obtain Lavender microcapsule.
(3) quilt processed: weigh, wire drawing, encapsulation, quilting, inspection, packaging, finished product
Embodiment 2
The preparation process of calming soporific function silk quilt mainly comprises: system is continuous, arranges, quilt processed.Concrete technology is as follows:
(1) system is continuous: stripping cocoon, opens silk floss, soaps, come unstuck, oil removing, dehydration, dry, silk floss
(2) arrange: silk floss, dipping calming soporific inorganic agent (Lavender microcapsule 4.5%OWF, adhesive 35g/L, penetrating agent JFC 5g/L, bath raio 1:10, dip time 50min, temperature 55 DEG C), dry (90 DEG C, 15min).Wherein, Lavender microcapsule preparation technology is as follows:
1. the preparation of O/w emulsion
By lavender in mass ratio 1:1 be dissolved in cyclohexanone; Add 2,4 toluene di-isocyanate(TDI)s (consumption is 1.5 times of lavender quality), polyvinyl alcohol (PVA) (consumption is 5 times of lavender quality), form oil phase; Measure 100L distilled water, and add PEG400 (PEG400) (consumption is 4 times of lavender) wherein, form aqueous phase; Water-oil phase is mixed, shakes up;
2. coated
O/w emulsion is proceeded in reaction ax, add catalyst dibutyl tin dilaurate 0.02% (corresponding 2, the molar percentage of 4 toluene di-isocyanate(TDI)s) while stirring, to bring out two kinds of monomer reactions, continue to stir 2h, the polymer that monomer reaction generates is coated by active ingredient;
3. solidify
Add cure-crosslinking agent ethylenediamine (consumption is 8% of isocyanates), continue to stir 1h, obtain Lavender microcapsule.
(3) quilt processed: weigh, wire drawing, encapsulation, quilting, inspection, packaging, finished product
Embodiment 3
The preparation process of calming soporific function silk quilt mainly comprises: system is continuous, arranges, quilt processed.Concrete technology is as follows:
(1) system is continuous: stripping cocoon, opens silk floss, soaps, come unstuck, oil removing, dehydration, dry, silk floss
(2) arrange: silk floss, dipping calming soporific inorganic agent (Lavender microcapsule 4.0%OWF, adhesive 40g/L, penetrating agent JFC 5g/L, bath raio 1:8, dip time 40min, temperature 60 C), dry (80 DEG C, 20min).Wherein, Lavender microcapsule preparation technology is as follows:
1. the preparation of O/w emulsion
By lavender in mass ratio 1:1 be dissolved in ethyl acetate; Add 2,6 toluene di-isocyanate(TDI)s (consumption is 1.2 times of lavender quality), polyvinyl alcohol (PVA) (consumption is 4.5 times of lavender quality), form oil phase; Measure 100L distilled water, and add PEG400 (PEG400) (consumption is 4 times of lavender) wherein, form aqueous phase; Water-oil phase is mixed, shakes up;
2. coated
O/w emulsion is proceeded in reaction ax, add catalyst dibutyl tin dilaurate 0.02% (corresponding 2, the molar percentage of 6 toluene di-isocyanate(TDI)s) while stirring, to bring out two kinds of monomer reactions, continue to stir 2h, the polymer that monomer reaction generates is coated by active ingredient;
3. solidify
Add cure-crosslinking agent ethylenediamine (consumption is 5% of isocyanates), continue to stir 1h, obtain Lavender microcapsule.
(3) quilt processed: weigh, wire drawing, encapsulation, quilting, inspection, packaging, finished product
Embodiment 4
The preparation process of calming soporific function silk quilt mainly comprises: system is continuous, arranges, quilt processed.Concrete technology is as follows:
(1) system is continuous: stripping cocoon, opens silk floss, soaps, come unstuck, oil removing, dehydration, dry, silk floss
(2) arrange: silk floss, dipping calming soporific inorganic agent (Lavender microcapsule 5%OWF, adhesive 35g/L, penetrating agent JFC 5g/L, bath raio 1:10, dip time 45min, temperature 55 DEG C), dry (85 DEG C, 20min).Wherein, Lavender microcapsule preparation technology is as follows:
1. the preparation of O/w emulsion
By lavender in mass ratio 1:1 be dissolved in carrene; Add 2,4 toluene di-isocyanate(TDI)s (consumption is 1.3 times of lavender quality), polyvinyl alcohol (PVA) (consumption is 5 times of lavender quality), form oil phase; Measure 100L distilled water, and add PEG400 (PEG400) (consumption is 4 times of lavender) wherein, form aqueous phase; Water-oil phase is mixed, shakes up;
2. coated
O/w emulsion is proceeded in reaction ax, add catalyst dibutyl tin dilaurate 0.02% (corresponding 2, the molar percentage of 4 toluene di-isocyanate(TDI)s) while stirring, to bring out two kinds of monomer reactions, continue to stir 2h, the polymer that monomer reaction generates is coated by active ingredient;
3. solidify
Add cure-crosslinking agent ethylenediamine (consumption is 6% of isocyanates), continue to stir 1h, obtain Lavender microcapsule.
(3) quilt processed: weigh, wire drawing, encapsulation, quilting, inspection, packaging, finished product.
Claims (10)
1. a preparation method for calming soporific silk quilt, comprising:
Silk floss is flooded calming soporific inorganic agent, dip time 30 ~ 55min, temperature 50 ~ 60 DEG C, bath raio is 1:8-10, dries, and dry, quilt processed, obtains calming soporific silk quilt; Wherein calming soporific inorganic agent component is: Lavender microcapsule 3.5%-5%OWF, adhesive 30-40g/L, penetrating agent JFC 5g/L.
2. the preparation method of a kind of calming soporific silk quilt according to claim 1, is characterized in that: being prepared as of described silk floss: stripping cocoon, open silk floss, soap, come unstuck, oil removing, dehydration, oven dry, obtain silk floss.
3. the preparation method of a kind of calming soporific silk quilt according to claim 1, it is characterized in that: the preparation method of Lavender microcapsule is: lavender is dissolved in organic solvent by (1), add oil soluble reaction monomer, emulsifying agent, form oil phase; Water-based reaction monomers will be added in distilled water, form aqueous phase; By aqueous phase and oil phase mixing, obtain emulsion; (2) proceed in reactor by emulsion, add catalyst, stirring reaction 1-2h, then adds cure-crosslinking agent, continues to stir 0.5-2h, obtains Lavender microcapsule.
4. the preparation method of a kind of calming soporific silk quilt according to claim 3, is characterized in that: in described step (1), organic solvent is the one in carrene, cyclohexanone, ethyl acetate; The mass ratio of lavender and organic solvent is 1:1.
5. the preparation method of a kind of calming soporific silk quilt according to claim 3, is characterized in that: described step (1) oil-soluble reaction monomers is the one in 2,4 toluene di-isocyanate(TDI)s, 2,6 toluene di-isocyanate(TDI)s; The mass ratio of oil soluble reaction monomer and lavender is 1:1-1.5.
6. the preparation method of a kind of calming soporific silk quilt according to claim 3, is characterized in that: in described step (1), emulsifying agent is PVAC polyvinylalcohol; The mass ratio of emulsifying agent and lavender is 4-5:1.
7. the preparation method of a kind of calming soporific silk quilt according to claim 3, is characterized in that: in described step (1), water-based reaction monomers is polyethylene glycol PEG, and molecular weight is 400; The mass ratio of water-based reaction monomers and lavender is 4-5:1.
8. the preparation method of a kind of calming soporific silk quilt according to claim 3, is characterized in that: in described step (2), catalyst is dibutyl tin dilaurate, and consumption is 0.02% of oil soluble reaction monomer molar quality; Cure-crosslinking agent is ethylenediamine or benzenediol; The consumption of cure-crosslinking agent is the 5%-10% of oil soluble reaction monomer mass.
9. the preparation method of a kind of calming soporific silk quilt according to claim 1, it is characterized in that: described bake out temperature is 80-95 DEG C, the time is 15-20min.
10. the preparation method of a kind of calming soporific silk quilt according to claim 1, is characterized in that: described system by process is: weigh, wire drawing, encapsulation, quilting.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510133668.8A CN104687904A (en) | 2015-03-25 | 2015-03-25 | Preparation method for sedative and dormitive silk quilt |
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|---|---|---|---|
| CN201510133668.8A CN104687904A (en) | 2015-03-25 | 2015-03-25 | Preparation method for sedative and dormitive silk quilt |
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| CN105133181A (en) * | 2015-07-20 | 2015-12-09 | 黄文丰 | Manufacturing method for tension cotton and product thereof |
| CN106377122A (en) * | 2016-08-30 | 2017-02-08 | 江西金铭丝绸有限公司 | Preparation method of silk quilt |
| CN107034682A (en) * | 2017-04-13 | 2017-08-11 | 段体奎 | Silk quilt that a kind of microcapsules technology lifting amino acid is fully absorbed and preparation method thereof |
| CN107513864A (en) * | 2017-08-10 | 2017-12-26 | 宁波广源纺织品有限公司 | A kind of lavender oil microcapsules dressing liquid and its application |
| CN113235308A (en) * | 2021-05-08 | 2021-08-10 | 江西钱皇丝绸制品有限公司 | Silk for relieving muscle and joint pain and preparation method and application thereof |
| CN115262214A (en) * | 2022-08-09 | 2022-11-01 | 浙江钱皇网络科技股份有限公司 | Method for manufacturing silk quilt with effects of improving sleep and aiding sleep |
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| CN113235308A (en) * | 2021-05-08 | 2021-08-10 | 江西钱皇丝绸制品有限公司 | Silk for relieving muscle and joint pain and preparation method and application thereof |
| CN115262214A (en) * | 2022-08-09 | 2022-11-01 | 浙江钱皇网络科技股份有限公司 | Method for manufacturing silk quilt with effects of improving sleep and aiding sleep |
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Application publication date: 20150610 |