CN102268326B - Slow-release controllable lavender essential oil microcapsule and preparation method thereof as well as finishing agent and application thereof - Google Patents
Slow-release controllable lavender essential oil microcapsule and preparation method thereof as well as finishing agent and application thereof Download PDFInfo
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- CN102268326B CN102268326B CN201010618460.2A CN201010618460A CN102268326B CN 102268326 B CN102268326 B CN 102268326B CN 201010618460 A CN201010618460 A CN 201010618460A CN 102268326 B CN102268326 B CN 102268326B
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Abstract
The invention discloses a slow-release controllable lavender essential oil microcapsule. The microcapsule is characterized in that the capsule wall of the microcapsule is made of melamine resin; and the capsule core of the microcapsule is formed by mixing lavender essential oil and a system regulator with water. The invention also discloses a preparation method of the slow-release controllable lavender essential oil microcapsule, a finishing agent prepared by utilizing the slow-release controllable lavender essential oil microcapsule as well as a post-treatment method of fabric by using the finishing agent. The invention further discloses application of the finishing agent in home textile products. According to the invention, a function of high-efficiency long-term slowly releasing the lavender essential oil can be achieved; a health care function is given to pillows and bedclothes; a development way of lavender essential oil treatment is effectively broadened; and post-finishing is carried out on the fabric by using a decal, and the fastness of the microcapsule can be improved, thereby ensuring the achievement of slow release of lavender essential oil in a product. By using the slow-release controllable lavender essential oil microcapsule, a good help can be provided for large pressure and unstable mood of people in daily life, and a convenient and effective health care method is provided for people having no time to consider own bodies due to busy work.
Description
Technical field
The present invention relates to the controlled Lavender microcapsules of a kind of slowly-releasing, finishing agent and its preparation method and application this finishing agent and fabric is carried out to the method for rear arrangement, and the application of the controlled Lavender microcapsule dressing agent of this slowly-releasing in the home textile products such as sheet, pillowcase.
Background technology
The pure and fresh gracefulness of lavender fragrance, character is gentle, is rich in volatile oil, cumarin, tannin, flavonoids etc., and complete stool can be used, and especially bud part, connects stem band leaf at duration of flowering flower fringe is cut off, and can be used for cooking, the each side such as medicinal, beauty treatment, and purposes is extremely wide.Roman and Persians understand very early and utilize fresh lavender to do aromatic bath, use and eliminate tired and ache, and get spirit and QI cleaning all over the body in return.Lavender is also often used as beauty treatment and anti-inflammatory articles for use, as fresh lavender is immersed in hot water and uses steaming face, has the effect of cleaning skin, anti-inflammatory and balanced fat secretion; Or the deposited spatula wound of fried juice, lacerated wound etc., can prevent to infect and inflammation.China's the Tang Dynasty " king of medicine " Sun Simiao finds that " Chinese medicine lavender " has fancy effect to improving insomnia, by the practice of practising medicine of gathering medicinal herbs for many years, finally develop the Chinese medicinal pillow that insomnia is had to excellent effect, it is with significant prevention effect and result for the treatment of, and by the successive dynasties, the world of medicine is approved.Because lavender character and human skin character approach, the very trickle very easily infiltration of its ingredient, and be completely absorbed, so can promote cellular metabolism, reparation, maintenance, acceleration regenerative cell, reach the anti-ageing whole body tight muscle that stimulates circulation and releive, eliminate fatigue,, the refuse in body and toxin can be excreted by lymphatic system meanwhile.In addition, lavender maintains mental health except treating some diseases, the more important thing is, the mood of releiving meets the requirement of modern to physiology and mental health.
Lavender is widely applied in beauty treatment Jie He the world of medicine at present, but in home textile product, is not applied.If can be by combinations such as lavender and home textile product pillow, sheets, lavender material just can act on human body by following approach: the one, and the ion that sucks lavender gas by mouth and nose reaches " Wen Xiang cures the disease "; The 2nd, lavender effective ingredient, by head, skin of neck pore, absorbs and enters human body blood vessels through slow-release transdermal, plays a role; The 3rd, during sleep, by body temperature, evaporate, impel lavender active ingredient to slowly release, be absorbed by the body, tranquilizing the mind, supports brain sleeping, fundamentally repairs impaired sleep nervous system, makes human body recover natural sleep state.The long-term pillow and sheet delaying sanility, enhancing immune function of human body that distributes lavender fragrance that use, to high blood pressure, coronary heart disease, cervical spondylopathy, neurosis, various rheumatism paralysis, cerebral hemorrhage and cerebral embolism sequela etc., have obvious therapeutic action.Thereby wish to have a kind of method that lavender and home textile product are combined and obtain the home textile product of various beneficial effects.
Summary of the invention
One of technical problem to be solved by this invention is to provide the controlled Lavender microcapsules of a kind of slowly-releasing, and the controlled Lavender microcapsules of this slowly-releasing, when being heated, can slowly distribute Lavender fugitive constituent.
Two of technical problem to be solved by this invention is to provide the preparation method of the controlled Lavender microcapsules of above-mentioned slowly-releasing.
Three of technical problem to be solved by this invention is to provide the finishing agent that the controlled Lavender microcapsules of a kind of above-mentioned slowly-releasing are prepared.
Four of technical problem to be solved by this invention is to provide above-mentioned finishing agent and fabric is carried out to the method for rear arrangement.
Five of technical problem to be solved by this invention is to provide the application of above-mentioned finishing agent in home textile product.
The controlled Lavender microcapsules of a kind of slowly-releasing as first aspect present invention, is characterized in that, described capsule wall is prepared from by melamine resin, and capsule core is mixed by the raw material of following percentage by weight:
Lavender 20%-30%
System modifier MS 10%～20%
Water surplus.
The preparation method of described system modifier MS is as follows: first by maleic anhydride and styrene monomer, polymerization in acetone soln obtains polymer acetone soln, again polymer acetone soln is distributed in the aqueous solution containing ammonium hydroxide and is neutralized, become ammonium carboxylate salt, obtain system modifier MS after removing aqueous acetone solution.
Preparation method as the controlled Lavender microcapsules of a kind of slowly-releasing of second aspect present invention, comprises the following steps:
A. by Lavender, system modifier, water in high shearing mixing emulsor high speed homogenising, under the condition stirring, add the melamine resin of Lavender weight 1.5%～3.0%, be warming up to 55 ℃, be incubated 1～2 hour, carry out individual layer wall building;
B, the system of steps A is cooled to after normal temperature, under the condition stirring, adds the melamine resin of Lavender weight 1.5%～3.0%, be warming up to 65 ℃, be incubated 2 hours, carry out double-deck wall building;
C. be then warming up to 80 ℃, add 1 of Lavender weight 2.0%-5.0%, 6-hexamethylene diamine carries out three layers of wall building.
The finishing agent that the controlled Lavender microcapsules of a kind of above-mentioned slowly-releasing of third aspect present invention are prepared, is characterized in that, formulated by the raw material of following percentage by weight:
Lavender microcapsules 10%～30%;
Aqueous polyurethane coating mill base 5%-10%;
Low-temperature adhesive 20%～30%;
Thickener 1%～2%;
Water surplus.
Described low-temperature adhesive is KG-101 low temperature COAT PRINTING composite adhesives.
Described thickener is AM-535 hydrophobically modified association type anion base swelling thickener.
The finishing agent that utilizes the controlled Lavender microcapsules of slowly-releasing to prepare of fourth aspect present invention carries out the method for rear arrangement to fabric, comprise following steps:
A, stamp step
Adopt common process to be printed on fabric described finishing agent;
B, baking step
The fabric producing is dried at 50～90 ℃;
C, tentering step
The fabric of oven dry is carried out to tentering to finished product at 100～105 ℃.
The application of the finishing agent of fifth aspect present invention in home textile product, is wherein characterised in that, described home textile product is to be made and formed by the fabric after described finishing agent is processed.
Described home textile product is sheet, pillowcase, quilt cover, curtain or tablecloth.
The present invention is by preparing the controlled Lavender microcapsules of slowly-releasing, and then preparation is containing the finishing agent of the controlled Lavender microcapsules of slowly-releasing, and utilize this finishing agent to carry out rear arrangement to fabric, after arrangement, obtain fabric and be sewn into the home textile products such as sheet, pillowcase, quilt cover, curtain or tablecloth, can realize the function of efficient, long-term slowly-releasing Lavender; Pillow, sheet health care have been given; Effectively widened the evolutionary path of lavender treatment.Adopt Decal to carry out rear arrangement to fabric, can improve the fastness of microcapsules, guarantee that the Lavender of product reaches the function of slow release.To solving the large and emotional lability of pressure in people's daily life, provide good help, for have no time to attend to the people of own health because being busy with one's work, provide a kind of convenient, effective health-care method.It is more washable that the present invention spins articles for use than existing family.
The specific embodiment
In order to make technological means of the present invention, creation characteristic, reach object and effect is easy to understand, below in conjunction with embodiment, further set forth the present invention, but embodiments of the present invention are not limited to this.
Embodiment 1
Lavender 20g, system modifier MS10g and 70g water, in high shearing mixing emulsor high speed homogenising, are added to the melamine resin of 0.3g under the condition stirring, be warming up to 55 ℃, be incubated 1.5 hours, carry out individual layer wall building; System is cooled to after normal temperature, under the condition stirring, adds the melamine resin of 0.3g, be warming up to 65 ℃, be incubated 2 hours, carry out double-deck wall building; Then be warming up to 80 ℃, add 0.6g1,6-hexamethylene diamine carries out three layers of wall building and obtains the controlled Lavender microcapsules of slowly-releasing.
Embodiment 2
Lavender 25g, system modifier MS15g and 60g water, in high shearing mixing emulsor high speed homogenising, are added to the melamine resin of 0.5g under the condition stirring, be warming up to 55 ℃, be incubated 1 hour, carry out individual layer wall building; System is cooled to after normal temperature, under the condition stirring, adds the melamine resin of 0.5g, be warming up to 65 ℃, be incubated 1 hour, carry out double-deck wall building; Then be warming up to 80 ℃, add 0.75g1,6-hexamethylene diamine carries out three layers of wall building and obtains the controlled Lavender microcapsules of slowly-releasing.
Embodiment 3
Lavender 30g, system modifier MS20g and 50g water, in high shearing mixing emulsor high speed homogenising, are added to the melamine resin of 0.9g under the condition stirring, be warming up to 55 ℃, be incubated 2 hours, carry out individual layer wall building; System is cooled to after normal temperature, under the condition stirring, adds the melamine resin of 0.9g, be warming up to 65 ℃, be incubated 2 hours, carry out double-deck wall building; Then be warming up to 80 ℃, add 1.2g1,6-hexamethylene diamine carries out three layers of wall building and obtains the controlled Lavender microcapsules of slowly-releasing.
Embodiment 4
Take the Lavender microcapsules 10kg, the aqueous polyurethane coating mill base 5kg that according to embodiment 1 method, prepare; KG-101 low temperature COAT PRINTING composite adhesives 20kg, AM-535 hydrophobically modified association type anion base swelling thickener thickener 1kg, prepare finishing agent after adding water to 100kg after mixing.
Utilize the finishing agent of preparation to carry out rear arrangement to cotton, rear arrangement process is: after stamp, oven dry, tentering, obtain finished product.Wherein in drying course, temperature is 70 ℃, and in tentering process, temperature is 102 ℃.In the cotton obtaining, the content of Lavender microcapsules is every square metre of cotton 5g-10g gram.
Embodiment 5
Take the Lavender microcapsules 20kg, the aqueous polyurethane coating mill base 8kg that according to embodiment 2 methods, prepare; KG-101 low temperature COAT PRINTING composite adhesives 25kg, AM-535 hydrophobically modified association type anion base swelling thickener thickener 1.5kg, prepare finishing agent after adding water to 100kg after mixing.
Utilize the finishing agent of preparation to carry out rear arrangement to cotton, rear arrangement process is: after stamp, oven dry, tentering, obtain finished product.Wherein in drying course, temperature is 60 ℃, and in tentering process, temperature is 100 ℃.In the cotton obtaining, the content of Lavender microcapsules is every square metre of cotton 5g-10g gram.
Embodiment 6
Take the Lavender microcapsules 30kg, the aqueous polyurethane coating mill base 10kg that according to embodiment 3 methods, prepare; KG-101 low temperature COAT PRINTING composite adhesives 30kg, AM-535 hydrophobically modified association type anion base swelling thickener thickener 2kg, prepare finishing agent after adding water to 100kg after mixing.
Utilize the finishing agent of preparation to carry out rear arrangement to cotton, rear arrangement process is: after stamp, oven dry, tentering, obtain finished product.Wherein in drying course, temperature is 90 ℃, and in tentering process, temperature is 105 ℃.In the cotton obtaining, the content of Lavender microcapsules is every square metre of cotton 5g-10g gram.
Embodiment 7
The cotton of gained in embodiment 2 is sewn into pillowcase.The finished product washing size changing rate of pillowcase: warp-wise≤3.0%, broadwise≤3.0%;
COLOR FASTNESS: washable (variable color, staining) >=3 grades;
Perspiration resistance (variable color, staining) >=3 grades;
Fastness to rubbing (unlubricated friction, wet rubbing) >=3 grades;
Content of formaldehyde: < 75mg/kg.
The shape criteria of lavender pillow: the length of adult's pillow should be between 50-70 centimetre, and width is no less than 30 centimetres, height is at 15-20 centimetre.Be specially: the headrest 6-7 centimetre that lies on the back, the neckpillow of lying on the back is 10-12 centimetre, lateral position face side pillow is 14-17 centimetre.
The selection of lavender material: originate from special cultivation elite Flora Region, and without any processing;
The fragrant effective storage life of storage of lavender pillow is: minimum 3-6 month.
The cotton that the present invention arranges after the controlled Lavender microcapsule dressing agent of slowly-releasing also can be used for preparing the home textile products such as sheet, tablecloth, curtain, quilt cover.
More than show and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and description, describes just illustrates principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (3)
1. with the finishing agent that the controlled Lavender microcapsules of slowly-releasing are prepared, fabric is carried out to a method for rear arrangement, it is characterized in that,
The finishing agent that the controlled Lavender microcapsules of described slowly-releasing are prepared, formulated by the raw material of following percentage by weight:
Described low-temperature adhesive is KG-101 low temperature COAT PRINTING composite adhesives;
Described thickener is AM-535 hydrophobically modified association type anion base swelling thickener;
The controlled Lavender microcapsules of slowly-releasing are prepared from by following steps:
A. by percentage by weight 20%～30% Lavender, percentage by weight 10%～20% system modifier MS, excess water in high shearing mixing emulsor high speed homogenising; under the condition stirring, add melamine resin; melamine resin dosage is 1.5%～3% of Lavender weight; be warming up to 55 ℃; be incubated 1～2 hour, carry out individual layer wall building;
B, the system of steps A is cooled to after normal temperature, under the condition stirring, adds melamine resin, melamine resin dosage is 1.5%～3% of Lavender weight, is warming up to 65 ℃, is incubated 2 hours, carries out double-deck wall building;
C. be then warming up to 80 ℃, add 1 of Lavender weight 2.0%～5.0%, 6-hexamethylene diamine carries out three layers of wall building;
Fabric carries out rear arrangement and is comprised of following steps:
(1), stamp step
Adopt common process to be printed on cotton described finishing agent;
(2), baking step
The cotton producing is dried at 50～90 ℃;
(3), tentering step
The cotton of oven dry is carried out to tentering to finished product at 100～105 ℃;
In the cotton obtaining, the content of the controlled Lavender microcapsules of slowly-releasing is every square metre of 5g-10g.
2. the application of finishing agent in home textile product as described in claim 1, is characterized in that, described home textile product is to be made and formed by the fabric after described finishing agent is processed.
3. application as claimed in claim 2, is characterized in that, described home textile product is sheet, pillowcase, quilt cover, curtain or tablecloth.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201010618460.2A CN102268326B (en) | 2010-12-30 | 2010-12-30 | Slow-release controllable lavender essential oil microcapsule and preparation method thereof as well as finishing agent and application thereof |
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| CN201010618460.2A CN102268326B (en) | 2010-12-30 | 2010-12-30 | Slow-release controllable lavender essential oil microcapsule and preparation method thereof as well as finishing agent and application thereof |
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| CN102268326B true CN102268326B (en) | 2014-04-23 |
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Families Citing this family (7)
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| CN103669013A (en) * | 2012-09-19 | 2014-03-26 | 江苏澳丹奴家纺有限公司 | Production method of detachable sleep-assistant quilt head |
| CN102965196B (en) * | 2012-11-09 | 2014-05-07 | 华南理工大学 | Preparation method of essential-oil-coated urea-modified melamine resin microcapsules |
| CN103554347B (en) * | 2013-10-18 | 2016-03-02 | 江南大学 | A kind of preparation method of after-finishing of textile products oxide compound/essential oil/emulsion particle composite particles |
| CN103554338B (en) * | 2013-10-18 | 2016-03-02 | 江南大学 | The preparation method of the fragrant camphor tree essential oil/emulsion particle of a kind of functions of textile fabrics finishing composition |
| CN104695221A (en) * | 2013-12-05 | 2015-06-10 | 福建恒安集团有限公司 | Nonwoven material capable of realizing one time absorption of articles |
| CN112962321B (en) * | 2021-03-12 | 2022-09-13 | 宁波广源纺织品有限公司 | Lavender essence microcapsule finishing liquid |
| WO2023228107A1 (en) * | 2022-05-25 | 2023-11-30 | Cristalfarma S.R.L. | Herbal composition for use in the treatment or prevention of postpartum depression |
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