CN104523752A - Process for producing cornu bubali concentration powder - Google Patents
Process for producing cornu bubali concentration powder Download PDFInfo
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- CN104523752A CN104523752A CN201410719148.0A CN201410719148A CN104523752A CN 104523752 A CN104523752 A CN 104523752A CN 201410719148 A CN201410719148 A CN 201410719148A CN 104523752 A CN104523752 A CN 104523752A
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- cornu bubali
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Abstract
The invention discloses a process for producing cornu bubali concentration powder, and belongs to the technical field of phytoextraction. According to the process, effective constituents of the cornu bubali powder are extracted and purified through the steps including raw material preprocessing, ultrasonic-assisted acid hydrolysis, edulcoration and refining; and drying is finally carried out to obtain the cornu bubali concentration powder. The ultrasonic-assisted acid hydrolysis method is adopted in the process, the extraction efficiency and the raw material using rate of the effective constituents are effectively improved; the product quality is stable; the yield is high; the process route is simple and practical; and the practicability is high.
Description
Technical field
The present invention relates to the field of Chinese medicines, be specifically related to a kind of production technology of Pulvis Cornus Bubali Concentratus.
Background technology
Pulvis Cornus Bubali Concentratus is that concentrated forming is extracted through processing in the angle of bovid water, and nature and flavor are bitter, cold, GUIXIN, Liver Channel.Be applicable to prurigo, epilepsy, the symptoms such as hyperpyrexia convulsion, mainly contain heart tonifying, antiinflammatory, infection, calm, relieving convulsion, shorten the bleeding time, reduce capillary permeability, the effects such as excited Pituitary Adrenalcortical system.Cornu Bubali is mainly containing compositions such as protein, peptide class, aminoacid, cholesterol, and prior art is prepared Pulvis Cornus Bubali Concentratus and adopted decocting method, and extracts active ingredients efficiency is low, raw material availability is low, cause the waste of raw material, and obtained unstable product quality, between batch, difference is large.
Summary of the invention
The object of this invention is to provide the production technology of a kind of steady quality, Pulvis Cornus Bubali Concentratus that productive rate is high.
The present invention is achieved by the following technical solutions:
A production technology for Pulvis Cornus Bubali Concentratus, comprises the following steps:
(1) pretreatment of raw material: water intaking Cornu Bovis seu Bubali, cleans, sawed-off, except chamfering plug, remaining part is ground to form 50-100 object powder;
(2) ultrasonic assistant acid hydrolysis: the acetum adding 6-8% by solid-liquid ratio 1:10-1:8, first 40-50 DEG C of Water Under solution 20-30h, supersound process 10-15min under 60-70 DEG C of condition again, add acetum 40-50 DEG C of hydrolysis 15-20h of same concentration, same volume again, supersound process 5-10min under 60-70 DEG C of condition again, filter and collect filtrate, obtaining extracting solution;
(3) remove impurity: the pH of extracting solution is adjusted to 6-7 with NaOH, filters after leaving standstill 2-4h;
(4) refining: the ethanol adding 4-6 times of volume 95% in the filtrate obtained in (3), leave standstill 12-24h under 4-10 DEG C of condition, after filtration, get supernatant, removing ethanol, concentrated after 70-80 DEG C dry, pulverize into fine powder, after sieving and get final product.
Wherein, the sonification power in step (2) is 100-150W.
Compared with prior art, advantage of the present invention is:
The present invention adopts the acid-hydrolyzed method of ultrasonic assistant to extract in Cornu Bubali and obtains effective ingredient, and effectively improve extraction efficiency and the utilization rate of raw materials of effective ingredient, constant product quality, productive rate are high, and process route is simple, practical.
Detailed description of the invention
Embodiment 1
The production technology of Pulvis Cornus Bubali Concentratus of the present invention, comprises the following steps:
(1) pretreatment of raw material: water intaking Cornu Bovis seu Bubali, cleans, sawed-off, except chamfering plug, remaining part is ground to form 50 object powder;
(2) ultrasonic assistant acid hydrolysis: add the acetum of 8% by solid-liquid ratio 1:10, first 50 DEG C of Water Under solution 25h, supersound process 10min under 70 DEG C of conditions again, add the acetum 50 DEG C hydrolysis 15h of same concentration, same volume again, supersound process 5min under 70 DEG C of conditions again, filter and collect filtrate, obtaining extracting solution;
(3) remove impurity: the pH of extracting solution is adjusted to 7 with NaOH, filters after leaving standstill 3h;
(4) refining: the ethanol adding 4 times of volumes 95% in the filtrate obtained in (3), leave standstill 12h under 4 DEG C of conditions, after filtration, get supernatant, removing ethanol, concentrated latter 70 DEG C dry, pulverize into fine powder, after sieving and get final product.
Wherein, the sonification power in step (2) is 100W.
Through inspection, product yield is greater than 15%, and wherein amino acid content is greater than 80%.
Claims (2)
1. a production technology for Pulvis Cornus Bubali Concentratus, is characterized in that, comprises the following steps:
(1) pretreatment of raw material: water intaking Cornu Bovis seu Bubali, cleans, sawed-off, except chamfering plug, remaining part is ground to form 50-100 object powder;
(2) ultrasonic assistant acid hydrolysis: the acetum adding 6-8% by solid-liquid ratio 1:10-1:8, first 40-50 DEG C of Water Under solution 20-30h, supersound process 10-15min under 60-70 DEG C of condition again, add acetum 40-50 DEG C of hydrolysis 15-20h of same concentration, same volume again, supersound process 5-10min under 60-70 DEG C of condition again, filter and collect filtrate, obtaining extracting solution;
(3) remove impurity: the pH of extracting solution is adjusted to 6-7 with NaOH, filters after leaving standstill 2-4h;
(4) refining: the ethanol adding 4-6 times of volume 95% in the filtrate obtained in (3), leave standstill 12-24h under 4-10 DEG C of condition, after filtration, get supernatant, removing ethanol, concentrated after 70-80 DEG C dry, pulverize into fine powder, after sieving and get final product.
2. the production technology of a kind of Pulvis Cornus Bubali Concentratus according to claim 1, is characterized in that, the sonification power in described step (2) is 100-150W.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410719148.0A CN104523752A (en) | 2014-12-03 | 2014-12-03 | Process for producing cornu bubali concentration powder |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410719148.0A CN104523752A (en) | 2014-12-03 | 2014-12-03 | Process for producing cornu bubali concentration powder |
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| Publication Number | Publication Date |
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| CN104523752A true CN104523752A (en) | 2015-04-22 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410719148.0A Pending CN104523752A (en) | 2014-12-03 | 2014-12-03 | Process for producing cornu bubali concentration powder |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106727349A (en) * | 2016-12-22 | 2017-05-31 | 江西济民可信药业有限公司 | A kind of preparation method for concentrating cornu bubali particle |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102372749A (en) * | 2010-08-25 | 2012-03-14 | 浙江科技学院 | Method for preparing D-glucosamine hydrochloride by utilizing sleeve-fish sheathes |
| CN103622998A (en) * | 2012-08-21 | 2014-03-12 | 黄胜文 | Production method for concentrated buffalo horn powder |
| CN104510758A (en) * | 2015-01-10 | 2015-04-15 | 江西济民可信药业有限公司 | Cornu bubali concentrated powder and preparation method for concentrated cornu bubali particles |
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2014
- 2014-12-03 CN CN201410719148.0A patent/CN104523752A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102372749A (en) * | 2010-08-25 | 2012-03-14 | 浙江科技学院 | Method for preparing D-glucosamine hydrochloride by utilizing sleeve-fish sheathes |
| CN103622998A (en) * | 2012-08-21 | 2014-03-12 | 黄胜文 | Production method for concentrated buffalo horn powder |
| CN104510758A (en) * | 2015-01-10 | 2015-04-15 | 江西济民可信药业有限公司 | Cornu bubali concentrated powder and preparation method for concentrated cornu bubali particles |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106727349A (en) * | 2016-12-22 | 2017-05-31 | 江西济民可信药业有限公司 | A kind of preparation method for concentrating cornu bubali particle |
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Application publication date: 20150422 |
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