CN104596808A - Rotary gas diffusion and continuous capture device - Google Patents

Rotary gas diffusion and continuous capture device Download PDF

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Publication number
CN104596808A
CN104596808A CN201510038288.6A CN201510038288A CN104596808A CN 104596808 A CN104596808 A CN 104596808A CN 201510038288 A CN201510038288 A CN 201510038288A CN 104596808 A CN104596808 A CN 104596808A
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China
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rotary
micro pump
gas
anemostat
quartz ampoule
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CN201510038288.6A
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Chinese (zh)
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董华斌
曾立民
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Institute of Atmospheric Physics of CAS
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Institute of Atmospheric Physics of CAS
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Priority to CN201510038288.6A priority Critical patent/CN104596808A/en
Publication of CN104596808A publication Critical patent/CN104596808A/en
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Abstract

The invention relates to a rotary gas diffusion and continuous capture device. The rotary gas diffusion and continuous capture device comprises a rotary diffusion tube, wherein the rotary diffusion tube is arranged in a groove-shaped support, a stepper motor is installed at one end of the groove-shaped support, and the output end of the stepper motor is connected with the input end of the rotary diffusion tube; a constant-temperature air supply device is arranged on the outer wall surface of the rotary diffusion tube; the absorption liquid inlet of the rotary diffusion tube is connected with the output end of a first micro pump, and the input end of the first micro pump is connected with an absorption liquid storage bottle; the absorption liquid outlet of the rotary diffusion tube is connected with a quantitative collector through a second micro pump, and the output end of the quantitative collector is connected with a gaseous pollutant sample continuous outlet through a third micro pump; the rotary diffusion tube is further connected with a gas flow controller, and the gas flow controller is connected with a gas extraction sampling pump; the stepper motor, the constant-temperature air supply device, the first micro pump, the second micro pump, the third micro pump, the sample quantitative collector, the gas flow controller and the gas extraction sampling pump are all connected with a peripheral drive control circuit, and the peripheral drive control circuit is connected with an upper computer.

Description

A kind of rotary gas spreads continuous capturing device
Technical field
The present invention relates to a kind of gas diffusion capturing device, particularly relate to a kind of rotary gas and spread continuous capturing device.
Background technology
Atmospheric water dissolubility gaseous contaminant mainly comprises gaseous ammonia (NH 3), sulphuric dioxide (SO 2), gaseous state nitric acid (HNO 3), gaseous state nitrous acid (HNO 2), gaseous hydrochloric acid (HCl), gaseous state organic acid (formic acid, acetic acid, oxalic acid etc.) etc., their concentration is in an atmosphere low, harm is large, how to its accurate acquisition with to measure be key issue in current environmental monitoring.In atmospheric environment, the state that primary water-soluble gaseous contaminant and airborne particulate state pollutant, common gases etc. are in Homogeneous phase mixing, balance each other, the prerequisite of its concentration of Accurate Determining gets rid of the interference, the particularly interference of particulate form pollutant of other materials in mixed state.Conventional solid detention method and condensation at low temperature all can not separating gaseous and particulate form atmosphere pollutions effectively, and during sampling, mutual interference ratio is between the two comparatively large, and collection efficiency is not high.And spread apart trapping technique can get rid of the interference between gas and particle well, be applied to the sampling of Atmospheric Trace pollutant in recent years.
The theoretical foundation of diffusion trapping technique is that gas and particle rate of diffusion difference are very large, in certain stroke range, gas is far longer than particle in the diffusion of air-flow longitudinal direction, now select particular absorber to catch the fast species of gases of diffusion at longitudinal direction, thus reach the object being separated noiseless divided gas flow and particle.Difform anemostat is had according to such principle design, absorbing agent is attached to anemostat inwall, gas molecule is diffused on tube wall trapped by absorbing agent, and particle is unaffected, can one straight through anemostat, measured by corresponding detecting instrument by the gas that absorbing agent traps, thus the concentration of the Gaseous Pollutants be captured can be obtained.For trapping the anemostat at least following condition of demand fulfillment of Gaseous Pollutants: 1, the material of anemostat needs affine absorbing liquid; 2, because Gaseous Pollutants concentration is low, anemostat wants high to the arresting efficiency of gaseous contaminant; 3, anemostat keeps stable to the arresting efficiency of gaseous contaminant in relatively long-time; 4, avoid interference the loss of composition granule thing in anemostat as far as possible; 5, because Gaseous Pollutants fluctuation of concentration scope is large, the capacity of the trapping gaseous pollutant of anemostat wants large.Foreign study person is designed with circular propagation pipe, annular denuder, parallel plate type anemostat etc. as the case may be, their application scenario is different, all there are respective relative merits, wherein because the inside surface of annular denuder is large, capacity large, are often applied to the trapping of Gaseous Pollutants.
Annular denuder conventional in the world at present has following defect: 1, unstable to the arresting efficiency of gaseous contaminant; 2, low to the trapping capacity of gaseous contaminant, under the environment of high pollution especially abroad, use in the world good annular denuder at home environmental applications time usually lost efficacy; 3, structure is partially complicated, and cause later maintenance loaded down with trivial details, cost is high.
Summary of the invention
The object of this invention is to provide a kind of rotary gas for trapping air vaporous water soluble pollutants and spread continuous capturing device.
For achieving the above object, the present invention takes following technical scheme: a kind of rotary gas spreads continuous capturing device, it is characterized in that: it comprises rotary anemostat, stepper motor, constant temperature air-supply arrangement, groove type support, the first micro pump, the second micro pump, absorbing liquid liquid storage bottle, quantitative collection device, the 3rd micro pump, the continuous delivery outlet of gaseous contamination matter sample, gas flow controller, sampling pump of bleeding, peripheral driver control circuit and host computer; Described rotary anemostat is arranged on described groove type internal stent, and described stepper motor is arranged on described groove type support one end, and the clutch end of described stepper motor connects the power intake of described rotary anemostat; Be positioned at described groove type carrier openings side, be provided with described constant temperature air-supply arrangement along its length in described rotary anemostat outside wall surface; The absorbing liquid inlet end of described rotary anemostat connects the endpiece of described first micro pump, and the inlet end of described first micro pump connects described absorbing liquid liquid storage bottle; The absorbing liquid endpiece of described rotary anemostat connects the inlet end of described quantitative collection device through described second micro pump, the endpiece of described quantitative collection device connects described 3rd micro pump inlet end, and described 3rd micro pump endpiece connects the continuous delivery outlet of described gaseous contamination matter sample; The gas outlet end of described rotary anemostat connects described gas flow controller, sampling pump of bleeding described in described gas flow controller connects; Described stepper motor, constant temperature air-supply arrangement, the first micro pump, the second micro pump, the 3rd micro pump, sample amounts gatherer, gas flow controller and sampling pump of bleeding all are connected with described peripheral driver control circuit, and described peripheral driver control circuit is connected with described host computer by USB line.
Described rotary anemostat comprises an air intake, two rotary seal adaptors, the annular quartz socket tube of bilayer, an annular plastics gear and a gas outlet; Described air intake is connected to the annular quartz socket tube one end of described bilayer by a described rotary seal adaptor, and the described double-deck quartz socket tube other end connects described gas outlet by rotary seal adaptor described in another; Described in another, rotary seal adaptor outside connects described annular plastics gear, and described annular plastics gear is by described stepper motor drive work.
Each described rotary seal adaptor encapsulates a stainless steel oilless bearing, and the two ends of described stainless steel oilless bearing are all provided with O shape circle.
The annular quartz socket tube of described bilayer comprises outer quartz ampoule, interior quartz ampoule, gas flow guiding cone, silicon rubber O shape circle, rear end cap and support bar; Described interior quartz ampoule outside surface and described outer inner surface of silica tube are all through frosted process; Be provided with described interior quartz ampoule in described outer quartz ampoule, and described constant temperature air-supply arrangement is arranged on described outer quartz ampoule outside wall surface, length is corresponding setting with described outer quartz ampoule length; Described interior quartz ampoule one end is bored with described gas flow guiding and is connected by described silicon rubber seal with O ring, the described interior quartz ampoule other end is connected by described silicon rubber seal with O ring with described rear end cap, described gas flow guiding cone inner face center position is connected with described support bar threaded one end, and the described support bar other end is threaded with described rear end cap inner face.
Described bilayer annular quartz socket tube one end and a described rotary seal adaptor are tightly connected by O type circle, then dock with described air intake, between described air intake docks with described rotary seal adaptor, be provided with that a silicon rubber O shape is enclosed successively, a quartzy thin slice of annular, a cyclic polytetrafluoroethylene thin slice and another silicon rubber O shape enclose; An absorbing liquid outlet is provided with in the bottom of described air intake.
The air intake of described rotary anemostat is connected with described groove type support by threaded connector, spring.
The annular quartz socket tube other end of described bilayer and rotary seal adaptor described in another are tightly connected by O type circle, and this rotary seal adaptor docks with described gas outlet; Described gas outlet is provided with between docking with described rotary seal adaptor that a silicon rubber O shape is enclosed successively, a quartzy thin slice of annular, a cyclic polytetrafluoroethylene thin slice and another silicon rubber O shape are enclosed; Bottom, described gas outlet is provided with an absorbing liquid import.
The gas outlet of described rotary anemostat is connected with described groove type support by described threading nut.
The clutch end of described stepper motor connects plastic gear, the annular plastics gears meshing of described plastic gear and described rotary anemostat.
The present invention is owing to taking above technical scheme, it has the following advantages: the double-deck quartz socket tube 1, in the rotary anemostat of the present invention has selected hydrophilic quartzy material, after meticulous frosted process has been carried out to inner tube outer surface and outward appearance inside surface, its water wettability is significantly improved further, not only improve the absorptive capacity of rotary anemostat, and ensure that rotary anemostat absorbs the efficient stable of additional water soluble pollution components for a long time.2, present invention utilizes constant temperature air-supply arrangement and constant temperature protection is carried out to the absorbing liquid in rotary anemostat; make the gas flow temperature of gas outlet constant; not only significantly improve rotary anemostat to additional water soluble pollution components absorption efficiency; and absorption efficiency is more stable, the fluctuation that the change effectively reducing environment temperature causes absorption efficiency.3, the rotation mode of stepper motor of the present invention and mechanical gear cooperation, changes the rotary rpm of rotary anemostat by control step motor speed, not only reliable and stable, and avoids other detectors of use to monitor rotary rpm.4, the present invention carries liquid by the micro pump of pulsed one-way only operation pattern, because peripheral driver control circuit controls the second micro pump frequency of operation higher than the first micro pump (namely micro pump conveying liquid velocity is fast), thus the absorbing liquid exit velocity of rotary anemostat is faster than absorbing liquid entrance, realize absorbing liquid liquid level in rotary anemostat and remain constant, avoid and use other detectors to carry out monitoring position of fluid level.5, inventive samples quantitative collection device carries out quantitatively the sample collected in a period of time, and cost is low.6, the display monitoring software of peripheral driver control circuit of the present invention and host computer makes device more humane, and function is more perfect, more powerful, has the functions such as real-time setting device parameter, follow-up work state and recording parameters data.The present invention is applicable to gas and spreads continuous trapping field.
Accompanying drawing explanation
Fig. 1 is one-piece construction schematic diagram of the present invention,---represent signal line;
Fig. 2 is rotary anemostat structural representation of the present invention.
Embodiment
Below in conjunction with drawings and Examples, the present invention is described in detail.
As shown in Figure 1, the present invention includes rotary anemostat 1, groove type support 2, stepper motor 3, constant temperature air-supply arrangement 4, first micro pump 5, absorbing liquid liquid storage bottle 6, second micro pump 7, quantitative collection device 8, the 3rd micro pump 9, the continuous delivery outlet 10 of gaseous contamination matter sample, gas flow controller 11, sampling pump 12 of bleeding, peripheral driver control circuit 13 and host computer 14.
It is inner that rotary anemostat 1 is arranged on groove type support 2, and stepper motor 3 is arranged on groove type support 2 one end, and the clutch end of this stepper motor 3 connects the power intake of rotary anemostat 1.Be positioned at groove type support 2 open side, be installed with constant temperature air-supply arrangement 4 along its length in rotary anemostat 1 outside wall surface, remain unchanged to make the fluid temperature flowing through rotary anemostat 1.The absorbing liquid inlet end of rotary anemostat 1 connects the endpiece of the first micro pump 5, and the inlet end of the first micro pump 5 connects absorbing liquid liquid storage bottle 6; The absorbing liquid endpiece of rotary anemostat 1 connects the inlet end of quantitative collection device 8 through the second micro pump 7, the endpiece of quantitative collection device 8 connects the 3rd micro pump 9 inlet end, and the 3rd micro pump 9 endpiece connects the continuous delivery outlet 10 of gaseous contamination matter sample.As shown in Figure 1, the left end of rotary anemostat 1 is the air intake end of atmospheric sample, right-hand member is the gas outlet end of atmospheric sample, gas outlet end connects gas flow controller 11, gas flow controller 11 connects sampling pump 12 of bleeding, by sampling pump 12 of bleeding by rotary for outside ambient air Sample introduction anemostat 1, then gas coming through flow controller 11 is extracted out.Stepper motor 3, constant temperature air-supply arrangement 4, first micro pump 5, second micro pump 7, the 3rd micro pump 9, sample amounts gatherer 8, gas flow controller 11 are all connected with peripheral driver control circuit 13 with sampling pump 12 of bleeding, peripheral driver control circuit 13 is connected with host computer 14 by USB line, is monitored the duty of each device by host computer 14 in real time.
As shown in Figure 2, rotary anemostat 1 comprises an air intake 1-1, two rotary seal adaptor 1-2, the annular quartz socket tube 1-3 of bilayer, an annular plastics gear 1-4 and gas outlet 1-5.Air intake 1-1 is connected to double-deck annular quartz socket tube 1-3 one end by a rotary seal adaptor 1-2, and the double-deck annular quartz socket tube 1-3 other end connects gas outlet 1-5 by another rotary seal adaptor 1-2; And connecting annular plastics gear 1-4 in another rotary seal adaptor 1-2 outside, annular plastics gear 1-4 drives work by stepper motor 3, and then drives another rotary seal adaptor 1-2 to rotate.Wherein:
Each rotary seal adaptor 1-2 encapsulates a stainless steel oilless bearing 1-2-1, the two ends of stainless steel oilless bearing 1-2-1 are all provided with O shape circle, for the protection of rotary seal adaptor 1-2.When rotary anemostat 1 of the present invention works, double-deck annular quartz socket tube 1-3, rotary seal adaptor 1-2 and annular plastics gear 1-4 rotate, and air intake 1-1 and gas outlet 1-5 is motionless, this running realizes by stainless steel oilless bearing 1-2-1, the rotor of bearing is connected with rotary seal adaptor 1-2, and the stator of bearing is fixed on air intake 1-1 and gas outlet 1-5.During work, first, stepper motor 3 works, annular plastics gear 1-4 is driven to rotate, and then rotary seal adaptor 1-2 is rotated, owing to being that to enclose 1-1-3 by O shape close-fitting between rotary seal adaptor 1-2 and bilayer annular quartz socket tube 1-3, so double-deck annular quartz socket tube 1-3 also rotates.
In above-described embodiment, double-deck annular quartz socket tube 1-3 comprises outer quartz ampoule 1-3-1, interior quartz ampoule 1-3-2, gas flow guiding cone 1-3-3, silicon rubber O shape circle 1-3-4, rear end cap 1-3-5 and support bar 1-3-6.In order to strengthen water wettability, the outside surface of interior quartz ampoule 1-3-2 and the inside surface of outer quartz ampoule 1-3-1 all will through frosted process, the diameter 3mm less of the diameter of outer quartz ampoule 1-3-1 of interior quartz ampoule 1-3-2, they are integrally welded coaxially to each other, its section is for being a loop configuration, and constant temperature air-supply arrangement 4 is arranged on outer quartz ampoule 1-3-1 outside wall surface, length is corresponding setting with outer quartz ampoule 1-3-1 length.Interior quartz ampoule 1-3-2 one end and gas flow guiding are bored 1-3-3 and are enclosed 1-3-4 by silicon rubber O shape and be tightly connected, the interior quartz ampoule 1-3-2 other end and rear end cap 1-3-5 enclose 1-3-4 by silicon rubber O shape and are tightly connected, gas flow guiding cone 1-3-3 inner face center position is connected with support bar 1-3-6 threaded one end, the support bar 1-3-6 other end is threaded with rear end cap 1-3-5 inner face, thus forms double-deck annular quartz socket tube 1-3.
As shown in Figure 2, left end and a rotary seal adaptor 1-2 of double-deck annular quartz socket tube 1-3 are tightly connected by O type circle, then dock with air intake 1-1, between air intake 1-1 docks with rotary seal adaptor 1-2, be provided with a silicon rubber O shape successively enclose 1-1-3, the quartzy thin slice 1-1-1 of annular, a cyclic polytetrafluoroethylene thin slice 1-1-2 and another silicon rubber O shape and enclose 1-1-3, wherein two silicon rubber O shapes circle 1-1-3 seal.An absorbing liquid outlet 1-1-4 is provided with, for connecting the second micro pump 7 in the bottom of air intake 1-1.
Right-hand member and another rotary seal adaptor 1-2 of double-deck annular quartz socket tube 1-3 are tightly connected by O type circle, and this rotary seal adaptor 1-2 is outside by tight sheathed annular plastics gear 1-4, then docks with gas outlet 1-5.Between gas outlet 1-5 docks with rotary seal adaptor 1-2, be provided with a silicon rubber O shape successively enclose 1-5-3, the quartzy thin slice 1-5-1 of annular, a cyclic polytetrafluoroethylene thin slice 1-5-2 and another silicon rubber O shape and enclose 1-5-3, wherein two silicon rubber O shapes circle 1-5-3 seal.Connecting threading nut 1-5-4 in gas outlet 1-5 end thread, being provided with an absorbing liquid import 1-5-5 in 1-5 bottom, gas outlet, for connecting the first micro pump 5.Gas outlet 1-5 right-hand member connects gas flow controller 11 and sampling pump 12 of bleeding.
In the various embodiments described above, the gas outlet 1-5 of rotary anemostat 1 is connected with groove type support 2 by threading nut 1-5-4, and the air intake 1-1 of rotary anemostat 1 is connected with groove type support 2 by threaded connector, spring.
In the various embodiments described above, the clutch end of stepper motor 3 connects plastic gear, and plastic gear engages with the annular plastics gear 1-4 of rotary anemostat 1, realizes power transmission.
In sum, in use, its principle of work is as follows in the present invention:
Ambient air sampling under the effect of sampling pump 12 of bleeding along with air-flow enters rotary anemostat 1, rotary anemostat 1 at the uniform velocity rotates under the drive of stepper motor 3, and rotating speed is undertaken setting (such as 20 rpms) by the monitoring software on host computer 14.Under the effect of the first micro pump 5, absorbing liquid (as water) enters from absorbing liquid import 1-5-5 the gas outlet 1-5 of rotary anemostat 1 continuously with slower speed, the inner pipe wall surface of double-deck quartz socket tube 1-3 is flooded profit gradually, and water is adsorbed in tube wall.Ambient air sampling enters double-deck quartz socket tube 1-3 through gas flow guiding cone 1-3-3 laminar flow, because the rate of diffusion of gaseous material in air is much larger than the rate of diffusion of particle, vaporous water soluble pollutants quickly diffuses to the inner pipe wall of double-deck quartz socket tube 1-3, the water being attached to tube wall absorbs, and particle under inertia effect along with air-flow is through double-deck quartz socket tube 1-3, sampling pump 12 of being bled after gas flow controller 11 is extracted out.Constant temperature air-supply arrangement 4 can send the air-flow of steady temperature, for carrying out constant temperature protection to the absorbing liquid flowing through double-deck quartz socket tube 1-3.Under the effect of the second micro pump 7, the aqueous solution absorbing vaporous water soluble pollutants flows out from absorbing liquid outlet 1-1-4 the air intake 1-1 of rotary anemostat 1, is collected and enters sample amounts gatherer 8.Sample amounts gatherer 8 can the volume of aqueous sample that arrives of measurement collection in real time.When aqueous sample is accumulated to certain period or certain volume, aqueous solution exports for subsequent detection or analysis by host computer 14 display monitoring software control the 3rd micro pump 9 continuously.
Host computer 14 is connected with peripheral driver control circuit 13 by USB line, the rotating speed of stepper motor 3 is set by the monitoring software of host computer 14, the frequency of operation of constant temperature air-supply arrangement 4, first micro pump 5, second micro pump 7, the frequency of operation of the 3rd micro pump 9, the collection duration of absorbing liquid, the parameters such as the start-up study of the 3rd micro pump 9 and the coutroi velocity of gas flow controller 11, and send the operation of instruction opertaing device, record the sample solution amount detected by sample amounts gatherer 8 simultaneously, gas outlet gas flow temperature on the air-flow velocity that gas flow controller 11 is measured in real time and constant temperature air-supply arrangement 4.
The various embodiments described above are only for illustration of the present invention; wherein the structure of each parts, connected mode and manufacture craft etc. all can change to some extent; every equivalents of carrying out on the basis of technical solution of the present invention and improvement, all should not get rid of outside protection scope of the present invention.

Claims (10)

1. rotary gas spreads a continuous capturing device, it is characterized in that: it comprises rotary anemostat, stepper motor, constant temperature air-supply arrangement, groove type support, the first micro pump, the second micro pump, absorbing liquid liquid storage bottle, quantitative collection device, the 3rd micro pump, the continuous delivery outlet of gaseous contamination matter sample, gas flow controller, sampling pump of bleeding, peripheral driver control circuit and host computer;
Described rotary anemostat is arranged on described groove type internal stent, and described stepper motor is arranged on described groove type support one end, and the clutch end of described stepper motor connects the power intake of described rotary anemostat; Be positioned at described groove type carrier openings side, be provided with described constant temperature air-supply arrangement along its length in described rotary anemostat outside wall surface; The absorbing liquid inlet end of described rotary anemostat connects the endpiece of described first micro pump, and the inlet end of described first micro pump connects described absorbing liquid liquid storage bottle; The absorbing liquid endpiece of described rotary anemostat connects the inlet end of described quantitative collection device through described second micro pump, the endpiece of described quantitative collection device connects described 3rd micro pump inlet end, and described 3rd micro pump endpiece connects the continuous delivery outlet of described gaseous contamination matter sample; The gas outlet end of described rotary anemostat connects described gas flow controller, sampling pump of bleeding described in described gas flow controller connects; Described stepper motor, constant temperature air-supply arrangement, the first micro pump, the second micro pump, the 3rd micro pump, sample amounts gatherer, gas flow controller and sampling pump of bleeding all are connected with described peripheral driver control circuit, and described peripheral driver control circuit is connected with described host computer by USB line.
2. a kind of rotary gas as claimed in claim 1 spreads continuous capturing device, it is characterized in that: described rotary anemostat comprises an air intake, two rotary seal adaptors, the annular quartz socket tube of bilayer, an annular plastics gear and a gas outlet; Described air intake is connected to the annular quartz socket tube one end of described bilayer by a described rotary seal adaptor, and the described double-deck quartz socket tube other end connects described gas outlet by rotary seal adaptor described in another; Described in another, rotary seal adaptor outside connects described annular plastics gear, and described annular plastics gear is by described stepper motor drive work.
3. a kind of rotary gas as claimed in claim 2 spreads continuous capturing device, it is characterized in that: each described rotary seal adaptor encapsulates a stainless steel oilless bearing, and the two ends of described stainless steel oilless bearing are all provided with O shape circle.
4. a kind of rotary gas as claimed in claim 2 spreads continuous capturing device, it is characterized in that: the annular quartz socket tube of described bilayer comprises outer quartz ampoule, interior quartz ampoule, gas flow guiding cone, silicon rubber O shape circle, rear end cap and support bar; Described interior quartz ampoule outside surface and described outer inner surface of silica tube are all through frosted process; Be provided with described interior quartz ampoule in described outer quartz ampoule, and described constant temperature air-supply arrangement is arranged on described outer quartz ampoule outside wall surface, length is corresponding setting with described outer quartz ampoule length; Described interior quartz ampoule one end is bored with described gas flow guiding and is connected by described silicon rubber seal with O ring, the described interior quartz ampoule other end is connected by described silicon rubber seal with O ring with described rear end cap, described gas flow guiding cone inner face center position is connected with described support bar threaded one end, and the described support bar other end is threaded with described rear end cap inner face.
5. a kind of rotary gas as claimed in claim 3 spreads continuous capturing device, it is characterized in that: the annular quartz socket tube of described bilayer comprises outer quartz ampoule, interior quartz ampoule, gas flow guiding cone, silicon rubber O shape close, the rear end cap of circle and support bar; Described interior quartz ampoule outside surface and described outer inner surface of silica tube are all through frosted process; Be provided with described interior quartz ampoule in described outer quartz ampoule, and described constant temperature air-supply arrangement is arranged on described outer quartz ampoule outside wall surface, length is corresponding setting with described outer quartz ampoule length; Described interior quartz ampoule one end is bored with described gas flow guiding and is connected by described silicon rubber seal with O ring, the described interior quartz ampoule other end is connected by described silicon rubber seal with O ring with described rear end cap, described gas flow guiding cone inner face center position is connected with described support bar threaded one end, and the described support bar other end is threaded with described rear end cap inner face.
6. a kind of rotary gas as described in Claims 2 or 3 or 4 or 5 spreads continuous capturing device, it is characterized in that: described bilayer annular quartz socket tube one end and a described rotary seal adaptor are tightly connected by O type circle, then dock with described air intake, between described air intake docks with described rotary seal adaptor, be provided with that a silicon rubber O shape is enclosed successively, a quartzy thin slice of annular, a cyclic polytetrafluoroethylene thin slice and another silicon rubber O shape enclose; An absorbing liquid outlet is provided with in the bottom of described air intake.
7. a kind of rotary gas as claimed in claim 6 spreads continuous capturing device, it is characterized in that: the air intake of described rotary anemostat is connected with described groove type support by threaded connector, spring.
8. a kind of rotary gas as described in Claims 2 or 3 or 4 or 5 spreads continuous capturing device, it is characterized in that: the annular quartz socket tube other end of described bilayer and rotary seal adaptor described in another are tightly connected by O type circle, and this rotary seal adaptor docks with described gas outlet; Described gas outlet is provided with between docking with described rotary seal adaptor that a silicon rubber O shape is enclosed successively, a quartzy thin slice of annular, a cyclic polytetrafluoroethylene thin slice and another silicon rubber O shape are enclosed; Bottom, described gas outlet is provided with an absorbing liquid import.
9. a kind of rotary gas as claimed in claim 8 spreads continuous capturing device, it is characterized in that: the gas outlet of described rotary anemostat is connected with described groove type support by described threading nut.
10. a kind of rotary gas as described in claim 1 or 2 or 3 or 4 or 5 or 9 spreads continuous capturing device, it is characterized in that: the clutch end of described stepper motor connects plastic gear, the annular plastics gears meshing of described plastic gear and described rotary anemostat.
CN201510038288.6A 2015-01-26 2015-01-26 Rotary gas diffusion and continuous capture device Pending CN104596808A (en)

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