CN104501948A - Preparation method of visual ultraviolet intensity detection glue - Google Patents
Preparation method of visual ultraviolet intensity detection glue Download PDFInfo
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- CN104501948A CN104501948A CN201510023919.7A CN201510023919A CN104501948A CN 104501948 A CN104501948 A CN 104501948A CN 201510023919 A CN201510023919 A CN 201510023919A CN 104501948 A CN104501948 A CN 104501948A
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Abstract
The invention relates to a preparation method of visual ultraviolet intensity detection glue. The preparation method of the visual ultraviolet intensity detection glue solves the problem that an existing detection device is difficult to popularize due to complex circuits or processing technology. The preparation method of the visual ultraviolet intensity detection glue includes: 1, preparing gel; 2, spreading the gel; 3, arranging a color colorimetric card. The visual ultraviolet intensity detection glue prepared through the preparation method of the visual ultraviolet intensity detection glue can indicate intensity of ultraviolet light in sunlight through color change of a film, can achieve color changes after irradiation of the ultraviolet light, enables a person to distinguish the color changes through naked eyes, and is suitable for convenient and fast detection of the ultraviolet light in the outdoor sunlight, simple in structure, low in cost and easy to manufacture. The preparation method of the visual ultraviolet intensity detection glue is used to manufacture the visual ultraviolet intensity detection glue used to detect the intensity of the ultraviolet light.
Description
Technical field
The present invention relates to the preparation method detecting sticker.
Background technology
Excessive ultraviolet causes photochemical reaction, can make function of human body that a series of change occurs, and especially works the mischief to the skin of human body, eyes and immune system etc.In recent years in state and some cities of China such as the U.S., Canada, Australia, start to issue ultraviolet radiation index prediction, taked corresponding safeguard procedures to remind the public.But pick-up unit relevant is in the market not suitable for large-scale popularization owing to relating to complicated circuit or processing technology.
Summary of the invention
The present invention will solve current pick-up unit owing to relating to complicated circuit or processing technology, is difficult to the problem promoted, and provides a kind of visual uitraviolet intensity to detect the preparation method of sticker.
Visual uitraviolet intensity detects a preparation method for sticker, specifically carries out according to following steps:
One, purpurine material is added in the aqueous solution containing polyvinyl alcohol (PVA), then add polymolybdote, stir, then add polyethyleneimine and become clarification to solution, continue to stir 24h, obtain visual uitraviolet intensity and detect sticker gel;
Two, the gel coating prepared by step one in the side of adhesive sticker substrate, natural drying;
Three, color colorimetric card is arranged on the opposite side of adhesive sticker substrate, completes the preparation method that a kind of visual uitraviolet intensity detects sticker.
The invention has the beneficial effects as follows:
The present invention adopts purpurine material, mineral acid and organic polymer to be prepared into gel, is coated in adhesive sticker substrate.Such plural gel coating has good response for UVB and UVC ultraviolet, and under film is subject to varying strength UV-irradiation, will become the different blueness of the depth, it is higher that blueness more deeply feels bright uitraviolet intensity.Therefore ultraviolet measuring ability can be realized by the change of coating before and after strong UV-irradiation.Another one function is, this sticker can return to colourless state after becoming blueness under the condition of steam, reusable more than 30 times of each sticker.The present invention can realize the change of the color after UV-irradiation, and naked eyes can be differentiated, and are suitable for the easy detection of outdoor solar UV, and structure is simple, with low cost, is easy to manufacture.
The present invention prepares a kind of visual uitraviolet intensity and detects sticker, and the color change by film indicates the power of daylight middle-ultraviolet lamp, instructs protection during trip.
The present invention can be pasted onto the surfaces such as mobile phone, dress ornament, personal effects, is changed the power indicating daylight middle-ultraviolet lamp by color.
The present invention prepares visual uitraviolet intensity and detects sticker for detecting uitraviolet intensity.
Accompanying drawing explanation
Fig. 1 is that visual uitraviolet intensity prepared by embodiment one detects sticker.
Embodiment
Technical solution of the present invention is not limited to following cited embodiment, also comprises the combination in any between each embodiment.
Embodiment one: a kind of visual uitraviolet intensity of present embodiment detects the preparation method of sticker, specifically carries out according to following steps:
One, purpurine material is added in the aqueous solution containing polyvinyl alcohol (PVA), then add polymolybdote, stir, then add polyethyleneimine and become clarification to solution, continue to stir 24h, obtain visual uitraviolet intensity and detect sticker gel;
Two, the gel coating prepared by step one in the side of adhesive sticker substrate, natural drying;
Three, color colorimetric card is arranged on the opposite side of adhesive sticker substrate, completes the preparation method that a kind of visual uitraviolet intensity detects sticker.
Embodiment two: present embodiment and embodiment one unlike: in step one, purpurine material is a kind of or any two kinds of potpourris by any mass ratio in methyl viologen, ethyl purpurine, propyl group purpurine and aminopropyl purpurine.Other is identical with embodiment one.
Embodiment three: present embodiment and embodiment one unlike: in step one polyvinyl alcohol (PVA) aqueous solution in the quality of polyvinyl alcohol (PVA) and the volume ratio of water be (20 ~ 150) mg:2mL.Other is identical with embodiment one.
Embodiment four: present embodiment and embodiment one unlike: in step one, polymolybdote is one or more potpourris by any mass ratio in 12 molybdophosphate sodium salts, 12 molybdophosphate sylvite, 12 molybdenum silicic acid sodium salts and 12 molybdophosphate sylvite.Other is identical with embodiment one.
Embodiment five: present embodiment and embodiment one unlike: in step 2, the area of gel coating is 1 ~ 4cm
2, thickness is 0.05 ~ 0.15mm.Other is identical with embodiment one.
Embodiment six: present embodiment and embodiment one unlike: in step 3, color colorimetric card is the high definition picture after Test paper is tested under different radiant quantity Ultraviolet radiation.Other is identical with embodiment one.
Embodiment seven: present embodiment and embodiment six unlike: EUV illuminating radiation amount is 100 μ W/cm
2, 200 μ W/cm
2, 300 μ W/cm
2, 350 μ W/cm
2with 500 μ W/cm
2.Other is identical with embodiment six.
Following examples are adopted to verify beneficial effect of the present invention:
Embodiment one:
A kind of visual uitraviolet intensity of the present embodiment detects the preparation method of sticker, specifically carries out according to following steps:
One, purpurine material is added in the aqueous solution containing polyvinyl alcohol (PVA), then add polymolybdote, stir, then add polyethyleneimine and become clarification to solution, continue to stir 24h, obtain visual uitraviolet intensity and detect sticker gel;
Two, the gel coating prepared by step one in the side of adhesive sticker substrate, natural drying;
Three, color colorimetric card is arranged on the opposite side of adhesive sticker substrate, completes the preparation method that a kind of visual uitraviolet intensity detects sticker.
In the present embodiment, in step one, purpurine material is methyl viologen, and in the aqueous solution of polyvinyl alcohol (PVA), the quality of polyvinyl alcohol (PVA) and the volume ratio of water are 150mg:2mL, and polymolybdote is 12 molybdophosphate sodium salts; In step 2, the area of gel coating is 1cm
2, thickness is 0.1mm, and in step 3, color colorimetric card is Test paper is 100 μ W/cm in radiant quantity
2, 200 μ W/cm
2, 300 μ W/cm
2, 350 μ W/cm
2with 500 μ W/cm
2high definition picture under Ultraviolet radiation after test.
Visual uitraviolet intensity prepared by the present embodiment detects sticker as shown in Figure 1, and wherein 1 represent gel, 2 represent adhesive sticker substrate, 3 representative color colorimetric cards, under film is subject to varying strength UV-irradiation, will become the different blueness of the depth, it is higher that blueness more deeply feels bright uitraviolet intensity, the change of the color after UV-irradiation can be realized, naked eyes can be differentiated, and be suitable for the easy detection of outdoor solar UV, structure is simple, with low cost, be easy to manufacture.
Claims (7)
1. visual uitraviolet intensity detects a preparation method for sticker, it is characterized in that what the method was specifically carried out according to following steps:
One, purpurine material is added in the aqueous solution containing polyvinyl alcohol (PVA), then add polymolybdote, stir, then add polyethyleneimine and become clarification to solution, continue to stir 24h, obtain visual uitraviolet intensity and detect sticker gel;
Two, the gel coating prepared by step one in the side of adhesive sticker substrate, natural drying;
Three, color colorimetric card is arranged on the opposite side of adhesive sticker substrate, completes the preparation method that a kind of visual uitraviolet intensity detects sticker.
2. a kind of visual uitraviolet intensity according to claim 1 detects the preparation method of sticker, it is characterized in that in step one, purpurine material is a kind of or any two kinds of potpourris by any mass ratio in methyl viologen, ethyl purpurine, propyl group purpurine and aminopropyl purpurine.
3. a kind of visual uitraviolet intensity according to claim 1 detects the preparation method of sticker, it is characterized in that the quality of polyvinyl alcohol (PVA) in the aqueous solution of polyvinyl alcohol (PVA) in step one and the volume ratio of water are (20 ~ 150) mg:2mL.
4. a kind of visual uitraviolet intensity according to claim 1 detects the preparation method of sticker, it is characterized in that in step one, polymolybdote is one or more potpourris by any mass ratio in 12 molybdophosphate sodium salts, 12 molybdophosphate sylvite, 12 molybdenum silicic acid sodium salts and 12 molybdophosphate sylvite.
5. a kind of visual uitraviolet intensity according to claim 1 detects the preparation method of sticker, it is characterized in that the area of gel coating in step 2 is 1 ~ 4cm
2, thickness is 0.05 ~ 0.15mm.
6. a kind of visual uitraviolet intensity according to claim 1 detects the preparation method of sticker, it is characterized in that in step 3, color colorimetric card is the high definition picture after Test paper is tested under different radiant quantity Ultraviolet radiation.
7. a kind of visual uitraviolet intensity according to claim 6 detects the preparation method of sticker, it is characterized in that EUV illuminating radiation amount is 100 μ W/cm
2, 200 μ W/cm
2, 300 μ W/cm
2, 350 μ W/cm
2with 500 μ W/cm
2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510023919.7A CN104501948A (en) | 2015-01-16 | 2015-01-16 | Preparation method of visual ultraviolet intensity detection glue |
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| CN201510023919.7A CN104501948A (en) | 2015-01-16 | 2015-01-16 | Preparation method of visual ultraviolet intensity detection glue |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106066204A (en) * | 2015-04-24 | 2016-11-02 | 南昌欧菲光学技术有限公司 | A kind of uitraviolet intensity detection device and the manufacture method of this device |
| CN110730902A (en) * | 2017-11-07 | 2020-01-24 | 图尔库大学 | Indicating the intensity of a predetermined type of radiation |
| CN113913061A (en) * | 2021-11-22 | 2022-01-11 | 亚士创能科技(上海)股份有限公司 | Heat-insulating heat-preserving weather-resistant coating and preparation method and application thereof |
| CN114497273A (en) * | 2021-12-17 | 2022-05-13 | 济南大学 | Preparation method of flexible visual ultraviolet detector |
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| CN1350048A (en) * | 2000-10-23 | 2002-05-22 | 阿托费纳化学股份有限公司 | Narrow-arranged poly-phosphinodifluoro-ethylene reversible and electrocontrollable transparent film, its making mehtod, product and composition therefrom |
| CN1928233A (en) * | 2005-09-08 | 2007-03-14 | 施乐公司 | Reimageable paper |
| CN201983858U (en) * | 2010-01-14 | 2011-09-21 | 陕西国防工业职业技术学院 | Portable ultraviolet detection device |
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Patent Citations (3)
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| CN1350048A (en) * | 2000-10-23 | 2002-05-22 | 阿托费纳化学股份有限公司 | Narrow-arranged poly-phosphinodifluoro-ethylene reversible and electrocontrollable transparent film, its making mehtod, product and composition therefrom |
| CN1928233A (en) * | 2005-09-08 | 2007-03-14 | 施乐公司 | Reimageable paper |
| CN201983858U (en) * | 2010-01-14 | 2011-09-21 | 陕西国防工业职业技术学院 | Portable ultraviolet detection device |
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| 姚振国等: "紫精类杂化光致变色材料的研究进展", 《广东化工》, vol. 41, no. 12, 31 December 2014 (2014-12-31), pages 237 - 238 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106066204A (en) * | 2015-04-24 | 2016-11-02 | 南昌欧菲光学技术有限公司 | A kind of uitraviolet intensity detection device and the manufacture method of this device |
| CN106066204B (en) * | 2015-04-24 | 2019-09-06 | 南昌欧菲光学技术有限公司 | A kind of production method of uitraviolet intensity detection device and the device |
| CN110730902A (en) * | 2017-11-07 | 2020-01-24 | 图尔库大学 | Indicating the intensity of a predetermined type of radiation |
| CN113913061A (en) * | 2021-11-22 | 2022-01-11 | 亚士创能科技(上海)股份有限公司 | Heat-insulating heat-preserving weather-resistant coating and preparation method and application thereof |
| CN114497273A (en) * | 2021-12-17 | 2022-05-13 | 济南大学 | Preparation method of flexible visual ultraviolet detector |
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Application publication date: 20150408 |