CN104531280A - Lubricating-type grease-type anti-rusting oil with good comprehensive performance, and preparation method thereof - Google Patents

Abstract

The invention discloses lubricating-type grease-type anti-rusting oil with good comprehensive performance. The anti-rusting oil is prepared from the following raw materials, by weight: 28-33 parts of solid paraffin, 30-35 parts of Vaseline, 4-6 parts of petroleum oxide grease, 2-3 parts of sodium petroleum sulfonate, 3.5-4.5 parts of alkenyl succinate, 10-14 parts of 46# machine oil, 11-13 parts of mineral oil, 2-3 parts of sucrose fatty acid ester, 0.7-0.9 parts of benzophenone, 2-3 parts of red iron oxide, and 2.5-4 parts of a protective agent. The anti-rusting oil has a reasonable formula. Lubricating oil is adopted as a base oil, and the materials such as red iron oxide are added, such that the anti-rusting oil is ultraviolet-resistant. With the protective agent, the anti-rusting oil is antibacterial and anti-corrosive. Also, a firm protective film can be formed on a metal surface, such that rusting caused by water and oxygen erosion can be prevented. The anti-rusting oil provided by the invention has high oil film strength, and is not prone to cracking in an outdoor environment. The anti-rusting oil has long service life and excellent comprehensive performance. With the anti-rusting oil, cost is reduced.

Description

Lubricating type grease type rust preventing oil of a kind of good combination property and preparation method thereof

Technical field

The present invention relates to rust protection liquid field, particularly a kind of lubricating type grease type rust preventing oil and preparation method thereof of good combination property.

Background technology

The metal that the whole world is scrapped due to corrosion every year accounts for the 20%-40% of world's metal annual production, and wherein the corrosion of iron and steel accounts for the half of corrosion of metal, and the wasting of resources is very serious.For metal is antirust timely, getting rusty of metal effectively can be avoided to scrap, thus save ample resources, the development for society provides larger guarantee.Metal antirusting agent kind is in the market more, but kind is comparatively single, and the demand for development rust preventing grease of modern industrial technology will improve antirust ability, extends the antirust cycle, has again good lubricant effect simultaneously.

The present invention is directed to society demand, invent a kind of oilness grease type rust preventing oil, have excellent uviolresistance, weathering resistance, oil film strength is large, and not easy to crack, duration of service is long.

Summary of the invention

Lubricating type grease type rust preventing oil that the object of this invention is to provide a kind of good combination property and preparation method thereof.

In order to realize object of the present invention, the present invention is by following scheme implementation:

A lubricating type grease type rust preventing oil for good combination property, is made up of the raw material of following weight part: solid paraffin 28-33, Vaseline 30-35, oxidized petrolatum 4-6, petroleum sodium sulfonate 2-3, alkenyl succinic acid ester 3.5-4.5,46# machinery oil 10-14, mineral oil 11-13, sucrose fatty ester 2-3, benzophenone 0.7-0.9, red iron oxide 2-3, protective material 2.5-4;

Described protective material is prepared from by the raw material of following weight part: bakelite 10-12, urethane 13-15, ethylene glycol diglycidylether 2-3, butyleneglycol 4.5-6, tween 80 1-2, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, red iron oxide 3-4, nano titanium oxide 2-4, Viscotrol C 5-7, Zinic stearas 2-3, silicon dioxide gel 3-5, sec.-propyl three isophthaloyl titanic acid ester 0.3-0.5; First preparation method adds Viscotrol C, silicon dioxide gel, agitation grinding 50-60 minute by after red iron oxide, nano titanium oxide mixing, forms dispersion; Then by bakelite, urethane, the mixing of sec.-propyl three isophthaloyl titanic acid ester, be heated to 90 DEG C-115 DEG C stirring reaction 2-3 hour, be cooled to 45 DEG C-60 DEG C again, add all the other remaining components except tween 80, myristyl benzyl dimethyl ammonium chloride, stir 30-40 minute with the speed of 400-500 rev/min; Finally be cooled to room temperature, add dispersion and tween 80, myristyl benzyl dimethyl ammonium chloride, stir and obtain protective material.

The lubricating type grease type rust preventing oil of a kind of good combination property of the present invention, be made up of following concrete steps:

(1) will add red iron oxide, solid paraffin in mineral oil, gradation adds Vaseline, fully grinding 2-2.5 hour;

(2) by oxidized petrolatum, petroleum sodium sulfonate, the mixing of alkenyl succinic acid ester, then temperature control is at 80 DEG C-95 DEG C, and insulation 50-70 minute, is then cooled to 55 DEG C-60 DEG C, adds benzophenone, insulation reaction 30-40 minute;

(3) step (1) is mixed with step (2), add protective material, stir 40-60 minute with the speed of 300-350 rev/min; then all the other remaining components are added; be heated to 50 DEG C-60 DEG C, continue to stir 0.5-1 hour, then namely cold going obtain rust preventing grease of the present invention to room temperature.

Excellent effect of the present invention is: the present invention fills a prescription rationally, adopts oil based on lubricating oil, adds the uvioresistants such as red iron oxide, add protective material, Antimicrobial preservative, and firmly protective membrane can be formed in metallic surface, the erosion of anti-sealing and oxygen causes getting rusty; Oil film strength of the present invention is large, and outdoor environment is not easy to crack, and duration of service is long, reduces cost, excellent combination property.

Embodiment

Below by specific examples, the present invention is described in detail.

A lubricating type grease type rust preventing oil for good combination property, is made up of the raw material of following weight part (kilogram): solid paraffin 28, Vaseline 30, oxidized petrolatum 4, petroleum sodium sulfonate 2, alkenyl succinic acid ester 3.5,46# machinery oil 10, mineral oil 11, sucrose fatty ester 2, benzophenone 0.7, red iron oxide 2, protective material 2.5;

Described protective material is prepared from by the raw material of following weight part (kilogram): bakelite 10, urethane 13, ethylene glycol diglycidylether 2, butyleneglycol 4.5, tween 80 1, myristyl benzyl dimethyl ammonium chloride 0.1, red iron oxide 3, nano titanium oxide 2, Viscotrol C 5, Zinic stearas 2, silicon dioxide gel 3, sec.-propyl three isophthaloyl titanic acid ester 0.3; First preparation method adds Viscotrol C, silicon dioxide gel, agitation grinding 50-60 minute by after red iron oxide, nano titanium oxide mixing, forms dispersion; Then by bakelite, urethane, the mixing of sec.-propyl three isophthaloyl titanic acid ester, be heated to 90 DEG C-115 DEG C stirring reaction 2-3 hour, be cooled to 45 DEG C-60 DEG C again, add all the other remaining components except tween 80, myristyl benzyl dimethyl ammonium chloride, stir 30-40 minute with the speed of 400-500 rev/min; Finally be cooled to room temperature, add dispersion and tween 80, myristyl benzyl dimethyl ammonium chloride, stir and obtain protective material.

The lubricating type grease type rust preventing oil of a kind of good combination property of the present invention, be made up of following concrete steps:

(1) will add red iron oxide, solid paraffin in mineral oil, gradation adds Vaseline, fully grinding 2-2.5 hour;

(2) by oxidized petrolatum, petroleum sodium sulfonate, the mixing of alkenyl succinic acid ester, then temperature control is at 80 DEG C-95 DEG C, and insulation 50-70 minute, is then cooled to 55 DEG C-60 DEG C, adds benzophenone, insulation reaction 30-40 minute;

(3) step (1) is mixed with step (2), add protective material, stir 40-60 minute with the speed of 300-350 rev/min; then all the other remaining components are added; be heated to 50 DEG C-60 DEG C, continue to stir 0.5-1 hour, then namely cold going obtain rust preventing grease of the present invention to room temperature.

The rust preventing grease outward appearance that the present invention makes is the ointment of smooth even, can room temperature coating or heating coating, and salt spray resistance is tested: be 35 DEG C in temperature, and through 150 hours, 45# steel was corrosion-free; Wet-heat resisting is tested: be 50 DEG C in temperature, and through 700 hours, 45# steel was corrosion-free.

Claims (2)

1. the lubricating type grease type rust preventing oil of a good combination property, it is characterized in that, be made up of the raw material of following weight part: solid paraffin 28-33, Vaseline 30-35, oxidized petrolatum 4-6, petroleum sodium sulfonate 2-3, alkenyl succinic acid ester 3.5-4.5,46# machinery oil 10-14, mineral oil 11-13, sucrose fatty ester 2-3, benzophenone 0.7-0.9, red iron oxide 2-3, protective material 2.5-4;

Described protective material is prepared from by the raw material of following weight part: bakelite 10-12, urethane 13-15, ethylene glycol diglycidylether 2-3, butyleneglycol 4.5-6, tween 80 1-2, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, red iron oxide 3-4, nano titanium oxide 2-4, Viscotrol C 5-7, Zinic stearas 2-3, silicon dioxide gel 3-5, sec.-propyl three isophthaloyl titanic acid ester 0.3-0.5; First preparation method adds Viscotrol C, silicon dioxide gel, agitation grinding 50-60 minute by after red iron oxide, nano titanium oxide mixing, forms dispersion; Then by bakelite, urethane, the mixing of sec.-propyl three isophthaloyl titanic acid ester, be heated to 90 DEG C-115 DEG C stirring reaction 2-3 hour, be cooled to 45 DEG C-60 DEG C again, add all the other remaining components except tween 80, myristyl benzyl dimethyl ammonium chloride, stir 30-40 minute with the speed of 400-500 rev/min; Finally be cooled to room temperature, add dispersion and tween 80, myristyl benzyl dimethyl ammonium chloride, stir and obtain protective material.

2. the lubricating type grease type rust preventing oil of a kind of good combination property according to claim 1, is characterized in that, be made up of following concrete steps:

(1) will add red iron oxide, solid paraffin in mineral oil, gradation adds Vaseline, fully grinding 2-2.5 hour;

(2) by oxidized petrolatum, petroleum sodium sulfonate, the mixing of alkenyl succinic acid ester, then temperature control is at 80 DEG C-95 DEG C, and insulation 50-70 minute, is then cooled to 55 DEG C-60 DEG C, adds benzophenone, insulation reaction 30-40 minute;

(3) step (1) is mixed with step (2), add protective material, stir 40-60 minute with the speed of 300-350 rev/min; then all the other remaining components are added; be heated to 50 DEG C-60 DEG C, continue to stir 0.5-1 hour, then namely cold going obtain rust preventing grease of the present invention to room temperature.