CN104664535B - Preparation method of kudzuvine root mineral spring beverage based on Wudalianchi bicarbonate mineral water - Google Patents
Preparation method of kudzuvine root mineral spring beverage based on Wudalianchi bicarbonate mineral water Download PDFInfo
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Abstract
A preparation method of kudzuvine root mineral spring drink based on Wudalianchi bicarbonate mineral water relates to a preparation method of mineral spring drink. The invention aims to solve the problems that the existing extract containing starch components is compounded with the Wudalianchi bicarbonate mineral water to easily form copolymerization precipitates, the quality and the stability of the mineral water drink are difficult to control, and the mineral water drink does not have the effects of expanding coronary arteries and preventing alcohol from damaging livers. A kudzuvine root mineral spring beverage based on Wudalianchi bicarbonate mineral water is prepared from 1 to 3 parts by weight of kudzuvine root extract, 0.5 to 2 parts by weight of kudzuvine flower extract and 100 parts by weight of treated Wudalianchi bicarbonate mineral water. The preparation method comprises the following steps: firstly, processing Wudalianchi bicarbonate mineral water; secondly, preparing a kudzu root extracting solution; thirdly, preparing a pueraria flower extracting solution; fourthly, configuration. The invention is suitable for preparing the kudzuvine root mineral spring drink based on the Wudalianchi bicarbonate mineral water.
Description
Technical field
The present invention relates to a kind of preparation method of mineral spring drink.
Background technology
Water is human survival, life and produces the irreplaceable material conditions of institute.Constantly carrying with people's living standard
Height, the requirement also more and more higher to safe drinking water and health.After wudalianchi minerals are colcanism, underground water follows through deep
The liquid mineral resources of the preciousness that ring is formed with country rock interaction, one of big cold spring in the world three, positioned at UNESCO Geopark five
In the conservation of scenic spots area of Dalian pond, its water source is pure, pollution-free, water-quality constituents constant rich in several mineral materials with trace element
And medical curative effect and be recognized.But its mineral composition type of Wudalianchi heavy carbonic mineral water and content are compared with metasilicic acid type
Mineral water is higher, and the extract containing starch component and heavy carbonic mineral water compound and easily form copolymerization precipitation, mineral spring drink
Quality and stability are difficult to control to.And the product after hydrolyzing, mainly based on glucose, can ensure product within a certain period of time
Stability, thus researching and developing a kind of process of suitable heavy carbonic mineral water drink.
The root of kudzu vine is the integration of drinking and medicinal herbs food that the Ministry of Public Health announces, and safety non-toxic can eat for a long time in a large number, its active ingredient Pueraria lobota
The effects such as root flavones has coronary artery dilator, prevents alcohol to hepar damnification.Research to the root of kudzu vine and research and development of products at present is relatively
Many, but do not combine mineral water speciality, especially Wudalianchi heavy carbonic type mineral water water quality characteristicses Pueraria DC drinks
Technique and formulating.Therefore, this invention patent can be enriched wudalianchi minerals product type, promote local mineral spring
Water enterprise development, the acceleration transformation of scientific and technical result.
Content of the invention
The invention aims to it is multiple with Wudalianchi heavy carbonic mineral water to solve the existing extract containing starch component
Complexion easily forms copolymerization precipitation, and the quality of mineral spring drink and stability are difficult to control to not have with mineral spring drink and expand crown moving
Arteries and veins, prevent the problem of alcohol effect to hepar damnification, and a kind of root of kudzu vine ore deposit based on Wudalianchi heavy carbonic mineral water is provided
The preparation method of spring drink.
A kind of root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water is carried by 1 part～3 parts roots of kudzu vine by weight
Wudalianchi heavy carbonic mineral water after taking liquid, 0.5 part～2 parts FI puerariae extracts and 100 parts to process is prepared from.
A kind of preparation method of the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water is to be prepared as follows
:
First, Wudalianchi heavy carbonic mineral water is processed:
1. it is, 10m in discharge3Under conditions of/h, Wudalianchi heavy carbonic mineral water is carried out spraying aeration 10s, obtain
Wudalianchi heavy carbonic mineral water after aeration；
2., using manganese sand filter, the Wudalianchi heavy carbonic mineral water after aeration is filtered, obtain filtration with manganese sand
Wudalianchi heavy carbonic mineral water after device filtration；
3. the Wudalianchi weight carbon after, manganese sand filter being filtered using more medium filter under hydraulic pressure is for 0.75mpa
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after more medium filter filters；
4., with the active fruit shell carbon of 0.6mm～1.2mm as filler, using active fruit shell carbon filter to multi-medium filtering
Wudalianchi heavy carbonic mineral water after device filters is filtered, and obtains the Wudalianchi weight after active fruit shell carbon filter filters
Carbonic acid mineral water；
5., with 5 μm～10 μm polypropylene as filter medium, after active fruit shell carbon filter being filtered using accurate filter
Wudalianchi heavy carbonic mineral water filtered, obtain accurate filter filter after Wudalianchi heavy carbonic mineral water；
6., with doughnut as filter medium, using ultrafiltration apparatus to the Wudalianchi weight carbon after accurate filter filtration
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filter；
7., using ultraviolet sterilization apparatus, the 5s that sterilizes is carried out to the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filtration
～10s, obtains the Wudalianchi heavy carbonic mineral water after ultraviolet sterilization；
8., using the ultimate filter that the aperture folding filter membrane is 0.22 μm, carbon is weighed to the Wudalianchi after ultraviolet sterilization
Sour mineral water is filtered, the Wudalianchi heavy carbonic mineral water after being processed；
2nd, prepare root of kudzu vine extract:
1., the root of kudzu vine cleaning up is dipped into 12h～18h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream
Extract 1h～2h, then filtered, obtain filtrate 1 and filter residue 1；
Step 2 1. described in the root of kudzu vine cleaning up and Wudalianchi metasilicic acid mineral water mass ratio be 1:(10～
15)；
2., filter residue 1 is dipped into 6h～12h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h～3h,
Filtered again, obtained filtrate 2 and filter residue 2；
Step 2 2. described in the quality of filter residue 1 and Wudalianchi metasilicic acid mineral water mass ratio be 1:(10～
15)；
3., filter residue 2 is dipped into 3h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h～3h, then enter
Row filters, and obtains filtrate 3 and filter residue 3；
Step 2 3. described in the quality of filter residue 2 and Wudalianchi metasilicic acid mineral water mass ratio be 1:(10～
15)；
4., filtrate 1, filtrate 2 and filtrate 3 are mixed, obtain mixing filtrate；The body of filtrate will be mixed using Rotary Evaporators
Amass and be concentrated into the 1/5 of original volume, obtain filtrate concentrate；By filtrate concentrate and mass fraction be 95% ethanol according to 1:10
Quality than alcohol precipitation 3 times, then filtered, obtained ethanol extract；Using Rotary Evaporators, ethanol extract revolving is extremely viscous
Thick shape；Thick ethanol extract is dried 1h～2h at temperature is -60 DEG C～-65 DEG C, obtains powdered rubber；
5., powdered rubber is dissolved in distilled water, obtains mixed solution a；Again mixed solution a is heated to 65 DEG C, then
The AMS that vigor is 20000u/ml is added in the mixed solution a being 65 DEG C to temperature, then the 25min that is hydrolyzed～
30min, then inactivate 5min～10min at temperature is 100 DEG C, then it is cooled to 60 DEG C, obtain the mixed liquor b that temperature is 60 DEG C；
The carbohydrase that vigor is 50000u/ml is added in the mixed liquor b being 60 DEG C to temperature, then the 20min～25min that is hydrolyzed, then
Inactivate 5min～10min at temperature is 100 DEG C, then filtered, filtrate is root of kudzu vine extract；
Step 2 5. described in the volume ratio of the quality of powdered rubber and distilled water be 1g:100ml；
Step 2 5. described in temperature be the AMS that 65 DEG C of mixed solution a and vigor is 20000u/ml body
Long-pending ratio is (2000～5000): 1；
Step 2 5. described in temperature be the carbohydrase that 60 DEG C of mixed liquor b and vigor is 50000u/ml volume ratio
For (2000～3000): 1；
3rd, prepare FI puerariae extract:
FI puerariae is dipped into 24h～36h in distilled water, reuses extraction by steam distillation FI puerariae and be dissolved in distilled water
Volatile ingredient, the distillate obtaining is FI puerariae extract；
The mass ratio of the FI puerariae described in step 3 and distilled water is 1:20；
4th, configure: weigh 1 part～3 parts root of kudzu vine extracts, 0.5 part～2 parts FI puerariae extracts and 100 parts by weight
Wudalianchi heavy carbonic mineral water after process, by weigh 1 part～3 parts root of kudzu vine extracts, 0.5 part～2 parts FI puerariae extracts
Wudalianchi heavy carbonic mineral water mixing after processing with 100 parts, then carry out sterilizing, filling, obtain based on Wudalianchi weight carbon
The root of kudzu vine mineral spring drink of sour mineral water.
Step one of the present invention 2. described in manganese sand filter filter medium be manganese dioxide and cobblestone；Described manganese
The filter medium of sand filter is manganese dioxide and cobblestone from top to bottom, and the mass ratio of manganese dioxide and cobblestone is 490:
2550；
Step one of the present invention 3. described in more medium filter filter medium be 0.5mm～2.5mm quartz sand and
The cobblestone of 5mm～40mm；The filter medium of described more medium filter is the quartz sand of 0.5mm～2.5mm from top to bottom
With the cobblestone of 5mm～40mm, the mass ratio of the quartz sand of 0.5mm～2.5mm and the cobblestone of 5mm～40mm is 490:
2500.
Advantages of the present invention:
First, the present invention solves Wudalianchi heavy carbonic mineral water due to ask relatively low compared with high product stability of salinity
Topic；
2nd, the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of present invention preparation is colourless transparent liquid,
There is the fragrance of FI puerariae, under light illumination, in 6 months, be visible by naked eyes precipitation；
3rd, the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of present invention preparation is rich in various trace elements
With kudzu root flavone beneficiating ingredient；Free co2Content is more than 1500mg/l, and total dissolved solid content is 700mg/l～1000mg/
L, puerarin content is 10mg/l～30mg/l.
The present invention is applied to the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water for the preparation.
Specific embodiment one: present embodiment is a kind of root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water
Wudalianchi weight after being processed by 1 part～3 parts root of kudzu vine extracts, 0.5 part～2 parts FI puerariae extracts and 100 parts by weight
Carbonic acid mineral water is prepared from.
The advantage of present embodiment:
First, present embodiment solve Wudalianchi heavy carbonic mineral water due to salinity relatively low compared with high product stability
Problem；
2nd, the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of present embodiment preparation is water white transparency liquid
Body, has the fragrance of FI puerariae, under light illumination, is visible by naked eyes precipitation in 6 months；
3rd, the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of present embodiment preparation is rich in lot of trace
Element and kudzu root flavone beneficiating ingredient；Free co2Content be more than 1500mg/l, total dissolved solid content be 700mg/l～
1000mg/l, puerarin content is 10mg/l～30mg/l.
Present embodiment is applied to the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water for the preparation.
Specific embodiment two: the difference from specific embodiment party one for the present embodiment is: described based on Wudalianchi
In the root of kudzu vine mineral spring drink of heavy carbonic mineral water, the concentration of carbon dioxide is 1500mg/l～1700mg/l.Other be embodied as
Mode one is identical.
Specific embodiment three: the difference from specific embodiment party one or two for the present embodiment is: after described process
Wudalianchi heavy carbonic mineral water is processed according to the following steps:
First, it is 10m in discharge3Under conditions of/h, Wudalianchi heavy carbonic mineral water is carried out spraying aeration 10s, obtain
Wudalianchi heavy carbonic mineral water after aeration；
2nd, using manganese sand filter, the Wudalianchi heavy carbonic mineral water after aeration is filtered, obtain filtration with manganese sand
Wudalianchi heavy carbonic mineral water after device filtration；
3rd, the Wudalianchi weight carbon after manganese sand filter being filtered using more medium filter under hydraulic pressure is for 0.75mpa
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after more medium filter filters；
4th, with the active fruit shell carbon of 0.6mm～1.2mm as filler, using active fruit shell carbon filter to multi-medium filtering
Wudalianchi heavy carbonic mineral water after device filters is filtered, and obtains the Wudalianchi weight after active fruit shell carbon filter filters
Carbonic acid mineral water；
5th, with 5 μm～10 μm polypropylene as filter medium, after active fruit shell carbon filter being filtered using accurate filter
Wudalianchi heavy carbonic mineral water filtered, obtain accurate filter filter after Wudalianchi heavy carbonic mineral water；
6th, with doughnut as filter medium, using ultrafiltration apparatus to the Wudalianchi weight carbon after accurate filter filtration
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filter；
7th, using ultraviolet sterilization apparatus, the 5s that sterilizes is carried out to the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filtration
～10s, obtains the Wudalianchi heavy carbonic mineral water after ultraviolet sterilization；
8th, using the ultimate filter that the aperture folding filter membrane is 0.22 μm, carbon is weighed to the Wudalianchi after ultraviolet sterilization
Sour mineral water is filtered, the Wudalianchi heavy carbonic mineral water after being processed.Other are with specific embodiment one or two-phase
With.
Specific embodiment four: the difference from specific embodiment party one to three for the present embodiment is: the described root of kudzu vine extracts
Liquid extracts by the following method:
First, the root of kudzu vine cleaning up is dipped into 12h～18h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream
Extract 1h～2h, then filtered, obtain filtrate 1 and filter residue 1；
The mass ratio of the root of kudzu vine cleaning up described in step one and Wudalianchi metasilicic acid mineral water be 1:(10～
15)；
2nd, filter residue 1 is dipped into 6h～12h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h～3h,
Filtered again, obtained filtrate 2 and filter residue 2；
The quality of filter residue 1 described in step 2 is 1:(10～15 with the mass ratio of Wudalianchi metasilicic acid mineral water)；
3rd, filter residue 2 is dipped into 3h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h～3h, then enter
Row filters, and obtains filtrate 3 and filter residue 3；
The quality of filter residue 2 described in step 3 is 1:(10～15 with the mass ratio of Wudalianchi metasilicic acid mineral water)；
4th, filtrate 1, filtrate 2 and filtrate 3 are mixed, obtain mixing filtrate；The body of filtrate will be mixed using Rotary Evaporators
Amass and be concentrated into the 1/5 of original volume, obtain filtrate concentrate；By filtrate concentrate and mass fraction be 95% ethanol according to 1:10
Quality than alcohol precipitation 3 times, then filtered, obtained ethanol extract；Using Rotary Evaporators, ethanol extract revolving is extremely viscous
Thick shape；Thick ethanol extract is dried 1h～2h at temperature is -60 DEG C～-65 DEG C, obtains powdered rubber；
5th, powdered rubber is dissolved in distilled water, obtains mixed solution a；Again mixed solution a is heated to 65 DEG C, then
The AMS that vigor is 20000u/ml is added in the mixed solution a being 65 DEG C to temperature, then the 25min that is hydrolyzed～
30min, then inactivate 5min～10min at temperature is 100 DEG C, then it is cooled to 60 DEG C, obtain the mixed liquor b that temperature is 60 DEG C；
The carbohydrase that vigor is 50000u/ml is added in the mixed liquor b being 60 DEG C to temperature, then the 20min～25min that is hydrolyzed, then
Inactivate 5min～10min at temperature is 100 DEG C, then filtered, filtrate is root of kudzu vine extract；
The quality of the powdered rubber described in step 5 and the volume ratio of distilled water are 1g:100ml；
Temperature described in step 5 is the volume of 65 DEG C of mixed solution a AMS for 20000u/ml with vigor
Than for (2000～5000): 1；
Temperature described in step 5 is that the volume ratio of the carbohydrase that 60 DEG C of mixed liquor b and vigor is 50000u/ml is
(2000～3000): 1.Other are identical with specific embodiment one to three.
Specific embodiment five: the difference from specific embodiment party one to four for the present embodiment is: described FI puerariae is extracted
Liquid extracts by the following method:
FI puerariae is dipped into 24h～36h in distilled water, reuses extraction by steam distillation FI puerariae and be dissolved in distilled water
Volatile ingredient, the distillate obtaining is FI puerariae extract；
The mass ratio of described FI puerariae and distilled water is 1:20.Other are identical with specific embodiment one to four.
Specific embodiment six: present embodiment is a kind of root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water
Preparation method be prepared as follows:
First, Wudalianchi heavy carbonic mineral water is processed:
1. it is, 10m in discharge3Under conditions of/h, Wudalianchi heavy carbonic mineral water is carried out spraying aeration 10s, obtain
Wudalianchi heavy carbonic mineral water after aeration；
2., using manganese sand filter, the Wudalianchi heavy carbonic mineral water after aeration is filtered, obtain filtration with manganese sand
Wudalianchi heavy carbonic mineral water after device filtration；
3. the Wudalianchi weight carbon after, manganese sand filter being filtered using more medium filter under hydraulic pressure is for 0.75mpa
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after more medium filter filters；
4., with the active fruit shell carbon of 0.6mm～1.2mm as filler, using active fruit shell carbon filter to multi-medium filtering
Wudalianchi heavy carbonic mineral water after device filters is filtered, and obtains the Wudalianchi weight after active fruit shell carbon filter filters
Carbonic acid mineral water；
5., with 5 μm～10 μm polypropylene as filter medium, after active fruit shell carbon filter being filtered using accurate filter
Wudalianchi heavy carbonic mineral water filtered, obtain accurate filter filter after Wudalianchi heavy carbonic mineral water；
6., with doughnut as filter medium, using ultrafiltration apparatus to the Wudalianchi weight carbon after accurate filter filtration
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filter；
7., using ultraviolet sterilization apparatus, the 5s that sterilizes is carried out to the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filtration
～10s, obtains the Wudalianchi heavy carbonic mineral water after ultraviolet sterilization；
8., using the ultimate filter that the aperture folding filter membrane is 0.22 μm, carbon is weighed to the Wudalianchi after ultraviolet sterilization
Sour mineral water is filtered, the Wudalianchi heavy carbonic mineral water after being processed；
2nd, prepare root of kudzu vine extract:
1., the root of kudzu vine cleaning up is dipped into 12h～18h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream
Extract 1h～2h, then filtered, obtain filtrate 1 and filter residue 1；
Step 2 1. described in the root of kudzu vine cleaning up and Wudalianchi metasilicic acid mineral water mass ratio be 1:(10～
15)；
2., filter residue 1 is dipped into 6h～12h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h～3h,
Filtered again, obtained filtrate 2 and filter residue 2；
Step 2 2. described in the quality of filter residue 1 and Wudalianchi metasilicic acid mineral water mass ratio be 1:(10～
15)；
3., filter residue 2 is dipped into 3h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h～3h, then enter
Row filters, and obtains filtrate 3 and filter residue 3；
Step 2 3. described in the quality of filter residue 2 and Wudalianchi metasilicic acid mineral water mass ratio be 1:(10～
15)；
4., filtrate 1, filtrate 2 and filtrate 3 are mixed, obtain mixing filtrate；The body of filtrate will be mixed using Rotary Evaporators
Amass and be concentrated into the 1/5 of original volume, obtain filtrate concentrate；By filtrate concentrate and mass fraction be 95% ethanol according to 1:10
Quality than alcohol precipitation 3 times, then filtered, obtained ethanol extract；Using Rotary Evaporators, ethanol extract revolving is extremely viscous
Thick shape；Thick ethanol extract is dried 1h～2h at temperature is -60 DEG C～-65 DEG C, obtains powdered rubber；
5., powdered rubber is dissolved in distilled water, obtains mixed solution a；Again mixed solution a is heated to 65 DEG C, then
The AMS that vigor is 20000u/ml is added in the mixed solution a being 65 DEG C to temperature, then the 25min that is hydrolyzed～
30min, then inactivate 5min～10min at temperature is 100 DEG C, then it is cooled to 60 DEG C, obtain the mixed liquor b that temperature is 60 DEG C；
The carbohydrase that vigor is 50000u/ml is added in the mixed liquor b being 60 DEG C to temperature, then the 20min～25min that is hydrolyzed, then
Inactivate 5min～10min at temperature is 100 DEG C, then filtered, filtrate is root of kudzu vine extract；
Step 2 5. described in the volume ratio of the quality of powdered rubber and distilled water be 1g:100ml；
Step 2 5. described in temperature be the AMS that 65 DEG C of mixed solution a and vigor is 20000u/ml body
Long-pending ratio is (2000～5000): 1；
Step 2 5. described in temperature be the carbohydrase that 60 DEG C of mixed liquor b and vigor is 50000u/ml volume ratio
For (2000～3000): 1；
3rd, prepare FI puerariae extract:
FI puerariae is dipped into 24h～36h in distilled water, reuses extraction by steam distillation FI puerariae and be dissolved in distilled water
Volatile ingredient, the distillate obtaining is FI puerariae extract；
The mass ratio of the FI puerariae described in step 3 and distilled water is 1:20；
4th, configure: weigh 1 part～3 parts root of kudzu vine extracts, 0.5 part～2 parts FI puerariae extracts and 100 parts by weight
Wudalianchi heavy carbonic mineral water after process, by weigh 1 part～3 parts root of kudzu vine extracts, 0.5 part～2 parts FI puerariae extracts
Wudalianchi heavy carbonic mineral water mixing after processing with 100 parts, then carry out sterilizing, filling, obtain based on Wudalianchi weight carbon
The root of kudzu vine mineral spring drink of sour mineral water.
The advantage of present embodiment:
First, present embodiment solve Wudalianchi heavy carbonic mineral water due to salinity relatively low compared with high product stability
Problem；
2nd, the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of present embodiment preparation is water white transparency liquid
Body, has the fragrance of FI puerariae, under light illumination, is visible by naked eyes precipitation in 6 months；
3rd, the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of present embodiment preparation is rich in lot of trace
Element and kudzu root flavone beneficiating ingredient；Free co2Content be more than 1500mg/l, total dissolved solid content be 700mg/l～
1000mg/l, puerarin content is 10mg/l～30mg/l.
Specific embodiment seven: the difference from specific embodiment six for the present embodiment is: described based on five Dalian
The root of kudzu vine mineral spring drink of pond heavy carbonic mineral water is pressed into carbon dioxide in pouring process.Other and specific embodiment one phase
With.
Specific embodiment eight: the difference from specific embodiment six or seven for the present embodiment is: described based on five
The root of kudzu vine mineral spring drink of Dalian pond heavy carbonic mineral water be pressed in pouring process carbon dioxide concentration be 1500mg/l～
1700mg/l.Other are identical with specific embodiment six or seven.
Specific embodiment nine: the difference from specific embodiment six to eight for the present embodiment is: press weight in step 4
Amount number weighs the Wudalianchi weight carbon after 1 part～2 parts root of kudzu vine extracts, 0.5 part～1 part FI puerariae extract and 100 parts are processed
Sour mineral water, five Dalian after weigh 1 part～2 parts root of kudzu vine extracts, 0.5 part～1 part FI puerariae extract and 100 parts are processed
The mixing of pond heavy carbonic mineral water, then carry out sterilizing, filling, obtain the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water
Product.Other are identical with specific embodiment six to eight.
Specific embodiment ten: the difference from specific embodiment six to nine for the present embodiment is: press weight in step 4
Amount number weighs the Wudalianchi heavy carbonic after 2 parts～3 parts root of kudzu vine extracts, 1 part～2 parts FI puerariae extracts and 100 parts are processed
Mineral water, the Wudalianchi weight after weigh 2 parts～3 parts root of kudzu vine extracts, 1 part～2 parts FI puerariae extracts and 100 parts are processed
Carbonic acid mineral water mixes, then carry out sterilizing, filling, obtain the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water.Its
He is identical with specific embodiment six to nine.
Using tests below checking beneficial effects of the present invention:
Test one: a kind of preparation method of the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water is by with lower section
Method preparation:
First, Wudalianchi heavy carbonic mineral water is processed:
1. it is, 10m in discharge3Under conditions of/h, Wudalianchi heavy carbonic mineral water is carried out spraying aeration 10s, obtain
Wudalianchi heavy carbonic mineral water after aeration；
2., using manganese sand filter, the Wudalianchi heavy carbonic mineral water after aeration is filtered, obtain filtration with manganese sand
Wudalianchi heavy carbonic mineral water after device filtration；
3. the Wudalianchi weight carbon after, manganese sand filter being filtered using more medium filter under hydraulic pressure is for 0.75mpa
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after more medium filter filters；
4., with the active fruit shell carbon of 0.6mm～1.2mm as filler, using active fruit shell carbon filter to multi-medium filtering
Wudalianchi heavy carbonic mineral water after device filters is filtered, and obtains the Wudalianchi weight after active fruit shell carbon filter filters
Carbonic acid mineral water；
5., with 5 μm～10 μm polypropylene as filter medium, after active fruit shell carbon filter being filtered using accurate filter
Wudalianchi heavy carbonic mineral water filtered, obtain accurate filter filter after Wudalianchi heavy carbonic mineral water；
6., with doughnut as filter medium, using ultrafiltration apparatus to the Wudalianchi weight carbon after accurate filter filtration
Sour mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filter；
7., using ultraviolet sterilization apparatus, the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filtration is sterilized
5s, obtains the Wudalianchi heavy carbonic mineral water after ultraviolet sterilization；
8., using the ultimate filter that the aperture folding filter membrane is 0.22 μm, carbon is weighed to the Wudalianchi after ultraviolet sterilization
Sour mineral water is filtered, the Wudalianchi heavy carbonic mineral water after being processed；
2nd, prepare root of kudzu vine extract:
1., the root of kudzu vine cleaning up is dipped into 12h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract
1h, then filtered, obtain filtrate 1 and filter residue 1；
Step 2 1. described in the mass ratio of the root of kudzu vine cleaning up and Wudalianchi metasilicic acid mineral water be 1:10；
2., filter residue 1 is dipped into 6h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h, then carried out
Filter, obtains filtrate 2 and filter residue 2；
Step 2 2. described in the mass ratio of the quality of filter residue 1 and Wudalianchi metasilicic acid mineral water be 1:10；
3., filter residue 2 is dipped into 3h in the metasilicic acid mineral water of Wudalianchi, then carries out backflow stream and extract 2h, then carried out
Filter, obtains filtrate 3 and filter residue 3；
Step 2 3. described in the mass ratio of the quality of filter residue 2 and Wudalianchi metasilicic acid mineral water be 1:10；
4., filtrate 1, filtrate 2 and filtrate 3 are mixed, obtain mixing filtrate；The body of filtrate will be mixed using Rotary Evaporators
Amass and be concentrated into the 1/5 of original volume, obtain filtrate concentrate；By filtrate concentrate and mass fraction be 95% ethanol according to 1:10
Quality than alcohol precipitation 3 times, then filtered, obtained ethanol extract；Using Rotary Evaporators, ethanol extract revolving is extremely viscous
Thick shape；Thick ethanol extract is dried 2h at temperature is -65 DEG C, obtains powdered rubber；
5., powdered rubber is dissolved in distilled water, obtains mixed solution a；Again mixed solution a is heated to 65 DEG C, then
The AMS that vigor is 20000u/ml is added in the mixed solution a being 65 DEG C to temperature, then the 25min that is hydrolyzed, then in temperature
Spend for inactivateing 8min at 100 DEG C, then be cooled to 60 DEG C, obtain the mixed liquor b that temperature is 60 DEG C；The mixed liquor being 60 DEG C to temperature
The carbohydrase that vigor is 50000u/ml is added in b, then the 20min that is hydrolyzed, then inactivate 8min at temperature is 100 DEG C, then enter
Row filters, and filtrate is root of kudzu vine extract；
Step 2 5. described in the volume ratio of the quality of powdered rubber and distilled water be 1g:100ml；
Step 2 5. described in temperature be the AMS that 65 DEG C of mixed solution a and vigor is 20000u/ml body
Long-pending ratio is 5000:1；
Step 2 5. described in temperature be the carbohydrase that 60 DEG C of mixed liquor b and vigor is 50000u/ml volume ratio
For 2000:1；
3rd, prepare FI puerariae extract:
FI puerariae is dipped into 24h in distilled water, reuses extraction by steam distillation FI puerariae and be dissolved in the volatilization in distilled water
Property composition, the distillate obtaining be FI puerariae extract；
The mass ratio of the FI puerariae described in step 3 and distilled water is 1:20；
4th, configure: weigh five after 1 part of root of kudzu vine extract, 0.5 part of FI puerariae extract and 100 parts are processed by weight
Dalian pond heavy carbonic mineral water, five Dalian after weigh 1 part of root of kudzu vine extract, 0.5 part of FI puerariae extract and 100 parts are processed
The mixing of pond heavy carbonic mineral water, then carry out sterilizing, filling, obtain the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water
Product；
Being pressed in pouring process based on the root of kudzu vine mineral spring drink of Wudalianchi heavy carbonic mineral water described in step 4
Carbon dioxide, the concentration of press-in carbon dioxide is 1500mg/l.
This test procedure one 2. described in manganese sand filter filter medium be manganese dioxide and cobblestone；Described manganese
The filter medium of sand filter is manganese dioxide and cobblestone from top to bottom, and the mass ratio of manganese dioxide and cobblestone is 490:
2550；
This test procedure one 3. described in more medium filter filter medium be 0.5mm～2.5mm quartz sand and
The cobblestone of 5mm～40mm；The filter medium of described more medium filter is the quartz sand of 0.5mm～2.5mm from top to bottom
With the cobblestone of 5mm～40mm, the mass ratio of the quartz sand of 0.5mm～2.5mm and the cobblestone of 5mm～40mm is 490:
2500.
Step one 1. described in Wudalianchi heavy carbonic mineral water main component and content be shown in Table 1.
The main component of table 1 heavy carbonic mineral water
| Inspection project | Unit | Content | Inspection project | Unit | Content |
| fe | mg/l | 35 | Total dissolved solid | mg/l | 1200 |
| Free co2 | mg/l | 1200 | ph | 5.0-6.8 | |
| k | mg/l | 70 | na | mg/l | 61 |
| ca | mg/l | 82 | mg | mg/l | 90 |
| cu | μg/l | 4.8 | zn | μg/l | 55 |
| Metasilicic acid | mg/l | 75 |
The main component of the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water that step 4 obtains and content are shown in
Table 2.
The Contents of Main Components of table 2 product
| Inspection project | Unit | Content | Inspection project | Unit | Content |
| Puerarin | mg/l | 10 | Total dissolved solid | mg/l | 800 |
| Free co2 | mg/l | 1500 | ph | 5.5-6.8 | |
| k | mg/l | 65 | na | mg/l | 55 |
| ca | mg/l | 70 | mg | mg/l | 60 |
| cu | μg/l | 4.2 | zn | μg/l | 50 |
| Metasilicic acid | mg/l | 45 | fe | mg/l | Do not detect |
This test solves the problems, such as that Wudalianchi heavy carbonic mineral water is relatively low compared with high product stability due to salinity；
The root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water of this test preparation is colourless transparent liquid, has
The fragrance of FI puerariae, under light illumination, is visible by naked eyes precipitation in 6 months；
This test preparation the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water be rich in various trace elements and
Kudzu root flavone beneficiating ingredient；Free co2Content is 1500mg/l, and total dissolved solid content is 800mg/l, and puerarin content is
10mg/l.
Claims (1)
1. a kind of preparation method of the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water is it is characterised in that the method is
Complete according to the following steps:
First, Wudalianchi heavy carbonic mineral water is processed:
1. it is, 10m in discharge3Under conditions of/h, Wudalianchi heavy carbonic mineral water is carried out spraying aeration 10s, obtain aeration
Wudalianchi heavy carbonic mineral water afterwards；
2., using manganese sand filter, the Wudalianchi heavy carbonic mineral water after aeration is filtered, obtain manganese sand filter mistake
Wudalianchi heavy carbonic mineral water after filter；
Step one 2. described in manganese sand filter filter medium be manganese dioxide and cobblestone；Described manganese sand filter
Filter medium is manganese dioxide and cobblestone from top to bottom, and the mass ratio of manganese dioxide and cobblestone is 490:2550；
3. the Wudalianchi heavy carbonic ore deposit after, manganese sand filter being filtered using more medium filter under hydraulic pressure is for 0.75mpa
Spring is filtered, and obtains the Wudalianchi heavy carbonic mineral water after more medium filter filters；
Step one 3. described in the filter medium of more medium filter be the quartz sand of 0.5mm～2.5mm and 5mm～40mm
Cobblestone；The filter medium of described more medium filter is quartz sand and the 5mm～40mm of 0.5mm～2.5mm from top to bottom
Cobblestone, the mass ratio of the quartz sand of 0.5mm～2.5mm and the cobblestone of 5mm～40mm is 490:2500；
4., with the active fruit shell carbon of 0.6mm～1.2mm as filler, using active fruit shell carbon filter to more medium filter mistake
Wudalianchi heavy carbonic mineral water after filter is filtered, and obtains the Wudalianchi heavy carbonic after active fruit shell carbon filter filters
Mineral water；
5., with 5 μm～10 μm polypropylene as filter medium, using accurate filter to five after the filtration of active fruit shell carbon filter
Dalian pond heavy carbonic mineral water is filtered, and obtains the Wudalianchi heavy carbonic mineral water after accurate filter filters；
6., with doughnut as filter medium, using ultrafiltration apparatus to the Wudalianchi heavy carbonic ore deposit after accurate filter filtration
Spring is filtered, and obtains the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filter；
7., using ultraviolet sterilization apparatus, the 5s that sterilizes is carried out to the Wudalianchi heavy carbonic mineral water after ultrafiltration apparatus filtration, obtain
Wudalianchi heavy carbonic mineral water to after ultraviolet sterilization；
8., using fold filter membrane aperture be 0.22 μm ultimate filter to the Wudalianchi heavy carbonic ore deposit after ultraviolet sterilization
Spring is filtered, the Wudalianchi heavy carbonic mineral water after being processed；
2nd, prepare root of kudzu vine extract:
1., the root of kudzu vine cleaning up is dipped into 12h in the metasilicic acid mineral water of Wudalianchi, then carries out refluxing extraction 1h, then enter
Row filters, and obtains filtrate 1 and filter residue 1；
Step 2 1. described in the mass ratio of the root of kudzu vine cleaning up and Wudalianchi metasilicic acid mineral water be 1:10；
2., filter residue 1 is dipped into 6h in the metasilicic acid mineral water of Wudalianchi, then carries out refluxing extraction 2h, then filtered, obtain
Filtrate 2 and filter residue 2；
Step 2 2. described in the mass ratio of the quality of filter residue 1 and Wudalianchi metasilicic acid mineral water be 1:10；
3., filter residue 2 is dipped into 3h in the metasilicic acid mineral water of Wudalianchi, then carries out refluxing extraction 2h, then filtered, obtain
Filtrate 3 and filter residue 3；
Step 2 3. described in the mass ratio of the quality of filter residue 2 and Wudalianchi metasilicic acid mineral water be 1:10；
4., filtrate 1, filtrate 2 and filtrate 3 are mixed, obtain mixing filtrate；Will be dense for the volume mixing filtrate using Rotary Evaporators
It is reduced to the 1/5 of original volume, obtain filtrate concentrate；By filtrate concentrate and mass fraction be 95% ethanol according to 1:10 matter
Amount is than alcohol precipitation 3 times, then is filtered, and obtains ethanol extract；Using Rotary Evaporators, ethanol extract revolving is extremely thick；
Thick ethanol extract is dried 2h at temperature is -65 DEG C, obtains powdered rubber；
5., powdered rubber is dissolved in distilled water, obtains mixed solution a；Again mixed solution a is heated to 65 DEG C, then to temperature
Spending for addition vigor in 65 DEG C of mixed solution a is the AMS of 20000u/ml, then the 25min that is hydrolyzed, then in temperature is
Inactivate 8min at 100 DEG C, then be cooled to 60 DEG C, obtain the mixed liquor b that temperature is 60 DEG C；In the mixed liquor b being 60 DEG C to temperature
Addition vigor is the carbohydrase of 50000u/ml, then the 20min that is hydrolyzed, then inactivates 8min at temperature is 100 DEG C, then carries out
Filter, filtrate is root of kudzu vine extract；
Step 2 5. described in the volume ratio of the quality of powdered rubber and distilled water be 1g:100ml；
Step 2 5. described in temperature be the AMS that 65 DEG C of mixed solution a and vigor is 20000u/ml volume ratio
For 5000:1；
Step 2 5. described in temperature be that the volume ratio of the carbohydrase that 60 DEG C of mixed liquor b and vigor is 50000u/ml is
2000:1；
3rd, prepare FI puerariae extract:
FI puerariae is dipped into 24h in distilled water, reuses the volatility one-tenth that extraction by steam distillation FI puerariae is dissolved in distilled water
Point, the distillate obtaining is FI puerariae extract；
The mass ratio of the FI puerariae described in step 3 and distilled water is 1:20；
4th, configure: weigh five Dalian after 1 part of root of kudzu vine extract, 0.5 part of FI puerariae extract and 100 parts are processed by weight
Pond heavy carbonic mineral water, the Wudalianchi weight after weigh 1 part of root of kudzu vine extract, 0.5 part of FI puerariae extract and 100 parts are processed
Carbonic acid mineral water mixes, then carry out sterilizing, filling, obtain the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water；
Described in step 4, dioxy is pressed in pouring process based on the root of kudzu vine mineral spring drink of Wudalianchi heavy carbonic mineral water
Change carbon, the concentration of press-in carbon dioxide is 1500mg/l；
In the root of kudzu vine mineral spring drink based on Wudalianchi heavy carbonic mineral water described in step 4, k content is 65mg/l, and ca contains
Measure as 70mg/l, cu content is 4.2 μ g/l, na content is 55mg/l, mg content is 60mg/l, zn content is 50 μ g/l, dissociates
co2Content is 1500mg/l, and total dissolved solid content is 800mg/l, and puerarin content is 10mg/l.
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| CN106721692B (en) * | 2016-11-17 | 2020-10-27 | 黑龙江省科学院火山与矿泉研究所 | Instant Wudalianchi recarbonic mineral water fruit juice beverage and preparation method thereof |
| CN110973427A (en) * | 2019-12-18 | 2020-04-10 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of gas-containing soda water based on Wudalianchi natural spring water |
| CN111011680A (en) * | 2019-12-18 | 2020-04-17 | 黑龙江省科学院火山与矿泉研究所 | Preparation method and application of micro-bubble water based on natural soda water of Wudalianchi |
| CN112021480A (en) * | 2020-09-09 | 2020-12-04 | 黑龙江省科学院自然与生态研究所 | Preparation method of mineral water containing ferrous pentagon hithijichi bicarbonate |
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