CN104473775B - A kind of tea polyphenols parcel system and preparation method thereof and product - Google Patents
A kind of tea polyphenols parcel system and preparation method thereof and product Download PDFInfo
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- CN104473775B CN104473775B CN201410671014.6A CN201410671014A CN104473775B CN 104473775 B CN104473775 B CN 104473775B CN 201410671014 A CN201410671014 A CN 201410671014A CN 104473775 B CN104473775 B CN 104473775B
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Abstract
The present invention relates to food and household chemicals field, and in particular to a kind of tea polyphenols parcel system and preparation method thereof and product.Tea polyphenols parcel system particle diameter is 70 1400 microns, from inside to outside successively comprising tea polyphenols kernel, filling oxidant layer and thin layer；Filling oxidant layer includes corn starch, Microcrystalline Cellulose and mannitol；Thin layer includes polylactic acid and polymethyl methacrylate；Mixture 15 part of the tea polyphenols parcel system by weight including 20 60 parts of tea polyphenols, 10 15 parts of corn starch, 10 15 parts of Microcrystalline Cellulose, 20 30 parts of mannitol, polylactic acid and polymethyl methacrylate.Its preparation includes successively：Dispensing；It is prepared by kernel；It is prepared by filling oxidant layer；It is prepared by thin layer：The mixture of polylactic acid and polymethyl methacrylate is added in 60 80 DEG C of ethanol and is placed 13 hours, after being completely dissolved and to form mixed liquor, using bed spray technique.Product of the present invention can effectively make tea polyphenols and air exclusion, storage time length, can discharge tea polyphenols when in use.
Description
Technical field
The present invention relates to food and household chemicals field, and in particular to a kind of tea polyphenols parcel system and preparation method thereof and system
Product.
Background technology
The technological means for currently existing are to be chemically modified tea polyphenols, and the defect of the method is the work of tea polyphenols
Property reduce, do not have due effect.Another kind of method is that tea polyphenols are fabricated to liposome, and the defect of the method is to store
The easy breakage of journey liposome causes tea polyphenols to be revealed, and easily becomes sepia.
CN101219123A (2008-7-16) discloses a kind of tea polyphenol pellet preparation, tea polyphenols weight in its pellet preparations
Amount percentage composition is 20-80%, and excipient weight percentage composition is 15-79%, and the percentage composition of binding agent is 1-5%.Can be according to
Requirement is prepared into slow release or enteric coated preparation.But the tea polyphenol preparation of the method preparation is apt to deteriorate, is difficult storage.
The content of the invention
An object of the present invention is to provide and a kind of can effectively make tea polyphenols and air exclusion, easily storage and not variable
Matter, the tea polyphenols that tea polyphenols can be discharged when in use parcel system.
The second object of the present invention is to provide and a kind of can effectively make tea polyphenols and air exclusion, easily storage and not variable
Matter, the tea polyphenols that tea polyphenols can be discharged when in use wrap up the preparation method of system.
The third object of the present invention is to provide and a kind of can effectively make tea polyphenols and air exclusion, easily storage and not variable
Matter, when in use can by tea polyphenols discharge comprising the tea polyphenols wrap up system product.
The present invention the first technical purpose technical scheme is that：
A kind of tea polyphenols wrap up system, and particle diameter is 70-1400 microns, include tea polyphenols kernel and parcel from inside to outside successively
Layer；The integument is successively wrapped up；
The integument includes filling oxidant layer and thin layer from inside to outside successively；
The filling oxidant layer includes corn starch, Microcrystalline Cellulose and mannitol；
The thin layer includes polylactic acid and polymethyl methacrylate；
The tea polyphenols parcel system includes following components by weight：Tea polyphenols 20-60 parts, corn starch 10-15 parts,
Mixture 1-5 parts of Microcrystalline Cellulose 10-15 part, mannitol 20-30 parts, polylactic acid and polymethyl methacrylate.
Tea polyphenols as kernel sandwich layer, in kernel sandwich layer outer wrapping filler, are then wrapped in filling oxidant layer by the present invention
Wrap up in the PLA of densification（Polylactic acid）And PMMA（Polymethyl methacrylate）, obtain final products；During preservation, can be every
Air, tea polyphenols stably can be wrapped in the inside absolutely, in atmosphere or not have after being added in all kinds of daily use chemicals, food
The leakage of tea polyphenols, enduringly keeps the activity of tea polyphenols；In use, specific filler material and thin-film material,
Tea polyphenols parcel system is smoothly crushed, discharge tea polyphenols.The time of more than three month, color are placed at normal temperatures can
Will not change.
Preferably, also including pigment 1-5 weight portions in the tea polyphenols parcel system.
Preferably, the polylactic acid and polymethyl methacrylate are according to mass ratio 1:1-4 mixing match.
Preferably, the integument number of plies is 3-100 layers；The tea polyphenols parcel system moisture is less than 10%,
Density is 0.3-1.0g/cm3, pH value is 4-6.
The tea polyphenols parcel system can be micro- for tea polyphenol powder, tea polyphenols edible tablet, tea-polyphenol capsules or tea polyphenols
Ball；Preferably tea polyphenol pellet.
The present invention the second technical purpose technical scheme is that：
A kind of tea polyphenols wrap up the preparation method of system, and which comprises the following steps successively：
（1）Dispensing：Tea polyphenols powder 20-60 parts, corn starch 10-15 parts, Microcrystalline Cellulose 10-15 are prepared by weight
Mixture 1-5 parts of part, mannitol 20-30 parts, polylactic acid and polymethyl methacrylate；
（2）It is prepared by kernel：The tea polyphenols powder is made using fluidized-bed process for the kernel of a diameter of 70-250 microns；
Inlet temperature 30-60 DEG C in fluid bed, 20-30 DEG C of leaving air temp；20-30 DEG C of feeding temperature, charging rate
10-50mL/min；
（3）It is prepared by filling oxidant layer：Filler is wrapped up the kernel using fluidized-bed process to be formed with filling oxidant layer
Particles B；
The filler includes the corn starch, Microcrystalline Cellulose and mannitol；
Inlet temperature 30-60 DEG C in fluid bed, 20-30 DEG C of leaving air temp；20-30 DEG C of feeding temperature, charging rate
10-50mL/min；
（4）It is prepared by thin layer：The mixture of the polylactic acid and polymethyl methacrylate is added to into 60-80 DEG C of second
In alcohol and 1-3 hours are placed, after being completely dissolved and to form mixed liquor, the mixed liquor is formed and is sprayed, using fluidized-bed process
The spraying parcel particles B that the mixed liquor is formed forms the final products with dense thin film layer；
Inlet temperature 30-60 DEG C in fluid bed, 20-30 DEG C of leaving air temp；20-30 DEG C of feeding temperature, charging rate
10-50mL/min。
The present invention using tea polyphenols as kernel sandwich layer, using specific fluidized-bed process successively in the outer multilamellar bag of kernel sandwich layer
Wrap up in the PLA of filler and densification（Polylactic acid）And PMMA（Polymethyl methacrylate）, wherein the composition of interior outer casing and containing
Amount and wrap up order particular importance, inventor through countless experiments, final choice filler as interior integument, PLA and
PMMA obtains final products as thin film outer casing；
Product is made during preservation, air can be completely cut off, tea polyphenols can be stably wrapped in the inside, in atmosphere
Or it is added in all kinds of daily use chemicals, food the leakage for not having tea polyphenols afterwards, enduringly keep the activity of tea polyphenols；Using
Cheng Zhong, specific filler material and thin-film material, enable tea polyphenols parcel system smoothly to crush, discharge tea polyphenols.Can
The time of more than three months is placed at normal temperatures, and color will not change.
Preferably, the mixture quality of the polylactic acid and polymethyl methacrylate with the mass ratio of the ethanol is
1:10-100。
Preferably, the polylactic acid and polymethyl methacrylate are according to mass ratio 1:1-4 mixing match.
Preferably, the step（3）Filler when prepared by filling oxidant layer also includes pigment 1-5 weight portions.
It is highly preferred that Mannitol of the filler also including 0.5-0.9 weight portions, Lactose, hydroxypropyl methyl cellulose
With one or more in polyvinylpyrrolidone.
Preferably, the step（3）Filling oxidant layer adds 0.5-0.8 part anion powder when preparing；The anion powder
It is made up of by mass parts following components：Gull rock 15-20 parts；Tourmaline 5-10 parts；Opal 30-35 parts；Serpentine 2-6 parts；
Maifanitum 4-6 parts；Rare ice stone 4-6 parts；Hokutolite 1-2 parts；Doctor king stone 5-7 part；Shell 1-3 parts；Kieselguhr 12-18 parts；Oxidation
Zirconium 5-8 parts；Zirconium phosphate 4-6 parts.
The anion powder of the present invention has good electronegative ion, for again further can improve in spherical system its
Completely cut off air during preservation and enduringly keep active, smoothly broken in use and discharge tea polyphenols.
It is highly preferred that the preparation of the anion powder is by the gull rock, tourmaline, opal, serpentine, wheat meal
Stone, rare ice stone, hokutolite, Doctor king stone, shell, kieselguhr, zirconium oxide and zirconium phosphate mix homogeneously, superfine grinding is to grain diameter
For 15-30nm, sieve, microwave treatment, microwave frequency are 500～650MHz, and microwave treatment time is 1～3min.
Anion powder is processed using the method, the protection that can be improved its electronegative ion and tea polyphenols are wrapped up with system is made
With.
The present invention the 3rd technical purpose technical scheme is that：
A kind of product that system is wrapped up comprising the tea polyphenols, the product are cosmetics, toothpaste, beverage or medicine.
In sum, the invention has the advantages that：
1st, during tea polyphenols inclusion enclave of the invention ties up to preservation, air can be completely cut off, enduringly keeps tea polyphenols
Activity.
2nd, in use, specific filler material and thin-film material, enable tea polyphenols parcel system smoothly to break
It is broken, discharge tea polyphenols.
Description of the drawings
Fig. 1 is a kind of structural representation that tea polyphenols of the present invention wrap up system.
Specific embodiment
The present invention is described in further detail below in conjunction with accompanying drawing.
Embodiment one
As shown in figure 1, tea polyphenols parcel architecture is tea polyphenol pellet, from inside to outside including tea polyphenols kernel 1, filling
Oxidant layer 2 and PLA/PMMA thin layers 3.Particle diameter is 70-200 microns, includes tea polyphenols kernel and integument from inside to outside successively；Bag
Covering layer is successively wrapped up；Integument includes filling oxidant layer and thin layer from inside to outside successively；Filling oxidant layer include corn starch,
Microcrystalline Cellulose and mannitol；Thin layer includes polylactic acid and polymethyl methacrylate；
The tea polyphenols parcel system integument number of plies is 3-20 layers, and less than 10%, density is 0.3-0.5g/ to moisture
cm3, pH value is 4-6.
It is prepared by tea polyphenol pellet：
Dispensing：20 parts of tea polyphenols powder, 10 parts of corn starch, 10 parts of Microcrystalline Cellulose, mannitol are prepared by weight
30 parts, 5 parts of the mixture of polylactic acid and polymethyl methacrylate；Polylactic acid and polymethyl methacrylate are according to mass ratio 1:
4 mixing match；
It is prepared by kernel：Tea polyphenols powder is made using fluidized-bed process for the kernel of a diameter of 70-250 microns；
30 DEG C of inlet temperature in fluid bed, 20 DEG C of leaving air temp；20 DEG C of feeding temperature, charging rate 10mL/min；
It is prepared by filling oxidant layer：Filler is wrapped up by kernel using fluidized-bed process and forms the particles B with filling oxidant layer；Fill out
Filling agent includes corn starch, Microcrystalline Cellulose and the mannitol of above-mentioned counterweight；30 DEG C of inlet temperature in fluid bed, goes out pathogenic wind-warm
20 DEG C of degree；20 DEG C of feeding temperature, charging rate 10mL/min；
It is prepared by thin layer：The mixture of polylactic acid and polymethyl methacrylate is added in 60 DEG C of ethanol and is placed
1 hour, after being completely dissolved and to form mixed liquor, mixed liquor is formed and is sprayed, spray mixed liquor formed using fluidized-bed process
Mist parcel particles B forms the final products with dense thin film layer；30 DEG C of inlet temperature in fluid bed, 20 DEG C of leaving air temp；
20 DEG C of feeding temperature, charging rate 10mL/min.
By commercially available tea polyphenol powder, commercially available tea polyphenols edible tablet, commercially available tea-polyphenol capsules, and tea is more prepared by the method
Phenol micropill is respectively placed in toothpaste（Or in any other cosmetics series）, place more than 6 months time under room temperature.Can be obvious
See, except the tea polyphenol pellet prepared by the method does not have any change, other products all have changed into sepia.
Illustrate that the method can stably be wrapped in tea polyphenols inside micropill, all kinds of daily use chemicals, food, tooth can be added to
In cream, beverage or medicine, the leakage of tea polyphenols is not had, can enduringly keep the activity of tea polyphenols.
Embodiment two
As shown in figure 1, tea polyphenols parcel architecture is tea polyphenol pellet, from inside to outside including tea polyphenols kernel 1, filling
Oxidant layer 2 and PLA/PMMA thin layers 3.Particle diameter is 201-800 microns, includes tea polyphenols kernel and integument from inside to outside successively；
Integument is successively wrapped up；Integument includes filling oxidant layer and thin layer from inside to outside successively；Filling oxidant layer includes that Semen Maydiss form sediment
Powder, Microcrystalline Cellulose and mannitol；Thin layer includes polylactic acid and polymethyl methacrylate；
The tea polyphenols parcel system integument number of plies is 20-60 layers；Moisture is less than 10%, and density is 0.6-0.8g/
cm3, pH value is 4-6.
It is prepared by tea polyphenol pellet：
Dispensing：60 parts of tea polyphenols powder, 15 parts of corn starch, 15 parts of Microcrystalline Cellulose, mannitol are prepared by weight
20 parts, 1 part of the mixture of polylactic acid and polymethyl methacrylate；Polylactic acid and polymethyl methacrylate are according to mass ratio 1:
1 mixing match；
It is prepared by kernel：Tea polyphenols powder is made using fluidized-bed process for the kernel of a diameter of 70-250 microns；For example may be used
Using with mannitol as crystal seed.
60 DEG C of inlet temperature in fluid bed, 30 DEG C of leaving air temp；30 DEG C of feeding temperature, charging rate 50mL/min；
It is prepared by filling oxidant layer：Filler is wrapped up by kernel using fluidized-bed process and forms the particles B with filling oxidant layer；Fill out
Filling agent includes corn starch, Microcrystalline Cellulose and mannitol；60 DEG C of inlet temperature in fluid bed, 30 DEG C of leaving air temp；Enter
30 DEG C of material temperature degree, charging rate 50mL/min；
It is prepared by thin layer：The mixture of polylactic acid and polymethyl methacrylate is added in 60-80 DEG C of ethanol simultaneously
1-3 hours are placed, after being completely dissolved and to form mixed liquor, mixed liquor is formed and is sprayed, using fluidized-bed process by mixed liquor shape
Into spraying parcel particles B formed with dense thin film layer final products；60 DEG C of inlet temperature in fluid bed, leaving air temp
30℃；30 DEG C of feeding temperature, charging rate 50mL/min.
More than 5 months time can be placed under this method product room temperature.
Embodiment three
As shown in figure 1, tea polyphenols parcel architecture is tea polyphenol pellet, from inside to outside including tea polyphenols kernel 1, filling
Oxidant layer 2 and PLA/PMMA thin layers 3.Particle diameter is 801-1400 microns, includes tea polyphenols kernel and integument from inside to outside successively；
Integument is successively wrapped up；Integument includes filling oxidant layer and thin layer from inside to outside successively；Filling oxidant layer includes that Semen Maydiss form sediment
Powder, Microcrystalline Cellulose and mannitol；Thin layer includes polylactic acid and polymethyl methacrylate；
The tea polyphenols parcel system integument number of plies is 61-100 layers；Moisture is less than 10%, and density is 0.9-1.0g/
cm3, pH value is 4-6.
It is prepared by tea polyphenol pellet：
Dispensing：30 parts of tea polyphenols powder, 12 parts of corn starch, 12 parts of Microcrystalline Cellulose, mannitol are prepared by weight
25 parts, 3 parts of the mixture of polylactic acid and polymethyl methacrylate；Polylactic acid and polymethyl methacrylate are according to mass ratio 1:
3 mixing match；
It is prepared by kernel：Tea polyphenols powder is made using fluidized-bed process for the kernel of a diameter of 70-250 microns；
40 DEG C of inlet temperature in fluid bed, 25 DEG C of leaving air temp；25 DEG C of feeding temperature, charging rate 30mL/min；
It is prepared by filling oxidant layer：Filler is wrapped up by kernel using fluidized-bed process and forms the particles B with filling oxidant layer；Fill out
Filling agent includes corn starch, Microcrystalline Cellulose and mannitol；30 DEG C of inlet temperature in fluid bed, 20 DEG C of leaving air temp；Enter
20 DEG C of material temperature degree, charging rate 10mL/min；
It is prepared by thin layer：The mixture of polylactic acid and polymethyl methacrylate is added in 70 DEG C of ethanol and is placed
2 hours, after being completely dissolved and to form mixed liquor, mixed liquor is formed and is sprayed, spray mixed liquor formed using fluidized-bed process
Mist parcel particles B forms the final products with dense thin film layer；60 DEG C of inlet temperature in fluid bed, 30 DEG C of leaving air temp；
30 DEG C of feeding temperature, charging rate 50mL/min.
More than 4 months time can be placed under this method product room temperature.
Example IV
The mixture quality of polylactic acid and polymethyl methacrylate when prepared by thin layer is 1 with the mass ratio of ethanol:
10。
Mannitol of the filler also including 0.5 weight portion；Filling oxidant layer adds 0.8 part of anion powder when preparing；Anion
The preparation method of powder is by 20 parts of gull rock；10 parts of tourmaline；35 parts of opal；6 parts of serpentine；6 parts of Maifanitum；Rare ice stone 6
Part；2 parts of hokutolite；7 parts of Doctor king stone；3 parts of shell；18 parts of kieselguhr；8 parts of zirconium oxide；4 parts of mix homogeneously of zirconium phosphate, micropowder
It is 30nm to be broken to grain diameter, is sieved, and microwave treatment, microwave frequency are 650MHz, and microwave treatment time is 3min.
More than 7 months time can be placed under this method product room temperature.
Embodiment five
The mixture quality of polylactic acid and polymethyl methacrylate when prepared by thin layer is 1 with the mass ratio of ethanol:
100。
Lactose of the filler also including 0.9 weight portion；Filling oxidant layer adds 0.5 part of anion powder when preparing；Anion powder
Preparation method be by 18 parts of gull rock；8 parts of tourmaline；32 parts of opal；4 parts of serpentine；5 parts of Maifanitum；5 parts of rare ice stone；
1.2 parts of hokutolite；6 parts of Doctor king stone；2 parts of shell；16 parts of kieselguhr；7 parts of zirconium oxide；5 parts of mix homogeneously of zirconium phosphate, superfine grinding
It is 20nm to grain diameter, sieves, microwave treatment, microwave frequency is 550MHz, and microwave treatment time is 2min.
Embodiment six
The mixture quality of polylactic acid and polymethyl methacrylate when prepared by thin layer is 1 with the mass ratio of ethanol:
80。
Filler also includes the polyvinylpyrrolidone of the hydroxypropyl methyl cellulose and 0.4 weight portion of 0.4 weight portion；Fill out
Fill when prepared by oxidant layer and add 0.6 part of anion powder；The preparation method of anion powder is by 15 parts of gull rock；5 parts of tourmaline；Albumen
30 parts of stone；2 parts of serpentine；4 parts of Maifanitum；4 parts of rare ice stone；1 part of hokutolite；5 parts of Doctor king stone；1 part of shell；12 parts of kieselguhr；
5 parts of zirconium oxide；6 parts of mix homogeneously of zirconium phosphate, superfine grinding to grain diameter are 15nm, are sieved, microwave treatment, and microwave frequency is
500MHz, microwave treatment time are 1min.
Comparative example one
With embodiment one, except for the difference that dispensing prepares 70 parts of tea polyphenols powder by weight, and 8 parts of corn starch, crystallite are fine
6 parts of the mixture of 10 parts of dimension element, 18 parts of mannitol, polylactic acid and polymethyl methacrylate.
Comparative example two
With embodiment two, except for the difference that thin layer preparation：The mixture of polylactic acid and polymethyl methacrylate is added
To in 50 DEG C of ethanol and place 4 hours.70 DEG C of inlet temperature in fluid bed, 40 DEG C of leaving air temp；10 DEG C of feeding temperature,
Charging rate 60mL/min.
Comparative example three
With embodiment three, it is that tea polyphenols powder is made a diameter of 50 using fluidized-bed process is micro- that except for the difference that prepared by kernel
The kernel of rice.When prepared by inner nuclear layer, 20 DEG C of the inlet temperature in fluid bed, 10 DEG C of leaving air temp；40 DEG C of feeding temperature, charging
Speed 8mL/min；When prepared by filling oxidant layer, 80 DEG C of the inlet temperature in fluid bed, 50 DEG C of leaving air temp；40 DEG C of feeding temperature,
Charging rate 80mL/min.
1 embodiment of table and comparative example's properties of product evaluating and test experience
This specific embodiment is only explanation of the invention, and which is not limitation of the present invention, people in the art
Member can make the modification for not having creative contribution after this specification is read as needed to the present embodiment, but as long as at this
All protected by Patent Law in the right of invention.
Claims (5)
1. a kind of tea polyphenols wrap up system, it is characterised in that：Particle diameter is 70-1400 microns, includes tea polyphenols from inside to outside successively
Kernel and integument；The integument is successively wrapped up；
The integument is from inside to outside successively comprising filling oxidant layer and thin layer；
The filling oxidant layer includes corn starch, Microcrystalline Cellulose and mannitol；
The thin layer includes polylactic acid and polymethyl methacrylate；
The tea polyphenols parcel system includes following components by weight：Tea polyphenols 20-60 parts, corn starch 10-15 parts, crystallite
Mixture 1-5 parts of cellulose 10-15 parts, mannitol 20-30 parts, polylactic acid and polymethyl methacrylate；
The integument number of plies is 3-100 layers；The tea polyphenols parcel system moisture is less than 10%, and density is 0.3-
1.0g/cm3, pH value is 4-6；
Tea polyphenols wrap up the preparation method of system, it is characterised in that comprise the following steps successively：
(1) dispensing：By weight prepare tea polyphenols powder 20-60 parts, corn starch 10-15 parts, Microcrystalline Cellulose 10-15 part,
Mixture 1-5 parts of mannitol 20-30 parts, polylactic acid and polymethyl methacrylate；
(2) prepared by kernel：The tea polyphenols powder is made using fluidized-bed process for the kernel of a diameter of 70-250 microns；
Inlet temperature 30-60 DEG C in fluid bed, 20-30 DEG C of leaving air temp；20-30 DEG C of feeding temperature, charging rate 10-
50mL/min；
(3) fill oxidant layer to prepare：Filler is wrapped up by the kernel using fluidized-bed process and forms the microgranule with filling oxidant layer
B；
The filler includes the corn starch, Microcrystalline Cellulose and mannitol；
Inlet temperature 30-60 DEG C in fluid bed, 20-30 DEG C of leaving air temp；20-30 DEG C of feeding temperature, charging rate 10-
50mL/min；
The step（3）Filling oxidant layer adds 0.5-0.8 part anion powder when preparing；The anion powder presses matter by following components
Amount part composition：Gull rock 15-20 parts；Tourmaline 5-10 parts；Opal 30-35 parts；Serpentine 2-6 parts；Maifanitum 4-6 parts；Very
BINGSHI 4-6 part；Hokutolite 1-2 parts；Doctor king stone 5-7 part；Shell 1-3 parts；Kieselguhr 12-18 parts；Zirconium oxide 5-8 parts；Zirconium phosphate
4-6 parts；
The preparation of the anion powder is by the gull rock, tourmaline, opal, serpentine, Maifanitum, rare ice stone, Peitou
Stone, Doctor king stone, shell, kieselguhr, zirconium oxide and zirconium phosphate mix homogeneously, superfine grinding to grain diameter be 15-30nm, mistake
Sieve, microwave treatment, microwave frequency are 500～650MHz, and microwave treatment time is 1～3min；
(4) prepared by thin layer：The mixture of the polylactic acid and polymethyl methacrylate is added in 60-80 DEG C of ethanol
And 1-3 hours are placed, after being completely dissolved and to form mixed liquor, the mixed liquor is formed and is sprayed, using fluidized-bed process by institute
The spraying parcel particles B for stating mixed liquor formation forms the final products with dense thin film layer；
Inlet temperature 30-60 DEG C in fluid bed, 20-30 DEG C of leaving air temp；20-30 DEG C of feeding temperature, charging rate 10-
50mL/min。
2. a kind of tea polyphenols according to claim 1 wrap up system, it is characterised in that：In the tea polyphenols parcel system also
Including pigment 1-5 weight portions.
3. a kind of tea polyphenols according to claim 2 wrap up system, it is characterised in that：The polylactic acid and polymethyl
The mixture quality of sour methyl ester is 1 with the mass ratio of the ethanol:10-100.
4. a kind of tea polyphenols according to claim 3 wrap up system, it is characterised in that：The polylactic acid and polymethyl
Sour methyl ester is according to mass ratio 1:1-4 mixing match.
5. a kind of tea polyphenols according to claim 4 wrap up system, it is characterised in that：The filler also includes 0.5-
One or more in the Mannitol of 0.9 weight portion, Lactose, hydroxypropyl methyl cellulose and polyvinylpyrrolidone.
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| CN106176376B (en) * | 2016-08-04 | 2020-01-07 | 广州悦创实业有限公司 | Microspheres wrapping tea extract complex and application of microspheres in natural edible toothpaste |
| CN106867110A (en) * | 2017-03-13 | 2017-06-20 | 浙江醒缘生物科技有限公司 | A kind of air conditioning exhausting grid for producing anion |
| CN109820747A (en) * | 2019-03-22 | 2019-05-31 | 广州品域美妆创新科技有限公司 | Particle and its preparation process containing anthocyanidin |
| CN110755309A (en) * | 2019-11-08 | 2020-02-07 | 苏州克劳丽化妆品有限公司 | Cordyceps militaris essence particles, cordyceps militaris toothpaste and preparation methods of cordyceps militaris essence particles and cordyceps militaris toothpaste |
| CN113413323B (en) * | 2021-04-23 | 2023-07-28 | 广州摩亚方舟贸易有限公司 | Peach-leaf phenol microcapsule and preparation method thereof |
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| CN101219123A (en) * | 2007-12-27 | 2008-07-16 | 天津市弗兰德医药科技发展有限公司 | Tea polyphenol pellet and method for preparing the same |
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| US20080213441A1 (en) * | 2006-12-27 | 2008-09-04 | Cathy Jean Ludwig | Reduction of Astringency in Polyphenol Compositions |
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