CN104664377B - A kind of preparation method of sugar-free natural product health-care powder - Google Patents

A kind of preparation method of sugar-free natural product health-care powder Download PDF

Info

Publication number
CN104664377B
CN104664377B CN201510071805.XA CN201510071805A CN104664377B CN 104664377 B CN104664377 B CN 104664377B CN 201510071805 A CN201510071805 A CN 201510071805A CN 104664377 B CN104664377 B CN 104664377B
Authority
CN
China
Prior art keywords
sugar
desugar
zymotic fluid
content
fermentation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510071805.XA
Other languages
Chinese (zh)
Other versions
CN104664377A (en
Inventor
王芳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shaanxi Xueqian Normal University
Original Assignee
Shaanxi Xueqian Normal University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shaanxi Xueqian Normal University filed Critical Shaanxi Xueqian Normal University
Priority to CN201510071805.XA priority Critical patent/CN104664377B/en
Publication of CN104664377A publication Critical patent/CN104664377A/en
Application granted granted Critical
Publication of CN104664377B publication Critical patent/CN104664377B/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Landscapes

  • Medicines Containing Plant Substances (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

The invention discloses a kind of preparation method of sugar-free natural product health-care powder, by pre-treatment, composition adjustment, one time fermentation desugar, except removing six steps such as alcohol, secondary fermentation desugar, spray drying finally prepared sugar-free natural product health-care powder admittedly.On the basis of one time fermentation is carried out to natural products, using low temperature countercurrent spray concentration technique, the ethanol content in zymotic fluid is reduced;Recycling is secondary to restart fermentation technique, and glucide is converted into ethanol to the full extent, reduces the content of sugar in zymotic fluid;The second alcohol and water in zymotic fluid is finally removed using the method for spray drying, finally prepared sugar-free natural product health-care powder, its sugar content is less than 0.5%, and manufacture craft is unique, advanced design, and product sugar content meets the requirement of GB sugarless products.

Description

A kind of preparation method of sugar-free natural product health-care powder
Technical field
The present invention relates to biological field, and in particular to a kind of preparation method of sugar-free natural product health-care powder.
Background technology
With the increasingly raising of living standard, the dietary structure of China consumer also greatly changes, due to glucide Intake increases year by year, and the incidence of disease of the disease such as obesity, diabetes, carious tooth also shows ascendant trend year by year.With people couple The growing interest of health, sugarfree foods are increasingly favored by consumer.Early in last century Mo, the developed country such as America and Europe has just gone out Existing " glucose-diet " concept, the healthy food of " low in calories, blood glucose increasing is slow " is received by increasing crowd.Then soon, In the market is even more and has emerged sugarless products, and such as Japanese carefree, the production of Mingzhi's brand many products are sugarfree foods. The beginning of this century, China starts to popularize sugarfree foods concept.Caused by the understanding to sugarfree foods it was recognized that sugarfree foods It is merely not only the special of diabetes patient, sugarfree foods also have functions that prevention decayed tooth, prevent obesity etc..It is such in order to prevent The harm that disease brings, increasing consumer starts gradually to adjust the eating habit of oneself, and notice is turned To sugarfree foods or food with low sugar content.Sugarfree foods as health-oriented products by increasing people cognition with receive.
Natural products refers to biological (animal, plant and microorganism) internal constituent or its metabolite, because it contains There are protein and its hydrolysate, glucide, nucleic acid, enzyme, lipid material, vitamin, alkaloid, volatile oil, flavones, terpene The native chemicals such as material, organic acid, aldehydes matter, quinones substance, steroidal compounds, tannins material, antibiotic agents into Point, therefore often there is nutritive value and medical value very high.But the such conventional medicine-food two-purpose natural products in part, often Containing glucide higher, it is unsuitable for the crowd with illnesss such as hyperglycaemia, high fat of blood, obesity, carious teeth and eats, it is such as big Jujube, arillus longan, mulberries, matrimony vine etc..Therefore, the exploitation special technique technique natural products higher to such sugar content is retaining it On the basis of peculiar nutritive value and medical value, desugar treatment is carried out to it, produce the edible sugar-free of suitable special population Natural products health product just seems very necessary.
From 1 day January in 2013 of China in " prepackaged food nutritional labeling general rule " (GB28050-2011) of implementation clearly Regulation, sugared content≤0.5g/100g (solid) or 100mL (liquid) could claim sugarfree foods.Existing desugar technique is (such as:It is a kind of Removed-sugar honey and preparation method thereof) glucide in raw material is transformed into second using biofermentation mode (disposable fermentation) Alcohol, and ethanol is steamed from product by way of rotary evaporation.But because sugar content is high in the natural products of part, saccharomycete When the alcohol content that fermentation is produced is higher, activity itself will be suppressed so that fermentation terminates, and hinder sugar to convert completely Exhaust, therefore sugar content is higher than national standard in final products, it is impossible to it is edible directly as sugarfree foods, can only be former as low sugar Material is added in all kinds of sugarless products.And such low sugar product is influenceed by itself sugar content so that it is in sugarfree foods In addition be limited, influence the performance of its trophic function and medicinal function.
The content of the invention
For higher sugar class material is contained in the natural products of part, it is unfavorable for hyperglycaemia, high fat of blood, obesity, carious tooth et al. The edible defect of group, the invention provides a kind of preparation method of sugar-free natural product health-care powder, to entering containing sugared natural products On the basis of row one time fermentation, using low temperature countercurrent spray concentration technique, the ethanol content in zymotic fluid is reduced;Recycle secondary Restart fermentation technique, glucide is converted into ethanol to the full extent, reduce the content of sugar in zymotic fluid;Finally using spraying Dry method removes the second alcohol and water in zymotic fluid, finally prepared sugar-free natural product health-care powder.
To achieve the above object, the technical scheme taken of the present invention is:
A kind of preparation method of sugar-free natural product health-care powder, comprises the following steps:
S1, screening after removing impurity, clean removal residues of pesticides, the raw material after must purifying containing sugared natural products raw material;
S2, the raw material after the purification obtained by step S1 is carried out attrition crushing or crush (graininess is crushed to dry product, it is right Water content fresh goods high carries out attrition crushing), suitable quantity of water is added, obtain raw material suspension;
S3, citric acid is added in the raw material suspension obtained by step S2, after regulation pH to 3.3, in the ratio of 70mg/L Addition pectase, is well mixed, then adds Angel SY yeast in the ratio of 200mg/L, is well mixed, and obtains mixture;
S4, the mixture obtained by step S3 is placed at a temperature of 25 DEG C, fermented 7~9 days, be measured by sampling every 24h and sent out Residual sugar content in ferment mixture, when residual sugar content is less than or equal to 0.5%, i.e. one time fermentation desugar terminates;
After S5, one time fermentation desugar terminate, filtering, by fermenting mixture separation of solid and liquid, removes solid residue, must ferment Liquid;
S6, zymotic fluid is carried out low temperature countercurrent spray concentration, until ethanol content is less than 4 ° (v/v) in concentrate, stopped Concentration, obtains concentrate;
S7, Angel SY yeast is added in concentrate in the ratio of 100mg/L, after being well mixed, be placed in 25 DEG C of temperature Under, ferment 5~7 days, the residual sugar content in 24h is measured by sampling zymotic fluid, when residual sugar content is less than or equal to 0.02%, That is secondary fermentation desugar terminates, and obtains secondary fermentation desugar liquid;
S8, take secondary fermentation desugar liquid and be spray-dried, obtain final products sugar-free natural product health-care powder.
The invention has the advantages that:
On the basis of one time fermentation is carried out to natural products, using low temperature countercurrent spray concentration technique, zymotic fluid is reduced In ethanol content;Recycling is secondary to restart fermentation technique, and glucide is converted into ethanol to the full extent, reduces zymotic fluid The content of middle sugar;The second alcohol and water in zymotic fluid is finally removed using the method for spray drying, finally prepared sugar-free natural product Health-care powder, its sugar content is less than 0.5%, and manufacture craft is unique, advanced design, and product sugar content meets GB sugarless products will Ask, can to greatest extent retain the peculiar nutritional ingredient and medicinal ingredient in natural products, be suitable for various people especially Crowd with the inedibility glucide such as hyperglycaemia, high fat of blood, obesity, carious tooth directly eats, or exists as nutritional ingredient Especially it is added in sugarfree foods in varieties of food items.
Brief description of the drawings
Fig. 1 is a kind of process chart of the preparation method of sugar-free natural product health-care powder of the embodiment of the present invention.
Specific embodiment
In order that objects and advantages of the present invention become more apparent, the present invention is carried out further with reference to embodiments Describe in detail.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair It is bright.
As shown in figure 1, a kind of preparation method of sugar-free natural product health-care powder is the embodiment of the invention provides, including it is as follows Step:
S1, screening after removing decayed fruit and impurity, clean removal residues of pesticides, after must purifying containing sugared natural products raw material Raw material;
S2, the raw material after the purification obtained by step S1 is carried out attrition crushing or crush (graininess is crushed to dry product, it is right Water content fresh goods high carries out attrition crushing), suitable quantity of water is added, obtain raw material suspension;
S3, citric acid is added in the raw material suspension obtained by step S2, after regulation pH to 3.3, in the ratio of 70mg/L Addition pectase, is well mixed, then adds Angel SY yeast in the ratio of 200mg/L, is well mixed, and obtains mixture;
S4, the mixture obtained by step S3 is placed at a temperature of 25 DEG C, fermented 7~9 days, be measured by sampling every 24h and sent out Residual sugar content in ferment mixture, when residual sugar content is less than or equal to 0.5%, i.e. one time fermentation desugar terminates;
After S5, one time fermentation desugar terminate, filtering, by fermenting mixture separation of solid and liquid, removes solid residue, must ferment Liquid;
S6, zymotic fluid is carried out low temperature countercurrent spray concentration, until ethanol content is less than 4 ° (v/v) in concentrate, stopped Concentration, obtains concentrate;
S7, Angel SY yeast is added in concentrate in the ratio of 100mg/L, after being well mixed, be placed in 25 DEG C of temperature Under, ferment 5~7 days, the residual sugar content in 24h is measured by sampling zymotic fluid, when residual sugar content is less than or equal to 0.02%, That is secondary fermentation desugar terminates, and obtains secondary fermentation desugar liquid;
S8, take secondary fermentation desugar liquid and be spray-dried, obtain final products sugar-free natural product health-care powder.
Wherein, under the conditions of uniform pressure, ethyl alcohol boiling point is less than aqueous water, in countercurrent spray concentration process, in zymotic fluid Ethanol evaporation amount be much larger than water, therefore ethanol content in concentrate can be reduced, and evaporation rate is fast.Under cryogenic (50 DEG C of hot air temperature, spray droplet actual temperature is about 40 DEG C) carries out countercurrent spray, can to greatest extent retain concentration Bioactive ingredients in liquid, it is to avoid its thermal decomposition.
Embodiment 1
Take 50kg mulberries raw material really, the net fruit of mulberries is obtained by screening, cleaning.Attrition crushing is carried out to it, mulberries are obtained Pulp.Citric acid is first added in mulberries pulp, pulp pH to 3.3 is adjusted, pectase is added in pulp according still further to 70mg/L, It is well mixed, Angel SY yeast is finally added in pulp according to 200mg/L, it is well mixed.Control mixing fruit jam fermentation temperature At 25 DEG C, the residual sugar content in 24h is measured by sampling fermentation pulp, residual sugar content is less than 0.5%, i.e. one time fermentation after 8 days Desugar terminates.After one time fermentation desugar terminates, filtering, by pulp separation of solid and liquid of fermenting, removes solid residue, retains liquid portion Point.Zymotic fluid is carried out into low temperature countercurrent spray concentration, ethanol content is less than 4 ° (v/v) into concentrate, now fermentating liquid volume About condensate precursor product 75%.Add Angel SY yeast again in concentrate according to 100mg/L, be well mixed.Control is mixed Concentrate fermentation temperature is closed at 25 DEG C, the residual sugar content in 24h is measured by sampling zymotic fluid, residual sugar content is less than after 5 days 0.02%, i.e. secondary fermentation desugar terminates.Take secondary fermentation desugar liquid to be spray-dried, obtain final products sugar-free mulberries Powder, after testing, its sugar content is 0.411%.
Embodiment 2
Take 50kg mulberries raw material really, the net fruit of mulberries is obtained by screening, cleaning.Attrition crushing is carried out to it, mulberries are obtained Pulp.Citric acid is first added in mulberries pulp, pulp pH to 3.3 is adjusted, pectase is added in pulp according still further to 70mg/L, It is well mixed, Angel SY yeast is finally added in pulp according to 200mg/L, it is well mixed.Control mixing fruit jam fermentation temperature At 25 DEG C, the residual sugar content in 24h is measured by sampling fermentation pulp, residual sugar content is less than 0.5%, i.e. one time fermentation after 7 days Desugar terminates.After one time fermentation desugar terminates, filtering, by pulp separation of solid and liquid of fermenting, removes solid residue, retains liquid portion Point.Zymotic fluid is carried out into low temperature countercurrent spray concentration, ethanol content is less than 4 ° (v/v) into concentrate, now fermentating liquid volume About condensate precursor product 75%.Add Angel SY yeast again in concentrate according to 100mg/L, be well mixed.Control is mixed Concentrate fermentation temperature is closed at 25 DEG C, the residual sugar content in 24h is measured by sampling zymotic fluid, residual sugar content is less than after 6 days 0.02%, i.e. secondary fermentation desugar terminates.Take secondary fermentation desugar liquid to be spray-dried, obtain final products sugar-free mulberries Powder, after testing, its sugar content is 0.402%.
Embodiment 3
Take 50kg mulberries raw material really, the net fruit of mulberries is obtained by screening, cleaning.Attrition crushing is carried out to it, mulberries are obtained Pulp.Citric acid is first added in mulberries pulp, pulp pH to 3.3 is adjusted, pectase is added in pulp according still further to 70mg/L, It is well mixed, Angel SY yeast is finally added in pulp according to 200mg/L, it is well mixed.Control mixing fruit jam fermentation temperature At 25 DEG C, the residual sugar content in 24h is measured by sampling fermentation pulp, residual sugar content is less than 0.5%, i.e. one time fermentation after 9 days Desugar terminates.After one time fermentation desugar terminates, filtering, by pulp separation of solid and liquid of fermenting, removes solid residue, retains liquid portion Point.Zymotic fluid is carried out into low temperature countercurrent spray concentration, ethanol content is less than 4 ° (v/v) into concentrate, now fermentating liquid volume About condensate precursor product 75%.Add Angel SY yeast again in concentrate according to 100mg/L, be well mixed.Control is mixed Concentrate fermentation temperature is closed at 25 DEG C, the residual sugar content in 24h is measured by sampling zymotic fluid, residual sugar content is less than after 7 days 0.02%, i.e. secondary fermentation desugar terminates.Take secondary fermentation desugar liquid to be spray-dried, obtain final products sugar-free mulberries Powder, after testing, its sugar content is 0.398%.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For member, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims (1)

1. a kind of preparation method of sugar-free natural product health-care powder, it is characterised in that comprise the following steps:
S1, take 50kg mulberries raw material really, after removing impurity, cleaning removal residues of pesticides, the raw material after must purifying;
S2, attrition crushing or crushing are carried out to the raw material after the purification obtained by step S1, add suitable quantity of water, obtain raw material suspension Liquid;
S3, citric acid is added in the raw material suspension obtained by step S2, after regulation pH to 3.3, added in the ratio of 70mg/L Pectase, is well mixed, then adds Angel SY yeast in the ratio of 200mg/L, is well mixed, and obtains mixture;
S4, the mixture obtained by step S3 is placed at a temperature of 25 DEG C, fermented 7~9 days, it is mixed that fermentation is measured by sampling every 24h Residual sugar content in compound, when residual sugar content is less than or equal to 0.5%, i.e. one time fermentation desugar terminates;
After S5, one time fermentation desugar terminate, filtering, by fermenting mixture separation of solid and liquid, removes solid residue, obtains zymotic fluid;
S6, zymotic fluid is carried out low temperature countercurrent spray concentration, until ethanol content is less than 4 ° (v/v) in concentrate, stops concentration, Obtain concentrate;
S7, Angel SY yeast is added in concentrate in the ratio of 100mg/L, after being well mixed, be placed at a temperature of 25 DEG C, sent out Ferment 5~7 days, the residual sugar content in 24h is measured by sampling zymotic fluid, when residual sugar content is less than or equal to 0.02%, i.e., two Secondary fermentation desugar terminates, and obtains secondary fermentation desugar liquid;
S8, take secondary fermentation desugar liquid and be spray-dried, obtain final products sugar-free natural product health-care powder.
CN201510071805.XA 2015-02-07 2015-02-07 A kind of preparation method of sugar-free natural product health-care powder Expired - Fee Related CN104664377B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510071805.XA CN104664377B (en) 2015-02-07 2015-02-07 A kind of preparation method of sugar-free natural product health-care powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510071805.XA CN104664377B (en) 2015-02-07 2015-02-07 A kind of preparation method of sugar-free natural product health-care powder

Publications (2)

Publication Number Publication Date
CN104664377A CN104664377A (en) 2015-06-03
CN104664377B true CN104664377B (en) 2017-06-16

Family

ID=53300382

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510071805.XA Expired - Fee Related CN104664377B (en) 2015-02-07 2015-02-07 A kind of preparation method of sugar-free natural product health-care powder

Country Status (1)

Country Link
CN (1) CN104664377B (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112369562A (en) * 2020-11-25 2021-02-19 龙海市金顺来食品有限公司 Processing technology of low-sugar puffed food
CN114982904B (en) * 2022-02-15 2023-08-01 滋养源食品科技(广东)有限公司 Low-sugar nutritional longan and egg noodles and preparation method thereof

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003204780A (en) * 2001-11-07 2003-07-22 Kyowa Hakko Kogyo Co Ltd Yeast and method for producing bread
CN102119741B (en) * 2011-01-19 2012-12-12 佳木斯大学 Edible fungi soy milk, edible fungi sugar-free soy flour and preparation method thereof
CN103070364A (en) * 2013-02-27 2013-05-01 河北农业大学 Liquid and powder persimmon tannin and separating extracting process thereof
CN103719751A (en) * 2013-12-04 2014-04-16 新疆楼兰庄园枣业有限公司 Preparation method for low-reducing sugar red jujube powder

Also Published As

Publication number Publication date
CN104664377A (en) 2015-06-03

Similar Documents

Publication Publication Date Title
KR100748263B1 (en) Grain syrup/taffy applying a pear and a platycodon and the manufacturing method thereof
JP4616413B1 (en) Fermented food manufacturing method and fermented food
CN104673594A (en) Production method of sweet tea wine
CN103103070B (en) Processing method of hawthorn fruit wine
KR100877374B1 (en) Mugwort vinegar and the manufacturing method
CN109251831A (en) A kind of jujube alcoholic drink mixed with fruit juice and its brew method
CN109527486A (en) A kind of passion fruit jam and preparation method
CN104012924B (en) A kind of phytoenzyme material wine and preparation method thereof
CN101824378B (en) Making method of passion fruit vinegar
CN104664377B (en) A kind of preparation method of sugar-free natural product health-care powder
CN105255631A (en) Method for preparing passion fruit and glutinous rice fermented wine
CN104997096A (en) Chinese fevervine sour soup beverage and preparation method thereof
CN101130728A (en) Wild jujube wine and method of producing the same
CN102311901B (en) Health-care low-alcohol-volume nutritional yellow wine with fruit fragrance
CN105238631A (en) Mandarin orange and glutinous rice wine
CN105255629A (en) Indian jujube fermented glutinous rice
CN112980641A (en) Method for making rice wine by using mulberry byproducts
CN110862900A (en) Preparation method and application of fruit and vegetable fermentation liquor
CN109182077A (en) Chick-pea vinegar and preparation method thereof
CN117322629B (en) Preparation method of horseshoe lipid-lowering composition based on fermentation enzymolysis technology
CN100453633C (en) Prepn process of yacon wine
KR100369637B1 (en) A manufacturing method of brewing vinegar using the main component as an extract from the medical buck wheat
CN101948723B (en) Garlic health wine and preparation method thereof
CN106360226A (en) Humulus scandens vinegar drink
CN106234599A (en) A kind of pitaya peel milk and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170616

Termination date: 20190207

CF01 Termination of patent right due to non-payment of annual fee