CN104522307A - Method for preparing allicin soluble clathrate granules - Google Patents
Method for preparing allicin soluble clathrate granules Download PDFInfo
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- CN104522307A CN104522307A CN201410834074.5A CN201410834074A CN104522307A CN 104522307 A CN104522307 A CN 104522307A CN 201410834074 A CN201410834074 A CN 201410834074A CN 104522307 A CN104522307 A CN 104522307A
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- allicin
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- monoglyceride
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Abstract
The invention provides a method for preparing allicin soluble clathrate granules. The method mainly comprises the following steps: firstly, adding natural edible oil into allicin at a weight ratio of 1: (0.5-1), and stirring for 5-10 minutes until the solution is clear, wherein the natural edible oil is preferably palm oil; secondly, heating to 60-70 DEG C by using a steaming plant to melt monoglyceride into a liquid state, mixing the liquid monoglyceride with the solution obtained in the first step, and stirring to form an allicin clathrate compound, wherein the dosage of the monoglyceride is 50-80% of that of the solution; thirdly, adding a carrier into the clathrate compound obtained in the second step, and further stirring to obtain clathrate granules, wherein the sum of the allicin clathrate compound and a carrier is 100%, and the carrier is preferably white carbon black. The steps of the method provided by the invention are carried out under normal temperature and normal pressure, the used equipment and operation are simple and feasible, the pungent smell of allicin products can be effectively alleviated, and the method has the advantages of obvious effect, remarkable effect, etc.
Description
One, technical field: the invention belongs to feed additive field, particularly relates to the preparation method that a kind of allicin fuses inclusion particle.
Two, technical background:
What China have " garlic goes on the market, and closes the door in herbal medicine shop " says.Record in Ming Dynasty's Li Shizhen (1518-1593 A.D.) Compendium of Material Medica: " garlic, its gas is smoked strong, logical the five internal organs, reach all keys, dispellieg cold and dampness, evils of avoiding evil spirits, detumescence pain, eliminate indigestion eat, this its merit is also ".Garlic (Allium Sativam L) has the medicine feeding value of several thousand in China, be under the jurisdiction of the underground bulb of Liliaceae allium, is also the medicine-food two-purpose plant that a kind of global, whole mankind generally acknowledges.It contains the volatile oil of 0.2%, i.e. the sulfide compound etc. of allicin, allicin and multiple pi-allyl, propyl group, methyl composition.Wherein, allicin is mainly generated by the alliin in garlic and allinase reaction, industrial can by a kind of water-fast yellowish clear oil material of the Material synthesis such as chloropropene, sodium thiosulfate, main component is Ailitridin, because having special stink and piquant taste, limit the application of garlic product.For this reason, people have developed multiple technologies and process allicin.As the odorless garlic manufacturing process of application, the organic solvent such as ethanol, acetic acid is utilized to carry out immersion treatment to obtain.The allicin production method of applying for for another example, in the liquid phase and under the protection of inert gas, tested the deodorization process of garlic by the step such as secondary sterilization, pulverizing.The present invention uses natural edible oil, monoglyceride processes, safety non-pollution, easy to operation.
Three, summary of the invention:
1, the object of this invention is to provide the preparation method that a kind of allicin fuses inclusion particle,
Another object of the present invention is that to be to provide a kind of take allicin as the functional feedstuff additive of main component, and its feature is that volatility is low, and excitant is little.
2, the present invention is realized by following processing step:
A, in allicin, add natural edible oil, weight ratio is 1: 0.5 ~ 1, stirs and clarifies to solution for 5-10 minute.
B, employing steaming plant are heated to 60-70 DEG C and monoglyceride are melted into liquid state, and mix with gained solution in step one, be stirred to and form allicin inclusion compound, monoglyceride consumption is the 50-80% of solution.
C, in step 2 gained inclusion compound in add carrier, continue to stir to obtain inclusion particle, allicin inclusion compound+carrier=100%.
Natural edible oil comprises: palm oil, soybean oil, rapeseed oil, sunflower oil, peanut oil.
Natural edible oil preferably palm oil.
Carrier comprises: white carbon, adds beneficial powder, silica flour.
The preferred white carbon of carrier.
For technical scheme of the present invention is described better, spy provides following examples, but the present invention is not limited to this.
Embodiment 1:
1, take allicin 15kg, add the palm oil of 7.5kg, at room temperature fully mix above-mentioned raw materials, stir and clarify to solution for 5-10 minute;
2, adopt steaming plant to be heated to 65 DEG C and melt 11.25kg monoglyceride, the solution in step 1 is mixed with monoglyceride, is stirred to and forms allicin inclusion compound;
3, will add the white carbon of 67.5kg in the inclusion compound of gained in step 2, continuation stirring obtains allicin and fuses inclusion particle.
Embodiment 2
1, take allicin 15kg, add the palm oil of 11.25kg, at room temperature fully mix above-mentioned raw materials, stir and clarify to solution for 5-10 minute;
2, adopt steaming plant to be heated to 65 DEG C and melt 17kg monoglyceride, the solution in step 1 is mixed with monoglyceride, is stirred to and forms allicin inclusion compound;
3, the inclusion compound worm of gained in step 2 is added the white carbon of 57kg, continuation stirring obtains allicin and fuses inclusion particle.
Embodiment 3
1, take allicin 15kg, add the palm oil of 15kg, at room temperature fully mix above-mentioned raw materials, stir and clarify to solution for 5-10 minute;
2, adopt steaming plant to be heated to 65 DEG C and melt 24kg monoglyceride, the solution in step 1 is mixed with monoglyceride, is stirred to and forms allicin inclusion compound;
3, will add the white carbon of 47kg in the inclusion compound of gained in step 2, continuation stirring obtains allicin and fuses inclusion particle.
Embodiment 4
Take above-mentioned gained allicin and fuse inclusion particle 200g, join in the animal feed of 100kg, stir and evenly mix, 20 DEG C of storages measured its changes of contents after 2 months; After 85 DEG C are granulated, measure the content of allicin in feed, result is as follows:
Claims (5)
1. allicin fuses a preparation method for inclusion particle, it is characterized in that it adopts following process steps:
A, in allicin, add natural edible oil, weight ratio is 1: 0.5 ~ 1, stirs and clarifies to solution for 5-10 minute.
B, employing steaming plant are heated to 60-70 DEG C and monoglyceride are melted into liquid state, and mix with gained solution in step one, be stirred to and form allicin inclusion compound, monoglyceride consumption is the 50=80% of solution.
C, in step 2 gained inclusion compound in add carrier, continue to stir to obtain inclusion particle, allicin inclusion compound+carrier=100%.
2. allicin according to claim 1 fuses the preparation method of inclusion particle, it is characterized in that the natural edible oil described in above-mentioned steps A comprises: palm oil, soybean oil, rapeseed oil, sunflower oil, peanut oil.
3. allicin according to claim 1 and 2 fuses the preparation method of inclusion particle, it is characterized in that the natural edible oil preferably palm oil described in above-mentioned steps A.
4. allicin according to claim 1 fuses the preparation method of inclusion particle, it is characterized in that the carrier described in above-mentioned steps C comprises: white carbon, adds beneficial powder, silica flour.
5. the allicin according to claim 1 or 4 fuses the preparation method of inclusion particle, it is characterized in that the preferred white carbon of carrier described in above-mentioned steps C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410834074.5A CN104522307A (en) | 2014-12-25 | 2014-12-25 | Method for preparing allicin soluble clathrate granules |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410834074.5A CN104522307A (en) | 2014-12-25 | 2014-12-25 | Method for preparing allicin soluble clathrate granules |
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| CN104522307A true CN104522307A (en) | 2015-04-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410834074.5A Pending CN104522307A (en) | 2014-12-25 | 2014-12-25 | Method for preparing allicin soluble clathrate granules |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111870588A (en) * | 2020-08-24 | 2020-11-03 | 广州立达尔生物科技股份有限公司 | Method for preparing allicin microcapsule by coupling carrier adsorption and precipitation |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565430A (en) * | 2003-06-22 | 2005-01-19 | 毛友昌 | Allicin cyclodextrin clathrate compound, formulation and its preparation method |
-
2014
- 2014-12-25 CN CN201410834074.5A patent/CN104522307A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1565430A (en) * | 2003-06-22 | 2005-01-19 | 毛友昌 | Allicin cyclodextrin clathrate compound, formulation and its preparation method |
Non-Patent Citations (2)
| Title |
|---|
| 徐帮学: "《最新食品工业生产新工艺新艺术与创新配方设计及产品分析检测实用手册 第2卷》", 31 May 2004, 银声音像出版社 * |
| 李祥明等: "《饲料药物添加剂质量标准与检验方法》", 31 March 1999, 中国科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111870588A (en) * | 2020-08-24 | 2020-11-03 | 广州立达尔生物科技股份有限公司 | Method for preparing allicin microcapsule by coupling carrier adsorption and precipitation |
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Owner name: BEIJING RESOURCE YATAI ANIMAL MEDICINE CO., LTD. Free format text: FORMER OWNER: ZIYUAN YATAI FEED SCIENCE + TECHNOLOGY CO., LTD., BEIJING Effective date: 20150515 |
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Effective date of registration: 20150515 Address after: 102600 Beijing city Daxing District yufazhen this Wing Street No. 98 Applicant after: Beijing Resource Yatai Animal Medicine Co., Ltd. Address before: 102600 Beijing city Daxing District Huangcun Xing Zheng Street No. 31 building eight layer technology Applicant before: Beijing Resource Asia-Pacific Feed Technology Co., Ltd. |
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Application publication date: 20150422 |