CN104498936B - The method that mechanical induction synthesizes metal ceramic wear-resisting layer - Google Patents
The method that mechanical induction synthesizes metal ceramic wear-resisting layer Download PDFInfo
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- CN104498936B CN104498936B CN201410749468.0A CN201410749468A CN104498936B CN 104498936 B CN104498936 B CN 104498936B CN 201410749468 A CN201410749468 A CN 201410749468A CN 104498936 B CN104498936 B CN 104498936B
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- metal ceramic
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C24/00—Coating starting from inorganic powder
- C23C24/02—Coating starting from inorganic powder by application of pressure only
- C23C24/06—Compressing powdered coating material, e.g. by milling
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/14—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silica
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Structural Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
- Coating By Spraying Or Casting (AREA)
Abstract
The invention discloses a kind of surface treatment method, especially a kind of method of mechanical induction synthesis metal ceramic wear-resisting layer.The present invention provides the method for mechanical induction synthesis metal ceramic wear-resisting layer a kind of easy to operate and relatively low energy consumption, comprise the following steps：A, friction pair is built using mechanical equipment, and pending part is formed the secondary part of friction；B, the surface spraying secondary on pending part time job surface and its corresponding friction covers one layer of anti-wear agent；C, load is applied to friction is secondary, operation mechanical equipment causes the subtask that rubs；D, after friction subtask to the time set, the part being disposed with higher temperature is taken out, is cooled to room temperature under field conditions (factors).Due to synthesizing metal ceramic wear-resisting layer using mechanical induction, compared with other surface modifying methods, this method has stronger stability, and will not produce because the uneven distribution that heat treatment causes part base solid materials microstructure structure to change with performance.
Description
Technical field
The present invention relates to a kind of surface treatment method, especially a kind of side of mechanical induction synthesis metal ceramic wear-resisting layer
Method.
Background technology
In order to improve the wearability of machine components and the working life in severe Service Environment, domestic and international researcher couple
The surface strengthening technology of part has carried out substantial amounts of research work, and the theory i.e. surface for foring comparative maturity is modified theory.
Such as traditional shot peening strengthening, Surface heat-treatent, the surface treatment of high-energy ionic beam and built-up welding, PVD coating surface engineering technologies.
Its reinforcing approach is predominantly by varying machinery part surface institutional framework or constituent so as to obtain required performance.
Matsumoto etc. uses induction coil electrode assembly, produces nitrogen or nitrogen-hydrogen plasma, thus to titanium, steel etc. into
Surfaces nitrided processing is gone, TiN layer and the Fe that thickness is about 10 μm in the Surface Creation of titanium and steel4N layers, finally so that material
Wear resistance and corrosion resistance be greatly improved, open using plasma this high energy beam to material table
Face is modified the new page of processing.Fang Yu of Harbin Institute of Technology et al. have studied a kind of using spark erosion technique
Surface modifying method, it is on the basis of traditional electric discharge machining method, by special semi-sintered electrode, in electrical fire
One layer of hard carbide ceramics can be quickly formed in workpiece surface in flower process, so that reaching improves workpiece surface performance
Purpose.PVD (physical vapour deposition (PVD)) coating process succeeded in developing in recent years by multi sphere Vacuum equipment maker of the U.S., Ke Yi
Material surface depositing TiN, Al2O3, TiC etc. there is high rigidity, high abrasion, Gao Naichong and the low coating of friction coefficient so that machinery
Part service life is obviously prolonged.
Although surface engineering technology is quickly grown, many technical problems are still remained in terms of engineer application, such as：It is right
For new technology, technical know-how research is still immature, and industrial applications effect is unsatisfactory, of high cost；In traditional table
In terms of face modification treatment technology, it is various and consume energy tight to equally exist manufacture long processing period, surface modification treatment process
Weight, problems of high cost；In addition some processing methods can also produce pollution to environment.At energy-efficient, environmentally friendly efficiency
Have in mind, it is very urgent to develop new processing technology for surface modification.
The content of the invention
The technical problems to be solved by the invention are to provide mechanical induction synthesis gold a kind of easy to operate and relatively low energy consumption
Belong to the method for ceramic wearing coat.
The method of mechanical induction synthesis metal ceramic wear-resisting layer used by its technical problem of present invention solution, including it is following
Step：
A, friction pair is built using mechanical equipment, and pending part is formed the secondary part of friction；
B, the surface spraying secondary on pending part time job surface and its corresponding friction covers one layer of anti-wear agent；
C, load is applied to friction is secondary, operation mechanical equipment causes the subtask that rubs；
D, after friction subtask to the time set, the part of being disposed with higher temperature is taken out and cold
But.
It is further that in step A, before structure friction is secondary, pending part is done into oil removal treatment first.
It is further that the oil removal treatment is in the following ways：Pending part is changed in electrochemical deoiling liquid
Oil removal treatment is learned, oil is dipped to and eliminates, then takes out and stands a period of time at room temperature.
It is 500N~8000N to the secondary load applied of friction in step C to be further.
Be further, in step C, when rub subtask when, it is resistance to according to the surface supply that actual conditions are secondary to friction
Grinding agent.
Be further, in D steps, time for setting as 5 minutes~16 it is small when.
It is further that the material of pending part is all metal materials.
It is further that anti-wear agent used is by SiO2、Al2O3、TiO2、Fe2O3、MgO、K2O、CaO、MoS2Mixed preparing
Form.
It is further that the mass percent of anti-wear agent component is：SiO2For 40~60%, Al2O3For 20~40%,
TiO2For 1~5%, Fe2O3It is 1~5%, K for 1~5%, MgO2O is that 0.3~4%, CaO is 0.1~3%, MoS2For 0.05~
2%.
It is further that the frequency of the friction subtask is per minute for 500~4000 times.Wait to locate for revolution class
Part is managed, working frequency is exactly 500~4000 rpms.
It is of the invention to be had the following advantages compared with existing conventional art：
1st, in the technique of surface treatment, the present invention synthesizes metal ceramic wear-resisting layer using mechanical induction, and other
Surface modifying method is compared, and this method has stronger stability, and will not be produced because heat treatment causes part base solid material
The uneven distribution that changes with performance of institutional framework.
2nd, on the other hand the cycle of the surface modification treatment of the present invention compared to shorter, under normal conditions the single treatment time be
2~4 it is small when, and can once handle multiple parts, greatly improve production efficiency.
3rd, in the method, the anti-wear agent not made full use of may be reused, and improve the utilization rate of raw material, section
About production cost.
4th, since the method for the present invention can significantly improve part in piece surface inductive formation metal ceramic wear-resisting layer
Surface abrasion resistance, so as to improve the service life of part；By the practice examining in factory, part is carried out using the present invention
The service life of more than 10 times of parts with frication pair can be generally improved after surface modification treatment.
5th, invention method can repair the parts with frication pair by long-time wear out failure again, so that part
Recycling, the cost of a large sum of renewal part is saved for factory.
6th, surface-treated machine parts is carried out by the method for the present invention, due to good surface property, greatly
Reduce work generation noise and vibration, save be wasted in abrasion on the energy.The serious energy is faced in the whole world
Today of crisis, has saved the substantial amounts of energy in terms of industrial production；The important meaning for having broad prospects and promoting.
Brief description of the drawings
Fig. 1 is schematic diagram when pending part is handled using the present invention；
Parts, position and numbering in figure：Motor 1, fixing device 2, force application apparatus 3, fixed friction block 4, transmission device
5th, pending part 6.
Embodiment
The invention will be further described below in conjunction with the accompanying drawings.
The present invention comprises the following steps：
A, is placed on progress electrochemical deoiling processing in steel product electrochemical deoiling liquid by pending part 6, is dipped to oil and removes
To the greatest extent, then take out and stand a period of time at room temperature；The working surface of pending part 6 can be cylindrical, hole, it is complex-curved or
Person's plane etc., this step can be saved in the case of pending part 6 is more clean；
B, by modes such as mechanical equipment or mechanical processings, builds friction pair, pending part 6 is become friction pair
A part；The secondary existing mechanical equipment of generally use of structure friction can be completed, and select that equipment to need according to pending zero
6 working surface of part determines, such as when working surface is cylindrical or hole, it is possible to utilize the structure rolling friction of existing lathe
It is secondary；When working surface is complex-curved, then numerically controlled lathe can be used to build sliding friction pair；In Fig. 1, pending part 6
It is fixed in fixing device 2, it forms friction pair with the fixed friction block 4 on force application apparatus 3；
C, carries out anti-wear agent spraying on the secondary surface of friction respectively, by the nozzle in device in pending part during spraying
The surface of 6 working surfaces and corresponding friction pair covers one layer of anti-wear agent；Spraying is preferably maintained in uniformly, so that follow-up is rubbed
Wipe；Anti-wear agent mainly uses common cermet raw material, such as oxide, carbide, nitride, boride, silicide etc.
Material, can match according to demand.
D, as shown in Figure 1, giving friction the secondary load for applying 500N~8000N by force application apparatus 3, runs motor 1, transmission
Device 5 pending part 6 rotated, be translatable or curvilinear motion, so that friction subtask, pending part 6 at this time
Working surface will rub with the fixed friction block 4 of another part, the anti-wear agent and pending zero under the action of high moderate pressure
The working surface of part 6 gradually mixes, and finally forms cermet coating in pending part 6, meanwhile, can root in the process of running
Anti-wear agent is fed in time according to the actual conditions surface secondary to friction；This mode is advantageous in that friction can not only produce office
Portion's high temperature, and anti-wear agent can be made to be evenly distributed, this causes the working face inductive formation metal ceramic wear-resisting layer of pending part 6
It is more uniform；
E, with 5min~16 when small after the part of being disposed with higher temperature is taken out, it is cold under field conditions (factors)
But to room temperature, finally part is cleared up；It can also use and force cooling, depending on needing as the case may be.
In above method, pending 6 material of part is all metals.Such as cast iron, steel, copper, aluminium metal material, can also
It is alloy material.
In above method, the anti-wear agent used in the step C is by including SiO2、Al2O3、TiO2、Fe2O3、MgO、K2O、
CaO、MoS2Component mixed preparing forms.Specific component and content are shown in Table 1.
1 anti-wear agent component (wt/%) of table
| Component | SiO2 | Al2O3 | TiO2 | Fe2O3 | MgO | K2O | CaO | MoS2 |
| Content | 40-60 | 20-40 | 1-5 | 1-5 | 1-5 | 0.3-4 | 0.1-3 | 0.05-2 |
In above method, in the step D parameter regulation scope of rotating speed and load according to workpiece material it is different
Difference, is specially：Fricting movement 500~4000r/min of rotating speed, pressure loading is in 500N~8000N scopes；On the other hand carry out
The time of surface modification treatment, its probable ranges was when 5min~16 are small depending on specific works condition.
Embodiment is given below so that the present invention to be specifically described, it is necessary to which indicated herein is following embodiments
It is used to further illustrate the present invention, it is impossible to be interpreted as limiting the scope of the invention, which is skilled in technique
Personnel's some nonessential modifications and adaptations that content makes the present invention according to the present invention still belong to protection scope of the present invention.
In addition, what deserves to be explained is the element percentage used in following embodiments is weight percentage；After processing
The hardness measurement of part carries out on the type Brinell's machines of HB -3000.
Case study on implementation 1
(No. 45 quenched for common machine parts steel for the part material of carry out surface modification treatment used in inventive embodiments
Steel), part outer surface is cylindrical, and friction pair is built by mechanical device on part outer surface, adds anti-wear agent operation, used
Wear-resisting agent prescription is 50%SiO2, 40%Al2O3, 3%TiO2, 2%Fe2O3, 2.5%MgO, 1.3%K2O, 0.3%CaO,
0.9%MoS2, rotating speed 900r/min, pressure 3500N, the secondary run time that rubs is 1h, completes mechanical induction synthesis table
Face ceramic layer thickness is 2 microns, and piece surface HB hardness is 210.
Case study on implementation 2
The part material of carry out surface modification treatment used in inventive embodiments is common machine parts steel (Q235), zero
Part outer surface is cylindrical, and friction pair is built by mechanical device on part outer surface, adds anti-wear agent operation, anti-wear agent used
It is formulated as 45%SiO2, 45%Al2O3, 2%TiO2, 2%Fe2O3, 3.5%MgO, 1.4%K2O, 0.2%CaO, 0.9%MoS2,
Rotating speed is 4000r/min, pressure 2000N, and the secondary run time that rubs is 7h, completes mechanical induction synthetic surface ceramics thickness
Spend for 12 microns, piece surface HB hardness is 260.
Case study on implementation 3
The part material of carry out surface modification treatment used in inventive embodiments is common machine parts steel (QT450),
Accessory inner surface is endoporus, and friction pair is built by mechanical device on accessory inner surface, adds anti-wear agent operation, used wear-resisting
Agent prescription is 50%SiO2, 41%Al2O3, 2%TiO2, 1%Fe2O3, 3.5%MgO, 1.1%K2O, 0.3%CaO, 1.1%
MoS2, rotating speed 1700r/min, pressure 8000N, the secondary run time that rubs is 16h, completes mechanical induction synthetic surface pottery
Porcelain thickness is 20 microns, and piece surface HB hardness is 280.
Case study on implementation 4
(No. 45 quenched for common machine parts steel for the part material of carry out surface modification treatment used in inventive embodiments
Steel), part outer surface is complex-curved, and friction pair is built by mechanical device on part outer surface, adds anti-wear agent operation,
Wear-resisting agent prescription used is 43%SiO2, 47%Al2O3, 1%TiO2, 4%Fe2O3, 2.5%MgO, 0.4%K2O, 2.1%CaO,
0.9%MoS2, rotating speed 3000r/min, pressure 7500N, the secondary run time that rubs is 3h, completes mechanical induction synthesis table
Face ceramic layer thickness is 21 microns, and piece surface HB hardness is 281.
Case study on implementation 5
The part material of carry out surface modification treatment used in inventive embodiments is common machine parts steel (2Cr13),
Part outer surface is complex-curved, and friction pair is built by mechanical device on part outer surface, adds anti-wear agent operation, used
Wear-resisting agent prescription is 40%SiO2, 50%Al2O3, 4%TiO2, 2%Fe2O3, 1.5%MgO, 1.3%K2O, 0.3%CaO,
0.9%MoS2, rotating speed 3000r/min, pressure 4500N, the secondary run time that rubs is 8h, completes mechanical induction synthesis table
Face ceramic layer thickness is 25 microns, and piece surface HB hardness is 300.
Claims (7)
1. the method that mechanical induction synthesizes metal ceramic wear-resisting layer, it is characterised in that：Comprise the following steps：
A, friction pair is built using mechanical equipment, and pending part is formed the secondary part of friction；
B, the surface even application secondary on pending part time job surface and its corresponding friction covers one layer of anti-wear agent, wear-resisting
The mass percent of agent component is：SiO2For 40~60%, Al2O3For 20~40%, TiO2For 1~5%, Fe2O3For 1~5%,
MgO is 1~5%, K2O is that 0.3~4%, CaO is 0.1~3%, MoS2For 0.05~2%；
C, load is applied to friction is secondary, operation mechanical equipment causes the subtask that rubs；
D, after when the subtask 5 minutes~16 that rubs is small, the part being disposed with higher temperature is taken out and cooled down.
2. the method for mechanical induction synthesis metal ceramic wear-resisting layer as claimed in claim 1, it is characterised in that：In step A,
Before structure friction is secondary, pending part is done into oil removal treatment first.
3. the method for mechanical induction synthesis metal ceramic wear-resisting layer as claimed in claim 2, it is characterised in that：At the oil removing
Reason is in the following ways：Pending part is subjected to electrochemical deoiling processing in electrochemical deoiling liquid, oil is dipped to and eliminates, Ran Houqu
Go out and stand a period of time at room temperature.
4. the method for mechanical induction synthesis metal ceramic wear-resisting layer as claimed in claim 1, it is characterised in that：In step C,
It is 500N~8000N to the secondary load applied of friction.
5. the method for mechanical induction synthesis metal ceramic wear-resisting layer as claimed in claim 1, it is characterised in that：In step C,
When rub subtask when, anti-wear agent is fed according to the surface that actual conditions are secondary to friction.
6. the method for mechanical induction synthesis metal ceramic wear-resisting layer as claimed in claim 1, it is characterised in that：Pending part
Material be all metal materials.
7. the method for the mechanical induction synthesis metal ceramic wear-resisting layer as described in claim 1 to 6 any claim, its feature
It is：The frequency of the friction subtask is per minute for 500~4000 times.
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Citations (4)
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| JPH09143671A (en) * | 1995-11-29 | 1997-06-03 | Suzuki Motor Corp | Surface treatment of aluminum material and its treatment film |
| CN101037635A (en) * | 2007-05-11 | 2007-09-19 | 徐远 | Abrasion-resistant agent having repairing function to metal frictional abrasion surface |
| CN102230063A (en) * | 2011-03-07 | 2011-11-02 | 孙静 | Method of forming nanostructure on friction surface of metal friction pair and special composition thereof |
| CN102344846A (en) * | 2011-09-06 | 2012-02-08 | 天津开发区双利工贸有限公司 | Lubricating oil with negative wear self-repair function and preparation method thereof |
-
2014
- 2014-12-09 CN CN201410749468.0A patent/CN104498936B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09143671A (en) * | 1995-11-29 | 1997-06-03 | Suzuki Motor Corp | Surface treatment of aluminum material and its treatment film |
| CN101037635A (en) * | 2007-05-11 | 2007-09-19 | 徐远 | Abrasion-resistant agent having repairing function to metal frictional abrasion surface |
| CN102230063A (en) * | 2011-03-07 | 2011-11-02 | 孙静 | Method of forming nanostructure on friction surface of metal friction pair and special composition thereof |
| CN102344846A (en) * | 2011-09-06 | 2012-02-08 | 天津开发区双利工贸有限公司 | Lubricating oil with negative wear self-repair function and preparation method thereof |
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