CN104663956A - Preparation method of frozen-dried quick-dissolving tea powder with red flowers and sea buckthorn - Google Patents
Preparation method of frozen-dried quick-dissolving tea powder with red flowers and sea buckthorn Download PDFInfo
- Publication number
- CN104663956A CN104663956A CN201510054854.2A CN201510054854A CN104663956A CN 104663956 A CN104663956 A CN 104663956A CN 201510054854 A CN201510054854 A CN 201510054854A CN 104663956 A CN104663956 A CN 104663956A
- Authority
- CN
- China
- Prior art keywords
- sea
- carry out
- buckthorn
- safflower
- leaves
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a preparation method of frozen-dried quick-dissolving tea powder with red flowers and sea buckthorn. According to the key points of the technical scheme, the preparation method comprises the following steps: taking red-flower velvet and sea-buckthorn processing slags as raw materials, utilizing water as an extraction medium to extract effective components in the red flowers, and carrying out refinement by purification and concentration; adopting ultrasonic waves to assist a compound-enzyme (cellulase and pectinase) extraction method to extract effective components in the sea-buckthorn branch and leaf slags, and carrying out concentration and foreign-matter removal on the effective components; and adopting a vacuum freezing method to carry out drying treatment, and finally adopting an ultra-micro crushing technology to carry out refinement, and thus obtaining the quick-dissolving tea powder. The preparation method has the advantages that the slags of red-flower leftover materials and the sea-buckthorn leaves are utilized, so that the resource waste is avoided; the quick-dissolving tea powder refined by ultramicro crushing is fine in taste and mellow in fragrance and has the nutritional value of the red flowers and the sea buckthorn.
Description
Technical field
The present invention relates to a kind of instant tea powder, particularly relate to a kind of safflower seabuckthorn freeze-dried instant tea powder.
Background technology
Safflower belongs to the dry tubular flower of feverfew, and history is loaded in " Kaibao Bencao ", " blood fortune lockjaw after main product, in abdomen, extravesated blood not to the utmost, and angina fails before being carrying out, and wine boils clothes, also blood under middle disease due to noxious agents produced by various parasites ".It has the multiple pharmacological effects such as coronary artery, hypotensive, resist oxygen lack, promoting blood circulation and removing blood stasis, anti-inflammatory and antalgic.
Containing multiple biochemical composition (flavonoids, fats, several amino acids, organic acid, unrighted acid) and abundant vitamin etc. in sea-buckthorn branches and leaves, there is good effect to the aspect such as human body immune function, antioxygenic property.
But a lot of leftover pieces can be left after safflower is processed, the disintegrating slag that sea-buckthorn branches and leaves stay after making sea-buckthorn tea, all also there is multiplex nutriment in the leftover pieces of safflower and the disintegrating slag of sea-buckthorn branches and leaves, just waste is caused if directly discarded, can be utilized so be badly in need of a kind of product, be avoided waste.
Summary of the invention
The technical problem to be solved in the present invention overcomes existing defect, provides a kind of safflower seabuckthorn freeze-dried instant tea powder.
A kind of safflower seabuckthorn freeze-dried instant tea powder, it is characterized in that, comprise the composition extracted the disintegrating slag of composition and the sea-buckthorn branches and leaves extracted in safflower leftover pieces, its manufacturing process comprises the following steps:
(1) first by the disintegrating slag of safflower leftover pieces and sea-buckthorn branches and leaves, cleaned and dried;
(2) utilize water to do extraction media and adopt active ingredient in reflux extraction safflower; Its step is as follows:
By the leftover bits and pieces in safflower process, pulverize after dry process, cross 40-80 mesh sieve, front and back add water in solid-liquid ratio 1:15-18, be lixiviate 1-2 hour at the temperature of 70-80 DEG C in temperature, front and back twice, merge leaching liquor, 500 order filtration treatment, leave standstill an evening, extract supernatant, cross D101 macroporous absorbent resin, regulate flow velocity 3B column volume/time; After upper prop terminates, the 3B column volume water yield is used to carry out rushing post removal of impurities; Adopt gradient method to carry out wash-out, alcohol gradient is 30%-35%, 80%, 95%; Collect eluent, eluent spirituosity concentration is 70-75%, leaves standstill 48 hours, and extract supernatant, recovered under reduced pressure thickening temperature is 50-65 DEG C, and concentrated amount is stored under refrigeration at 1/2,4 DEG C of original volume, extracts supernatant and is the clear cream of safflower;
(3) adopt the active ingredient in ultrasonic assistant multiplex-enzyme extraction method extraction sea-buckthorn branches and leaves disintegrating slag, its step is as follows:
By the leftover bits and pieces in sea-buckthorn tea processing process, carry out cleaning-drying process, cross 40-80 mesh sieve after pulverizing, 1:15 adds water in proportion, add the cellulase of 1-2%, pectase complex enzyme hydrolysis system 1.5-2:1, regulate pH to 4.5-5.0,50 DEG C of temperature enzymolysis 60-80min under ultrasonic power 500-600W power, raised temperature is to after boiling the ferment treatment 10min that goes out, stop heating, lixiviate 1 hour, every 20min stirs once, releases filtrate; Add water in 1:10 ratio in residue, at temperature is 80 DEG C, 1h is got in warm lixiviate, releases filtrate; Merging filtrate, left standstill for 1 evening, release precipitation, 500 suction filtrations now, carry out desalting processing by filtrate cationic ion-exchange resin and anion exchange resin, collect and flow through liquid, carry out ultrafiltration, be evaporated under 60-70 degree Celsius containing dry 30%-40%, concentrate 0-4 DEG C of refrigeration, extract supernatant and be hippophae rhamnoides;
(4) in active ingredient safflower leftover pieces extracted and sea-buckthorn branches and leaves disintegrating slag the active ingredient extracted carry out mixing according to the ratio of 4:6, homogeneous;
(5) by the material mixed through staticly settling, get supernatant and carry out freeze drying, ultramicro grinding is carried out to dry thing, be crushed to particle about 10 μm;
(6) pack.
Compared with prior art, the invention has the beneficial effects as follows: safflower is effectively combined with the nutritive value of sea-buckthorn, the extraction process of pure natural is utilized to be prepared, embody green, healthy theory, with discarded leftover bits and pieces for raw material, embody 18 large since thrifty, resource make full use of, the call of environmental protection, keep up with the trend of the times.The safflower seabuckthorn freeze-dried instant tea powder that the present invention obtains can be taken after mixing it with water in the hot water, tea powder particles≤10 μm after ultramicro grinding, solubility >=98%, possesses immunity moderation systemic-function, useful sleep, antifatigue, anti-aging, prevention cardiovascular and cerebrovascular disease, norcholesterol, hypotensive health care.
Detailed description of the invention
The following examples, are described in further detail the specific embodiment of the present invention.Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment one: accurately, unambiguously
(1) by the leftover bits and pieces in safflower process, pulverize after dry process, cross 50 mesh sieves, front and back add water in solid-liquid ratio 1:18,1:15 (g/g), are lixiviate 1h at the temperature of 80 DEG C in temperature, twice, front and back, merge leaching liquor, 500 order filtration treatment, leave standstill an evening, extract supernatant
(2) supernatant is crossed D101 large pore resin absorption column, regulate flow velocity 3B column volume/h; After upper prop terminates, the 3B column volume water yield is used to carry out rushing post removal of impurities; Alcohol gradient method is adopted to carry out wash-out; Collect eluent, eluent spirituosity concentration is 75%, leaves standstill 48 hours, extracts supernatant.
(3) gained elution supernatant 60 DEG C of recovered under reduced pressure concentrated, concentrated amount is 1/2 of original volume,
(4) stored under refrigeration at 0-4 DEG C, extracts supernatant for subsequent use.
(5) by the leftover bits and pieces in sea-buckthorn tea processing process, carry out cleaning-drying process, 40-80 mesh sieve is crossed after pulverizing, 1:15 adds water in proportion, add the cellulase of 1%, pectase complex enzyme hydrolysis system (1.5:1), regulate pH to 4.5,50 DEG C of temperature enzymolysis 60min under ultrasonic power 500W power.
(6) raised temperature is to boiling the ferment treatment 10min that goes out, after, stop heating, lixiviate 1h, every 20min stirs once, releases filtrate; Add water in 1:10 ratio in residue, at temperature is 80 DEG C, 1h is got in warm lixiviate, releases filtrate; Merging filtrate, left standstill for 1 evening.
(7) precipitation is released, 500 suction filtrations now, filtrate cationic ion-exchange resin and anion exchange resin are carried out desalting processing, liquid is flow through in collection, carry out ultrafiltration (0.45 micron, 0.2Mpa), 60 DEG C are evaporated to containing soluble solid 37%, concentrate 4 DEG C refrigeration, extracts supernatant and is hippophae rhamnoides.
(8) in 1:2 ratio mixing step (4), (7) gained clear liquid, add the beta-schardinger dextrin-of 8%, homogeneous process, carry out freeze drying.
(9) gained dry product carries out ultramicro grinding, makes its particle≤10 μm.
(10) aseptic packaging.
Embodiment two,
(1) by the leftover bits and pieces in safflower process, pulverize after dry process, cross 80 mesh sieves, front and back add water in solid-liquid ratio 1:15 (g/g), are lixiviate 1.5h at the temperature of 70 DEG C in temperature, twice, front and back, merge leaching liquor, 500 order filtration treatment, leave standstill an evening, extract supernatant
(2) supernatant is crossed D101 large pore resin absorption column, regulate flow velocity 3B column volume/h; After upper prop terminates, the 3B column volume water yield is used to carry out rushing post removal of impurities; Adopt alcohol gradient method to carry out wash-out, collect eluent, eluent spirituosity concentration is 70%, leaves standstill 48 hours, extracts supernatant.
(3) gained elution supernatant 60 DEG C of recovered under reduced pressure concentrated, concentrated amount is 1/2 of original volume,
(4) stored under refrigeration at 0-4 DEG C, extracts supernatant for subsequent use.
(5) by the leftover bits and pieces in sea-buckthorn tea processing process, carry out cleaning-drying process, 480 mesh sieves are crossed after pulverizing, 1:15 adds water in proportion, add the cellulase of 2%, pectase complex enzyme hydrolysis system (2:1), regulate pH to 4.5,50 DEG C of temperature enzymolysis 80min under ultrasonic power 550W power
(6) raised temperature is to boiling the ferment treatment 10min that goes out, after, stop heating, lixiviate 1h, every 20min stirs once, releases filtrate; Add water in 1:15 ratio in residue, at temperature is 80 DEG C, 1h is got in warm lixiviate, releases filtrate; Merging filtrate, left standstill for 1 evening.
(7) precipitation is released, 500 suction filtrations now, filtrate cationic ion-exchange resin and anion exchange resin are carried out desalting processing, liquid is flow through in collection, carry out ultrafiltration (0.45 micron, 0.2Mpa), 60 DEG C are evaporated to containing soluble solid about 30%, concentrate 4 DEG C refrigeration, extracts supernatant and is hippophae rhamnoides.
(8) in 2:3 ratio mixing step (4), (7) gained clear liquid, add the beta-schardinger dextrin-of 8%, homogeneous process, carry out freeze drying.
(9) gained dry product carries out ultramicro grinding, makes its particle≤10 μm.
(10) sterilizing, aseptic packaging.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (1)
1. a safflower seabuckthorn freeze-dried instant tea powder, is characterized in that, comprise the composition extracted the disintegrating slag of composition and the sea-buckthorn branches and leaves extracted in safflower leftover pieces, its manufacturing process comprises the following steps:
(1) first by the disintegrating slag of safflower leftover pieces and sea-buckthorn branches and leaves, cleaned and dried;
(2) utilize water to do extraction media and adopt active ingredient in reflux extraction safflower; Its step is as follows:
By the leftover bits and pieces in safflower process, pulverize after dry process, cross 40-80 mesh sieve, front and back add water in solid-liquid ratio 1:15-18, be lixiviate 1-2 hour at the temperature of 70-80 DEG C in temperature, front and back twice, merge leaching liquor, 500 order filtration treatment, leave standstill an evening, extract supernatant, cross D101 macroporous absorbent resin, regulate flow velocity 3B column volume/time; After upper prop terminates, the 3B column volume water yield is used to carry out rushing post removal of impurities; Adopt gradient method to carry out wash-out, alcohol gradient is 30%-35%, 80%, 95%; Collect eluent, eluent spirituosity concentration is 70-75%, leaves standstill 48 hours, and extract supernatant, recovered under reduced pressure thickening temperature is 50-65 DEG C, and concentrated amount is stored under refrigeration at 1/2,4 DEG C of original volume, extracts supernatant and is the clear cream of safflower;
(3) adopt the active ingredient in ultrasonic assistant multiplex-enzyme extraction method extraction sea-buckthorn branches and leaves disintegrating slag, its step is as follows:
By the leftover bits and pieces in sea-buckthorn tea processing process, carry out cleaning-drying process, cross 40-80 mesh sieve after pulverizing, 1:15 adds water in proportion, add the cellulase of 1-2%, pectase complex enzyme hydrolysis system 1.5-2:1, regulate pH to 4.5-5.0,50 DEG C of temperature enzymolysis 60-80min under ultrasonic power 500-600W power, raised temperature is to after boiling the ferment treatment 10min that goes out, stop heating, lixiviate 1 hour, every 20min stirs once, releases filtrate; Add water in 1:10 ratio in residue, at temperature is 80 DEG C, 1h is got in warm lixiviate, releases filtrate; Merging filtrate, left standstill for 1 evening, release precipitation, 500 suction filtrations now, carry out desalting processing by filtrate cationic ion-exchange resin and anion exchange resin, collect and flow through liquid, carry out ultrafiltration, be evaporated under 60-70 degree Celsius containing dry 30%-40%, concentrate 0-4 DEG C of refrigeration, extract supernatant and be hippophae rhamnoides;
(4) in active ingredient safflower leftover pieces extracted and sea-buckthorn branches and leaves disintegrating slag the active ingredient extracted carry out mixing according to the ratio of 4:6, homogeneous;
(5) by the material mixed through staticly settling, get supernatant and carry out freeze drying, ultramicro grinding is carried out to dry thing, be crushed to particle about 10 μm;
(6) pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510054854.2A CN104663956B (en) | 2015-02-02 | 2015-02-02 | Safflower seabuckthorn freeze-dried instant tea powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510054854.2A CN104663956B (en) | 2015-02-02 | 2015-02-02 | Safflower seabuckthorn freeze-dried instant tea powder |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104663956A true CN104663956A (en) | 2015-06-03 |
| CN104663956B CN104663956B (en) | 2018-04-03 |
Family
ID=53299961
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510054854.2A Active CN104663956B (en) | 2015-02-02 | 2015-02-02 | Safflower seabuckthorn freeze-dried instant tea powder |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104663956B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104996645A (en) * | 2015-08-30 | 2015-10-28 | 余芳 | Processing method of schisandra chinensis tea essence |
| CN108244295A (en) * | 2018-03-23 | 2018-07-06 | 青海康普生物科技股份有限公司 | A kind of preparation method of sea-buckthorn Fu tea |
| CN108902405A (en) * | 2018-06-26 | 2018-11-30 | 新疆超越歆生物科技有限公司 | The manufacture craft of lycium ruthenicum sea-buckthorn freeze-dried instant powder |
| CN109480017A (en) * | 2018-12-17 | 2019-03-19 | 邵阳学院 | A kind of Ramulus et Folium Mussaendae Pubescentis extract and the preparation method and application thereof |
| CN115005300A (en) * | 2022-05-17 | 2022-09-06 | 铜仁市印江青耕茶叶有限公司 | Internal heat-reducing scented tea and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101238842A (en) * | 2007-02-05 | 2008-08-13 | 高原圣果沙棘制品有限公司 | Sea-buckthorn instant tea and preparation thereof |
| CN103271187A (en) * | 2013-05-21 | 2013-09-04 | 宁波优美肽生物科技有限公司 | Enzyme immobilization method for preparing tea concentrated juice or instant tea powder |
| CN104189031A (en) * | 2014-09-04 | 2014-12-10 | 南京标科生物科技有限公司 | Method for extracting total flavones of hippophae rhamnoides from hippophae rhamnoides leaves |
-
2015
- 2015-02-02 CN CN201510054854.2A patent/CN104663956B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101238842A (en) * | 2007-02-05 | 2008-08-13 | 高原圣果沙棘制品有限公司 | Sea-buckthorn instant tea and preparation thereof |
| CN103271187A (en) * | 2013-05-21 | 2013-09-04 | 宁波优美肽生物科技有限公司 | Enzyme immobilization method for preparing tea concentrated juice or instant tea powder |
| CN104189031A (en) * | 2014-09-04 | 2014-12-10 | 南京标科生物科技有限公司 | Method for extracting total flavones of hippophae rhamnoides from hippophae rhamnoides leaves |
Non-Patent Citations (2)
| Title |
|---|
| 岳鹏翔等: "速溶茶提制技术研究发展及发展趋势", 《中国会议》 * |
| 武永刚等: "中压制备与大孔树脂联用快速分离羟基红花黄色素A", 《湖北农业科学》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104996645A (en) * | 2015-08-30 | 2015-10-28 | 余芳 | Processing method of schisandra chinensis tea essence |
| CN108244295A (en) * | 2018-03-23 | 2018-07-06 | 青海康普生物科技股份有限公司 | A kind of preparation method of sea-buckthorn Fu tea |
| CN108902405A (en) * | 2018-06-26 | 2018-11-30 | 新疆超越歆生物科技有限公司 | The manufacture craft of lycium ruthenicum sea-buckthorn freeze-dried instant powder |
| CN109480017A (en) * | 2018-12-17 | 2019-03-19 | 邵阳学院 | A kind of Ramulus et Folium Mussaendae Pubescentis extract and the preparation method and application thereof |
| CN115005300A (en) * | 2022-05-17 | 2022-09-06 | 铜仁市印江青耕茶叶有限公司 | Internal heat-reducing scented tea and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104663956B (en) | 2018-04-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101559157B (en) | Method for fractional extraction of asparagus saponin and asparagus amylose using asparagus slag | |
| CN104663956A (en) | Preparation method of frozen-dried quick-dissolving tea powder with red flowers and sea buckthorn | |
| CN109810201A (en) | The ultrasonic wave combination of acidic water extracting method of Cordyceps sinensis polysaccharide and cordycepin in a kind of Cordyceps militaris | |
| CN101053589B (en) | Method for extracting active constituent from Tibetan capillary | |
| CN103478838B (en) | Honeysuckle kudzuvine root beverage and preparation method thereof | |
| CN103435486A (en) | Novel method for preparing high-purity chlorogenic acid in honeysuckle | |
| CN102048885A (en) | Extraction process for lychee seed saponin | |
| CN104840501A (en) | Preparation method for total flavonoids of chrysanthemum | |
| CN103860631A (en) | Method for preparing liquorice active substances | |
| CN106720752A (en) | Camellia chrysantha beverage and preparation method thereof | |
| CN109645304A (en) | A kind of preparation method of mulberry leaf material for healthy food | |
| CN102304501A (en) | Complex enzyme preparation and application and method thereof for extracting plant polysaccharides by using same | |
| CN101503357A (en) | Method for extracting chlorogenic acid in honeysuckle | |
| CN102327312A (en) | Method for extracting effective ingredients from leaf, stem and vine of honeysuckle | |
| CN105732741B (en) | The method that perilla leaf extracts anthocyanin and ursolic acid | |
| CN109966327A (en) | A kind of method of the double assisted extraction passionflower seed oil meal general flavones of ultrasonic wave, microwave | |
| CN101352616B (en) | Method for preparing pine tree bark extract using barrier separation integrated process engineering | |
| CN102204950B (en) | Method for extracting flavonoid from liquorice waste residue | |
| CN106119429A (en) | A kind of production method of Radix Notoginseng sugar | |
| CN104098636B (en) | A kind of method extracting rutin in the Flos Sophorae Immaturus | |
| CN103333213A (en) | Method for extracting oleuropein from olive leaves | |
| CN110592167A (en) | Purslane polypeptide extract and preparation method thereof | |
| CN102614231A (en) | Method for preparing cynomorium songaricum terpene and cynomorium songaricum polysaccharose from cynomorium songaricum | |
| CN102477105A (en) | Method for combined preparation of polysaccharide and flavone by using pumpkin stems and leaves as raw material | |
| CN104857108A (en) | Method for preparing hawthorn extractive through continuous countercurrent ultrasonic equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180625 Address after: 831100 the Xinjiang Uygur Autonomous Region, Changji, Changji, Jimsar County [twelve district] and the south side of the Mancheng road and the Democratic Road, the south side of the green landscape Jiayuan residential quarter 7 merchants 8 (only for office use) Patentee after: Xinjiang Xin beyond biological technology Co. Ltd. Address before: 831100 the Xinjiang Uygur Autonomous Region Changji Hui Autonomous Prefecture Jimsar County Mancheng Road Flower Garden Green Garden 7 building two building tenth room. Patentee before: Jimusar County productivity promotion center (Co., Ltd) |
|
| TR01 | Transfer of patent right |