CN104624026B - A kind of air purifying preparation and preparation method thereof - Google Patents
A kind of air purifying preparation and preparation method thereof Download PDFInfo
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- CN104624026B CN104624026B CN201510049426.0A CN201510049426A CN104624026B CN 104624026 B CN104624026 B CN 104624026B CN 201510049426 A CN201510049426 A CN 201510049426A CN 104624026 B CN104624026 B CN 104624026B
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Abstract
The invention discloses a kind of air purifying preparation and preparation method thereof, raw material of the air purifying preparation comprising following mass ratio：100 parts of activated carbon, 10 20 parts of attapulgite, 5 10 parts of surfactant sodium dodecyl base benzene sulfonic acid sodium salt, 24 parts of additive glucose, 5 10 parts of purification of air active constituent titanium dioxide, 12 parts of Zinc Oxide, 0.5 1 parts of cerium oxide.The air purifying preparation is synthesized by chemical method, with attapulgite and activated carbon as compound adsorbent, there is stronger absorbability to pollutants in air, it is compounded with Multimetal oxide simultaneously, including titanium oxide, Zinc Oxide and cerium oxide, efficiently can go to eliminate the unusual smell, while producing anion beneficial to health in a large number.
Description
Technical field
The present invention relates to air purifying preparation technical field, and in particular to it is a kind of go to eliminate the unusual smell, the sky of sustained release anion
The preparation method of gas cleanser.
Background technology
Currently, air pollution（Such as haze, PM2.5 is exceeded）Daily life, many respiratory tracts are badly influenced
Disease causes very major injury to human body, therefore, seeking effective air purifying preparation becomes a kind of inexorable trend.
Titanium dioxide is a kind of catalysis material of excellent performance, is a kind of active ingredient in air purifying preparation,
CN103446874A discloses the preparation method of nanometer titanium dioxide complex air-purifying agent, and CN102151562A discloses one kind
The carbon fiber cloth material of composite titanium dioxide, used as air purifying preparation, it is net that CN103190442A discloses composite antibacterial type air
The preparation method of agent.Above-mentioned patent employs titanium dioxide as catalysis material, by Physical mixed rare-earth materials,
For purify air has good action.Chemical synthesiss be it is a kind of can effectively compositing organic material and inorganic material means,
Can excellent, the cheap composite of rapid batch preparation multiple performance.
Therefore, finding a kind of environmental protection, the air purifying preparation of the anion that efficiently goes to eliminate the unusual smell, produce becomes environment-friendly materials
A kind of urgent needss in field.
The content of the invention
It is an object of the invention to：A kind of air purifying preparation and preparation method thereof is provided, with reference to organic chemistry modification technology
And the advantageous property of inorganic material, rapid batch preparation Compound Punch rod soil, activated carbon, surfactant, glucose, dioxy
Change the air purifying preparation of titanium, Zinc Oxide and cerium oxide.
Technical scheme：First, in a certain amount of water, surfactant sodium dodecyl base benzene sulfonic acid sodium salt, Portugal are added
Grape sugar, warming-in-water, stirring obtain solution A；Secondly, organic titanate, zinc nitrate are sequentially added in a certain amount of concentrated nitric acid with
And cerous nitrate, it is stirred vigorously and obtains solution B；Then, solution A is poured in solution B, water-bath temperature control, mixing stands a period of time
Afterwards, pH value of solution is adjusted to neutrality, obtain suspension C；Subsequently, C Jing are filtered and are obtained filter cake and add into ethanol, add activated carbon and
Attapulgite, stirring temperature control keep alcohol reflux for a period of time, obtain suspension D；Finally, D is filtered, obtains filter cake Jing bakings
It is dry, air purifying preparation is obtained.
The present invention compared with prior art, with remarkable advantage：One, the air purifying preparation are with attapulgite and activated carbon
For compound adsorbent, there is stronger absorbability to pollutants in air；Second, the air purifying preparation is compounded with various metals oxygen
Compound, including titanium oxide, Zinc Oxide and cerium oxide, efficiently can go to eliminate the unusual smell, at the same produce in a large number it is beneficial to human body bear from
Son.
Specific embodiment
The technical solution of the present invention is illustrated with reference to specific embodiment, these embodiments are it is not intended that to technology
The restriction of scheme.
Embodiment 1：A kind of air purifying preparation is prepared according to step in detail below.
Step 1, in 200mL water, add 15g surfactant sodium dodecyl base benzene sulfonic acid sodium salts, 2g glucoses, warming-in-water
To 60oC, stirring, obtain homogeneous phase solution A；
Step 2,20g butyl titanates, six hydration of 2.5g zinc nitrates and 1.5g are sequentially added in 40mL60% concentration nitric acid
Cerous nitrate, is stirred vigorously and obtains solution B；
Step 3, solution A is poured in solution B, water-bath temperature control 60oC, after mixing stands 12h, hydro-oxidation sodium adjusts molten
Liquid pH obtains suspension C to neutrality；
Step 4, C Jing filtrations obtain wet cake and add into 200mL ethanol, add 100g activated carbons and 10g attapulgites,
Mechanical agitation, temperature control keep alcohol reflux 2h, obtain suspension D；
Step 5, D is filtered, obtain filter cake Jing 80oC is dried, and air purifying preparation is obtained.
Embodiment 2：A kind of air purifying preparation is prepared according to step in detail below.
Step 1, in 200mL water, add 30g surfactant sodium dodecyl base benzene sulfonic acid sodium salts, 4g glucoses, warming-in-water
To 40oC, stirring, obtain homogeneous phase solution A；
Step 2,40g butyl titanates, six nitric hydrate of 5g zinc nitrates and 3g are sequentially added in 60mL50% concentration nitric acid
Cerium, is stirred vigorously and obtains solution B；
Step 3, solution A is poured in solution B, water-bath temperature control 40oC, after mixing stands 48h, hydro-oxidation sodium adjusts molten
Liquid pH obtains suspension C to neutrality；
Step 4, C Jing filtrations obtain wet cake and add into 200mL ethanol, add 100g activated carbons and 20g attapulgites,
Mechanical agitation, temperature control keep alcohol reflux 4h, obtain suspension D；
Step 5, D is filtered, obtain filter cake Jing 90oC is dried, and air purifying preparation is obtained.
Embodiment 3：A kind of air purifying preparation is prepared according to step in detail below.
Step 1, in 200mL water, add 20g surfactant sodium dodecyl base benzene sulfonic acid sodium salts, 3g glucoses, warming-in-water
To 50oC, stirring, obtain homogeneous phase solution A；
Step 2,30g butyl titanates, six nitric hydrate of 4g zinc nitrates and 2g are sequentially added in 5mL55% concentration nitric acid
Cerium, is stirred vigorously and obtains solution B；
Step 3, solution A is poured in solution B, water-bath temperature control 60oC, after mixing stands 36h, hydro-oxidation sodium adjusts molten
Liquid pH obtains suspension C to neutrality；
Step 4, C Jing filtrations obtain wet cake and add into 200mL ethanol, add 100g activated carbons and 15g attapulgites,
Mechanical agitation, temperature control keep alcohol reflux 2h, obtain suspension D；
Step 5, D is filtered, obtain filter cake Jing 85oC is dried, and air purifying preparation is obtained.
Claims (3)
1. a kind of air purifying preparation, it is characterised in that its product formula is constituted, quality component includes：100 parts of activated carbon, attapulgite
Native 10-20 parts, surfactant sodium dodecyl base benzene sulfonic acid sodium salt 5-10 parts, additive glucose 2-4 parts, purification of air active constituent
Titanium dioxide 5-10 parts, Zinc Oxide 1-2 part, cerium oxide 0.5-1 parts.
2. a kind of air purifying preparation according to claim 1, its raw material are constituted, and quality component includes：100 parts of activated carbon,
Attapulgite 10-20 parts, surfactant sodium dodecyl base benzene sulfonic acid sodium salt 5-10 parts, additive glucose 2-4 parts, butyl titanate
20-40 parts, zinc nitrate 2.5-5 parts, six nitric hydrate cerium 1.5-3 parts.
3. a kind of preparation method of air purifying preparation, it is characterised in that comprise the steps of：
The first step：In a certain amount of water, surfactant sodium dodecyl base benzene sulfonic acid sodium salt, glucose, warming-in-water 40-60 are addedoC、
Stirring, obtains solution A；
Second step：In nitric acid of a certain amount of mass concentration for 50%-60%, butyl titanate, zinc nitrate and nitric acid are sequentially added
Cerium, is stirred vigorously and obtains solution B；
3rd step：Solution A is poured in solution B, water-bath temperature control 40-60oC, after mixing stands 12-48h, regulation pH value of solution is into
Property, obtain suspension C；
4th step：C Jing filtrations obtain filter cake and add into ethanol, add activated carbon and attapulgite, stirring, temperature control to keep ethanol
Backflow 2-4h, obtains suspension D；
5th step：D is filtered, filter cake drying is obtained, air purifying preparation is obtained.
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106824155A (en) * | 2015-12-07 | 2017-06-13 | 山东佳星环保科技有限公司 | A kind of preparation method of composite air cleanser |
| CN106139893A (en) * | 2016-07-13 | 2016-11-23 | 吴美燕 | A kind of preparation method of the effervesce air purifying preparation removing pernicious gas |
| CN106110883A (en) * | 2016-07-13 | 2016-11-16 | 吴美燕 | A kind of preparation method of the air purifying preparation removing harmful gas |
| CN106665653A (en) * | 2016-12-15 | 2017-05-17 | 龚娟 | Preparation method of odor-less disinfection solution |
| CN106902736A (en) * | 2017-03-04 | 2017-06-30 | 南京市雨花台区绿宝工业设计服务中心 | A kind of preparation method of composite material for air cleaning |
| CN107008139A (en) * | 2017-05-19 | 2017-08-04 | 深圳市天得环境科技有限公司 | Air-deodouring agent |
| CN108246046B (en) * | 2018-01-25 | 2021-05-14 | 广州然益生物科技有限公司 | Sterilizing air purifying agent and preparation method and application thereof |
| CN113769706A (en) * | 2021-08-31 | 2021-12-10 | 南京信息工程大学 | Air purification material and preparation method thereof |
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| KR100271137B1 (en) * | 1998-06-24 | 2000-11-01 | 유병택 | Trichosporonoides media ds911 and method for producing erythritol using the same |
| JP2000070729A (en) * | 1998-08-27 | 2000-03-07 | Nec Corp | Catalyst for environmental improvement and air purifying device using the environment catalyst |
| JP3352421B2 (en) * | 1999-02-04 | 2002-12-03 | 静雄 宇山 | Toilet paper and manufacturing method thereof |
| CN102502678A (en) * | 2011-09-21 | 2012-06-20 | 镇江忆诺唯记忆合金有限公司 | Preparation method of nanometer TiO2-ATP (Adenosine Triphosphate) powder material |
| CN103495387A (en) * | 2013-08-30 | 2014-01-08 | 蚌埠凤凰滤清器有限责任公司 | Easily dispersible modified activated carbon adsorbent and its preparation method |
| CN103721759B (en) * | 2014-01-07 | 2015-12-30 | 中国人民解放军防化学院 | A kind of air purifying preparation and preparation method thereof |
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Inventor after: Guo Junli Inventor after: Zhuansun Haihong Inventor after: Wang Lihua Inventor after: Guo Genzuo Inventor before: Gong Juan |
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Effective date of registration: 20170228 Address after: 257200 Dongsheng Shandong Shengli oil field oil production management area Applicant after: Guo Junli Address before: A small road in Yuhuatai District of Nanjing City, Jiangsu province 210000 City family No. 58 2-505 Applicant before: Gong Juan |
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