CN104651049A - Preparation of essence having fragrance of carnation - Google Patents

Preparation of essence having fragrance of carnation Download PDF

Info

Publication number
CN104651049A
CN104651049A CN201310587943.4A CN201310587943A CN104651049A CN 104651049 A CN104651049 A CN 104651049A CN 201310587943 A CN201310587943 A CN 201310587943A CN 104651049 A CN104651049 A CN 104651049A
Authority
CN
China
Prior art keywords
isoeugenol
essence
present
rhodinol
eugenol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201310587943.4A
Other languages
Chinese (zh)
Inventor
唐青
姜文海
高桂新
唐铖
高维昆
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANJIN BOLAIEN TECHNOLOGY DEVELOPMENT Co Ltd
Original Assignee
TIANJIN BOLAIEN TECHNOLOGY DEVELOPMENT Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TIANJIN BOLAIEN TECHNOLOGY DEVELOPMENT Co Ltd filed Critical TIANJIN BOLAIEN TECHNOLOGY DEVELOPMENT Co Ltd
Priority to CN201310587943.4A priority Critical patent/CN104651049A/en
Publication of CN104651049A publication Critical patent/CN104651049A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0042Essential oils; Perfumes compounds containing condensed hydrocarbon rings
    • C11B9/0046Essential oils; Perfumes compounds containing condensed hydrocarbon rings containing only two condensed rings
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0061Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)

Abstract

The invention aims to prepare of an essence having a fragrance of carnation. The essence is composed of eugenol, isoeugenol, vanillin, benzyl salicylate, phenethyl alcohol, rhodinol, ionone, isoeugenol ether, hydroxyl citronellal, terpilenol, heliotropin, natural jasmine paste, isoeugenol acetate, anisic aldehyde and methyl ionone. The essence is a yellow oily transparent liquid, is stable in performance, can be used as a fragrant additive in hard candies, biscuits and other baking foods, and cosmetics, detergents and industrial and the like products. The preparation method is free of waste gas, waste water and solid waste and is in conformity with a national environmental production standard.

Description

A kind of essence with carnation fragrance makes
[technical field]
The invention reside in and manufacture the making of a kind of essence with carnation fragrance.
[background technology]
Carnation, has another name called chimera China pink, carnation, great Hua China pink, carnation.For Caryophyllaceae, carnation, be distributed in the ground such as the Fujian of European temperate zone and China's Mainland, Hubei, originating in Mediterranean Zone, is apply one of the most general flowers in the world at present.Carnation comprises many mutation and cross-fertilize seed, almost can successively bloom in greenhouse.
[summary of the invention]
The present invention is characterized in that being made up of Eugenol, isoeugenol, vanillin food grade,1000.000000ine mesh, benzyl salicylate, phenylethyl alcohol, rhodinol, jononeionone, isoeugenol ether, laurine, Terpineol 350, piperonal, natural jasmine cream, acetyl isoeugenol, anisyl aldehyde, methylionone.。
The present invention is yellow oily transparent liquid, pH value 6-8, stability 42 DEG C of envrionment temperatures: 24 hours not stratified; 0 DEG C of envrionment temperature: do not freeze.
The present invention can do odor additive at hard candy, biscuit and other bakery etc., and general consumption is 0.1-0.2%; Can do odor additive in the products such as makeup, washing composition, commercial auxiliaries, general consumption is 0.3-0.5%.
In manufacturing processed of the present invention, without waste gas, waste water, solid waste, meet national environmental protection production standard.
The weight percent of the present invention's composition: Eugenol 24-27%, isoeugenol 6-8%, vanillin food grade,1000.000000ine mesh 0.5-1.5%, benzyl salicylate 12-14%, phenylethyl alcohol 3-4%, rhodinol 11-13%, jononeionone 6-8%, isoeugenol ether 6-8%, laurine 2-4%, Terpineol 350 2-4%, piperonal 2-4%, natural jasmine cream 4-6%, acetyl isoeugenol 0.5-1.5%, anisyl aldehyde 0.3-0.6%, methylionone 6-8%.
Manufacture craft of the present invention is: in essence special batching retort, add Eugenol, isoeugenol, vanillin food grade,1000.000000ine mesh, benzyl salicylate, phenylethyl alcohol, rhodinol, jononeionone, isoeugenol ether, laurine, Terpineol 350, piperonal, natural jasmine cream, acetyl isoeugenol, anisyl aldehyde, methylionone successively, stir 60 minutes, batching retort stirs speed of rotation and controls at 60 revs/min; Whole manufacture craft temperature remains on 40 ± 2 DEG C.After reaction terminates, sampling and measuring Specifications, qualified rear filtration loads packaging.
[embodiment]
Embodiment 1
Formula: Eugenol 26.32%, isoeugenol 7.37%, vanillin food grade,1000.000000ine mesh 1.05%, benzyl salicylate 13.16%, phenylethyl alcohol 3.16%, rhodinol 12.63%, jononeionone 6.32%, isoeugenol ether 7.37%, laurine 2.63%, Terpineol 350 2.63%, piperonal 2.63%, natural jasmine cream 5.26%, acetyl isoeugenol 1.05%, anisyl aldehyde 0.53%, methylionone 7.89% form.
Manufacture craft: in essence special batching retort, add Eugenol 26.32 kilograms successively, isoeugenol 7.3 kilograms, vanillin food grade,1000.000000ine mesh 1.05 kilograms, benzyl salicylate 13.16 kilograms, phenylethyl alcohol 3.15 kilograms, rhodinol 12.63 kilograms, jononeionone 6.32 kilograms, isoeugenol ether 7.37 kilograms, laurine 2.63 kilograms, Terpineol 350 2.63 kilograms, piperonal 2.63 kilograms, natural jasmine cream 5.26 kilograms, acetyl isoeugenol 1.05 kilograms, anisyl aldehyde 0.53 kilogram, methylionone 7.89 kilograms, stir 60 minutes, batching retort stirs speed of rotation and controls at 60 revs/min, whole manufacture craft temperature remains on 40 ± 2 DEG C.After reaction terminates, sampling and measuring Specifications, qualified rear filtration loads packaging.
Embodiment 2
Formula: Eugenol 26.90%, isoeugenol 6.42%, vanillin food grade,1000.000000ine mesh 0.95%, benzyl salicylate 11.24%, phenylethyl alcohol 3.05%, rhodinol 11.24%, jononeionone 5.68%, isoeugenol ether 8.45%, laurine 3.34%, Terpineol 350 3.34%, piperonal 3.34%, natural jasmine cream 4.98%, acetyl isoeugenol 0.95%, anisyl aldehyde 1.67%, methylionone 8.45% form.
manufacture craft: in essence special batching retort, add Eugenol 26.90 kilograms successively, isoeugenol 6.42 kilograms, vanillin food grade,1000.000000ine mesh 0.95 kilogram, benzyl salicylate 11.24 kilograms, phenylethyl alcohol 3.05 kilograms, rhodinol 11.24 kilograms, jononeionone 5.68 kilograms, isoeugenol ether 8.45 kilograms, laurine 3.34 kilograms, Terpineol 350 3.34 kilograms, piperonal 3.34 kilograms, natural jasmine cream 4.98 kilograms, acetyl isoeugenol 0.95 kilogram, anisyl aldehyde 1.67 kilograms, methylionone 8.45 kilograms, stir 60 minutes, batching retort stirs speed of rotation and controls at 60 revs/min, whole manufacture craft temperature remains on 40 ± 2 DEG C.After reaction terminates, sampling and measuring Specifications, qualified rear filtration loads packaging.

Claims (7)

1. the invention reside in and manufacture the making of a kind of essence with carnation fragrance.
2. according to claim 1, the present invention is characterized in that being made up of Eugenol, isoeugenol, vanillin food grade,1000.000000ine mesh, benzyl salicylate, phenylethyl alcohol, rhodinol, jononeionone, isoeugenol ether, laurine, Terpineol 350, piperonal, natural jasmine cream, acetyl isoeugenol, anisyl aldehyde, methylionone.
3. according to claim 1, weight percent proportioning of the present invention: Eugenol 24-27%, isoeugenol 6-8%, vanillin food grade,1000.000000ine mesh 0.5-1.5%, benzyl salicylate 12-14%, phenylethyl alcohol 3-4%, rhodinol 11-13%, jononeionone 6-8%, isoeugenol ether 6-8%, laurine 2-4%, Terpineol 350 2-4%, piperonal 2-4%, natural jasmine cream 4-6%, acetyl isoeugenol 0.5-1.5%, anisyl aldehyde 0.3-0.6%, methylionone 6-8%.
4. according to claim 1, manufacture craft of the present invention is: in essence special batching retort, add Eugenol, isoeugenol, vanillin food grade,1000.000000ine mesh, benzyl salicylate, phenylethyl alcohol, rhodinol, jononeionone, isoeugenol ether, laurine, Terpineol 350, piperonal, natural jasmine cream, acetyl isoeugenol, anisyl aldehyde, methylionone successively, stir 60 minutes, batching retort stirs speed of rotation and controls at 60 revs/min; Whole manufacture craft temperature remains on 40 ± 2 DEG C; After reaction terminates, sampling and measuring Specifications, qualified rear filtration loads packaging.
5. according to claim 1, the present invention is yellow oily transparent liquid, pH value 6-8, stability 42 DEG C of envrionment temperatures: 24 hours not stratified; 0 DEG C of envrionment temperature: do not freeze.
6. according to claim 1, the present invention can do odor additive at hard candy, biscuit and other bakery etc., and general consumption is 0.1-0.2%; Can do odor additive in the products such as makeup, washing composition, commercial auxiliaries, general consumption is 0.3-0.5%.
7., according to claim 1, in manufacturing processed of the present invention, without waste gas, waste water, solid waste, meet national environmental protection production standard.
CN201310587943.4A 2013-11-21 2013-11-21 Preparation of essence having fragrance of carnation Pending CN104651049A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310587943.4A CN104651049A (en) 2013-11-21 2013-11-21 Preparation of essence having fragrance of carnation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310587943.4A CN104651049A (en) 2013-11-21 2013-11-21 Preparation of essence having fragrance of carnation

Publications (1)

Publication Number Publication Date
CN104651049A true CN104651049A (en) 2015-05-27

Family

ID=53242702

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310587943.4A Pending CN104651049A (en) 2013-11-21 2013-11-21 Preparation of essence having fragrance of carnation

Country Status (1)

Country Link
CN (1) CN104651049A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109069386A (en) * 2016-04-20 2018-12-21 株式会社 Lg 生活健康 Spice composition

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109069386A (en) * 2016-04-20 2018-12-21 株式会社 Lg 生活健康 Spice composition
CN109069386B (en) * 2016-04-20 2022-02-25 株式会社 Lg 生活健康 Perfume composition

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20150527

WD01 Invention patent application deemed withdrawn after publication