CN104631147A - Buffering type substitution alkali and preparation method thereof - Google Patents

Buffering type substitution alkali and preparation method thereof Download PDF

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Publication number
CN104631147A
CN104631147A CN201410073057.4A CN201410073057A CN104631147A CN 104631147 A CN104631147 A CN 104631147A CN 201410073057 A CN201410073057 A CN 201410073057A CN 104631147 A CN104631147 A CN 104631147A
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CN
China
Prior art keywords
alkali
type substitution
buffering type
fixation
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410073057.4A
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Chinese (zh)
Inventor
何德军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Foshan Defulong Chemical Technology Co Ltd
Original Assignee
Foshan Defulong Chemical Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Foshan Defulong Chemical Technology Co Ltd filed Critical Foshan Defulong Chemical Technology Co Ltd
Priority to CN201410073057.4A priority Critical patent/CN104631147A/en
Publication of CN104631147A publication Critical patent/CN104631147A/en
Pending legal-status Critical Current

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Abstract

The invention discloses buffering type substitution alkali and a preparation method thereof. The buffering type substitution alkali is prepared from the following components in percentage by weight: 65% of potassium hydroxide, 17% of potassium carbonate, 10% of potassium citrate and 8% of acrylate. According to the buffering type substitution alkali, the color fixation rate is increased, an ingredient having the buffering property is added, so that process of color fixation of reactive dyes is slow, the color fixation uniformity is ensured in the state and the dyeing defect cannot be caused easily.

Description

Buffer-type substitute alkali and manufacture method thereof
Technical field
The present invention relates to a kind of substitute alkali and manufacture method thereof, particularly relate to a kind of buffer-type substitute alkali and manufacture method thereof.
Background technology
Substitute alkali can be called dyeing alkali, when substitute alkali is based on textile printing and dyeing reactive dyeing, substitute industrial soda fixation, use amount is 1/10th of soda ash, reduces COD of sewage (COD) value, production cost can be saved, reduce labor strength, substitute alkali Color is not good in the early time, is embodied in: color is too shallow, dyeing coloured light is out unstable, causes uneven color (look flower, two tone colour) than being easier to.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of buffer-type substitute alkali and manufacture method thereof, it is except promoting degree of fixation, slow fixation when adding acrylates with the composition of buffering property to ensure reactive dye color fixing, fixation can ensure that fixation is even in this state, not easily look flower.
The present invention solves above-mentioned technical problem by following technical proposals: a kind of buffer-type substitute alkali, is characterized in that, it comprises following component, by weight percentage:
The present invention also provides a kind of manufacture method of buffer-type substitute alkali, it is characterized in that, it comprises the following steps: add potassium hydroxide, potash, potassium citrate and acrylates successively to reactor, stirs 60 minutes, puts into 2KG plastic bag or 25KG plastic bag packaging.
Positive progressive effect of the present invention is: the present invention is except substituting traditional sodium carbonate, under the prerequisite that degree of fixation is close, ensure that reactive dye color fixing uniformity, product is originally with it with PH buffering property, fixation uniformity has exceeded sodium carbonate, can reduce product defect rate.
Detailed description of the invention
Buffer-type substitute alkali of the present invention comprises following component, by weight percentage:
Reactive dyeing sodium carbonate and substitute alkali fixation PH change contrast as shown in table 1.
Table 1
Note: 1. add alkali number of times three times, adds in 1/10,3/10,6/10 ratio respectively.
2. sodium sulphate plays short dye (colouring) effect when vital staining, alkali (sodium carbonate, a substitute alkali) tint retention, thus the colouring principle of REACTIVE DYES be first on contaminate fixation again.
By above-mentioned pH value change contrast, the initial pH value ascensional range of substitute alkali is little, and now the change of pH value has certain influence to fixation uniformity.PH value initially rises too fast, the quick set of dyestuff.Be unfavorable for even dyeing.From dyeing theory, when the pH value change of substitute alkali is favourable dye fixing, continue even look, to reach maximum even dyeing effect.
Fixation formula of liquid is as shown in table 2 below.
Table 2
The manufacture method of buffer-type substitute alkali of the present invention comprises the following steps: add potassium hydroxide, potash, potassium citrate and acrylates successively to reactor, stirs 60 minutes, puts into 2KG plastic bag or 25KG plastic bag packaging.
The present invention is except substituting traditional sodium carbonate, and under the prerequisite that degree of fixation is close, ensure that reactive dye color fixing uniformity, product is originally with it with PH buffering property, and fixation uniformity has exceeded sodium carbonate, can reduce product defect rate.
Those skilled in the art can carry out various remodeling and change to the present invention.Therefore, present invention covers the various remodeling in the scope falling into appending claims and equivalent thereof and change.

Claims (2)

1. a buffer-type substitute alkali, is characterized in that, it comprises following component, by weight percentage:
2. a manufacture method for buffer-type substitute alkali, is characterized in that, it comprises the following steps: add potassium hydroxide, potash, potassium citrate and acrylates successively to reactor, stirs 60 minutes, puts into 2KG plastic bag or 25KG plastic bag packaging.
CN201410073057.4A 2013-11-11 2014-02-27 Buffering type substitution alkali and preparation method thereof Pending CN104631147A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410073057.4A CN104631147A (en) 2013-11-11 2014-02-27 Buffering type substitution alkali and preparation method thereof

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CN201310576695 2013-11-11
CN2013105766953 2013-11-11
CN201410073057.4A CN104631147A (en) 2013-11-11 2014-02-27 Buffering type substitution alkali and preparation method thereof

Publications (1)

Publication Number Publication Date
CN104631147A true CN104631147A (en) 2015-05-20

Family

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Application Number Title Priority Date Filing Date
CN201410073057.4A Pending CN104631147A (en) 2013-11-11 2014-02-27 Buffering type substitution alkali and preparation method thereof

Country Status (1)

Country Link
CN (1) CN104631147A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110306359A (en) * 2019-07-10 2019-10-08 广东湛丰精细化工有限公司 It is a kind of for the alkali donor of reactive dyeing, preparation method and applications

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5372611A (en) * 1992-09-30 1994-12-13 Apollo Chemical Corporation Liquid alkali for reactive dyeing of textiles
US5603736A (en) * 1992-04-27 1997-02-18 Burlington Chemical Co., Inc. Liquid alkali for reactive dyeing of textiles
CN102251417A (en) * 2011-05-25 2011-11-23 石狮市清源精细化工有限公司 Color fixing substitution alkali for low-salt dyeing by using reactive dye pad steaming process

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5603736A (en) * 1992-04-27 1997-02-18 Burlington Chemical Co., Inc. Liquid alkali for reactive dyeing of textiles
US5372611A (en) * 1992-09-30 1994-12-13 Apollo Chemical Corporation Liquid alkali for reactive dyeing of textiles
CN102251417A (en) * 2011-05-25 2011-11-23 石狮市清源精细化工有限公司 Color fixing substitution alkali for low-salt dyeing by using reactive dye pad steaming process

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
禚子瑜等: "代用碱的配制及应用性能", 《印染助剂》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110306359A (en) * 2019-07-10 2019-10-08 广东湛丰精细化工有限公司 It is a kind of for the alkali donor of reactive dyeing, preparation method and applications

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Application publication date: 20150520