CN104592902A - Preparation method of adhesive for architectural engineering - Google Patents
Preparation method of adhesive for architectural engineering Download PDFInfo
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- CN104592902A CN104592902A CN201510022356.XA CN201510022356A CN104592902A CN 104592902 A CN104592902 A CN 104592902A CN 201510022356 A CN201510022356 A CN 201510022356A CN 104592902 A CN104592902 A CN 104592902A
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- Prior art keywords
- ethylene glycol
- adhesive
- construction work
- tetrahydroquinoline
- benzoquinone
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Abstract
The invention discloses a preparation method of an adhesive for architectural engineering. The preparation method is characterized in that the adhesive comprises triuret ethylene glycol bis-methyl acrylate, cumyl hydroperoxide, 1,2,3,4-tetrahydroquinoline, p-benzoquinone, p-toluene sulfonic acid, saccharin, polystyrene, polyacetal ethylene glycol dioctyl phthalate and colloidal silicon dioxide in a mass ratio of 110:3.4:0.5:(0.06-0.08):0.2:0.3:15:14:11. In a metal adhesion process, the curing within 30 minutes is complete; moreover, the adhesive has functions of preventing vibration, leakage, corrosion and the like, and has very strong practicability.
Description
Technical field
The present invention relates to a kind of collocation method of the sizing agent for construction work, particularly relate to a kind of collocation method of anaerobic type engineering sizing agent.
Background technology
Bonding technology is the newer technique of in mechanical industry, and its application is to improving the quality of products, and simplify assembly technology, locking, there is very large effect the aspect such as leak-stopping and save energy.Just day by day be subject to people's attention in China.Anaerobic glue is the tackiness agent widely applied the external sixties, has now become one of the most frequently used tackiness agent in machinery, building.Its annual production progressive increase rate, always about 25%, is much higher than other tackiness agent.Anaerobic type tackiness agent is a most important type in acrylic resin adhesive, and since the 1950's, anaerobic glue experienced by the development research of three generation products, and existing tens kinds, are widely used in the industries such as machinofacture, maintenance, building now.The characteristic of Anaerobic adhesive is anaerobic cure, is in a liquid state when namely glue contacts with air, and when seams such as injection metals, during with air exclusion, solidification of just getting together voluntarily under normal temperature, is formed and firmly bond.The performance of its excellence is: single component, does not need proportioning to mix, ambient cure, easy and simple to handle, good penetrability, shrinks few, have good vibration resistance and stopping property during solidification; Glue-line has excellent media-resistant, oil resistant, the ability such as water-fast, acidproof, alkaline-resisting, and has rust inhibition to metal, containing solvent, substantially nontoxic; Cohesive strength, between structure glue and non-structural glue, allows assembly dismounting to use again.Anaerobic glue full name is anaerobic adhesive, belong to thermosetting polymer organic compound, be monosomy liquid in atmosphere, containing single polymers and radical, this group is owing to having larger reaction to oxygen, so anaerobic glue can keep liquid in atmosphere for a long time, but when glue being placed between two metals, owing to having completely cut off air, and in the presence of metal ion, free son just can cause rapidly the polyreaction of monomer, become superpolymer, thus be cured as tough and tensile glue-line, and invest metallic surface securely, equipment is made to reach reliable sealing, effective locking and firmly bonding.Traditional Anaerobic adhesive sticks agent, and to there is solidification effect when mechanical surface solidifies insufficient, do not reach practical cohesive strength, especially the metal in construction work in power distribution room arranges assembling, the installation etc. of the hardware such as camera, radar on motorway, always there will be " three leak " phenomenon.
Summary of the invention
The object of the invention is the problem solving the adhesion agent weather resisteant used in hardware assembling process in construction work.
The technical solution used in the present invention is: for the collocation method of the sizing agent of construction work, comprise triethylene Glycol double methyl methacrylate, hydrogen phosphide cumene, 1,2,3,4-tetrahydroquinoline, benzoquinone, p-methyl benzenesulfonic acid, asccharin, polystyrene, multicondensed ethylene glycol dioctyl ester and colloid silica, each component in the ratio of quality is: 110:3.4:0.5:0.06 ~ 0.08:0.2:0.3:15:14:11;
Making step:
(1) by triethylene Glycol double methyl methacrylate and benzoquinone at 40-50 DEG C, stir 2h with 300-600r/min speed, reactant dissolved completely;
(2) interpolation asccharin, 1,2,3,4-tetrahydroquinoline and p-methyl benzenesulfonic acid is stirred to and dissolves completely;
(3) add colloid silica, multicondensed ethylene glycol dioctyl ester, polystyrene, after dissolving to be mixed completely, be cooled to normal temperature;
(4) add hydrogen phosphide cumene and stir 50min, make it be uniformly dispersed;
The glue splendid attire be made in step (4) is in opaque polythene container, and load the half of vessel volume, sealed type storage is stand-by.
As a further improvement on the present invention, each component in mass ratio example be: 120:5.8:0.7:0.09:0.4:0.3:16:13:10.
As a further improvement on the present invention, each component in mass ratio example be: 100:6.2:0.6:0.06:0.2:0.3:15:12:10.
The invention has the beneficial effects as follows: the present invention is in metal sticking process, and 30min completion of cure, and have the functions such as vibrationproof, leakproof, protection against corrosion, has very strong practicality.
Embodiment
Embodiment 1:
(1) by 110kg triethylene Glycol double methyl methacrylate and 0.06kg benzoquinone at 40-50 DEG C, stir 2h with 300-600r/min speed, reactant dissolved completely;
(2) interpolation 0.3kg asccharin, 1,2,3,4-tetrahydroquinoline 0.5kg and 0.2kg p-methyl benzenesulfonic acid are stirred to and dissolve completely;
(3) add 11kg colloid silica, 14kg multicondensed ethylene glycol dioctyl ester, 15kg polystyrene, after dissolving to be mixed completely, be cooled to normal temperature;
(4) add 3.4kg hydrogen phosphide cumene and stir 1h, make it be uniformly dispersed;
The glue splendid attire be made in step (4) is in opaque polythene container, and load the half of vessel volume, sealed type storage is stand-by.
Embodiment 2:
(1) by 120kg triethylene Glycol double methyl methacrylate and 0.09kg benzoquinone at 40-50 DEG C, stir 2h with 300-600r/min speed, reactant dissolved completely;
(2) interpolation 0.3kg asccharin, 1,2,3,4-tetrahydroquinoline 0.7kg and 0.4kg p-methyl benzenesulfonic acid are stirred to and dissolve completely;
(3) add 10kg colloid silica, 13kg multicondensed ethylene glycol dioctyl ester, 16kg polystyrene, after dissolving to be mixed completely, be cooled to normal temperature;
(4) add 5.8kg hydrogen phosphide cumene and stir 1h, make it be uniformly dispersed;
The glue splendid attire be made in step (4) is in opaque polythene container, and load the half of vessel volume, sealed type storage is stand-by.
Embodiment 3:
(1) by 100kg triethylene Glycol double methyl methacrylate and 0.06kg benzoquinone at 40-50 DEG C, stir 2h with 300-600r/min speed, reactant dissolved completely;
(2) interpolation 0.5kg asccharin, 1,2,3,4-tetrahydroquinoline 0.6kg and 0.2kg p-methyl benzenesulfonic acid are stirred to and dissolve completely;
(3) add 10kg colloid silica, 12kg multicondensed ethylene glycol dioctyl ester, 15kg polystyrene, after dissolving to be mixed completely, be cooled to normal temperature;
(4) add 6.2kg hydrogen phosphide cumene and stir 1h, make it be uniformly dispersed;
The glue splendid attire be made in step (4) is in opaque polythene container, and load the half of vessel volume, sealed type storage is stand-by.
Above embodiments of the present invention are described, but the invention is not restricted to above-mentioned embodiment, in the ken that art those of ordinary skill possesses, can also make a variety of changes under the prerequisite not departing from present inventive concept.
Claims (3)
1. for the collocation method of the sizing agent of construction work, it is characterized in that: comprise triethylene Glycol double methyl methacrylate, hydrogen phosphide cumene, 1,2,3,4-tetrahydroquinoline, benzoquinone, p-methyl benzenesulfonic acid, asccharin, polystyrene, multicondensed ethylene glycol dioctyl ester and colloid silica, each component in the ratio of quality is: 110:3.4:0.5:0.06 ~ 0.08:0.2:0.3:15:14:11;
Making step:
By triethylene Glycol double methyl methacrylate and benzoquinone at 40-50 DEG C, stir 2h with 300-600r/min speed, reactant is dissolved completely;
Interpolation asccharin, 1,2,3,4-tetrahydroquinoline and p-methyl benzenesulfonic acid are stirred to and dissolve completely;
Add colloid silica, multicondensed ethylene glycol dioctyl ester, polystyrene, after dissolving to be mixed completely, be cooled to normal temperature;
Add hydrogen phosphide cumene and stir 50min, make it be uniformly dispersed;
The glue splendid attire be made in step (4) is in opaque polythene container, and load the half of vessel volume, sealed type storage is stand-by.
2. the collocation method of the sizing agent for construction work according to claim 1, it is characterized in that described each component in mass ratio example be: 120:5.8:0.7:0.09:0.4:0.3:16:13:10.
3. the collocation method of the sizing agent for construction work according to claim 1, it is characterized in that described each component in mass ratio example be: 100:6.2:0.6:0.06:0.2:0.3:15:12:10.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510022356.XA CN104592902A (en) | 2015-01-16 | 2015-01-16 | Preparation method of adhesive for architectural engineering |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510022356.XA CN104592902A (en) | 2015-01-16 | 2015-01-16 | Preparation method of adhesive for architectural engineering |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104592902A true CN104592902A (en) | 2015-05-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510022356.XA Pending CN104592902A (en) | 2015-01-16 | 2015-01-16 | Preparation method of adhesive for architectural engineering |
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| CN (1) | CN104592902A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104946169A (en) * | 2015-05-08 | 2015-09-30 | 南通长航船舶配件有限公司 | Automatic safe control device for ship |
| CN107558658A (en) * | 2017-10-20 | 2018-01-09 | 浙江宏博新型建材有限公司 | A kind of architectural shape with crashworthiness |
-
2015
- 2015-01-16 CN CN201510022356.XA patent/CN104592902A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104946169A (en) * | 2015-05-08 | 2015-09-30 | 南通长航船舶配件有限公司 | Automatic safe control device for ship |
| CN107558658A (en) * | 2017-10-20 | 2018-01-09 | 浙江宏博新型建材有限公司 | A kind of architectural shape with crashworthiness |
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| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150506 |