CN104447371B - Hat monosodium glutamate monoammonium glutamate selenium and preparation method thereof - Google Patents
Hat monosodium glutamate monoammonium glutamate selenium and preparation method thereof Download PDFInfo
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- CN104447371B CN104447371B CN201410625927.4A CN201410625927A CN104447371B CN 104447371 B CN104447371 B CN 104447371B CN 201410625927 A CN201410625927 A CN 201410625927A CN 104447371 B CN104447371 B CN 104447371B
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- selenium
- glutamate
- monoammonium
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- monosodium glutamate
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Abstract
The present invention relates to a kind of new material hat monosodium glutamate monoammonium glutamate selenium and preparation method thereof, comprise the following steps: glutamic acid, ammonium carbonate and selenium oxide are put into reaction vessel by (1), solid state reaction occurs after grinding；(2), after fully reacting, product is put into baking oven, heated at constant temperature product；(3) after being cooled to room temperature, it is thus achieved that product monoammonium glutamate selenium.The hat monosodium glutamate monoammonium glutamate selenium of the present invention is prepared from by glutamic acid, ammonium carbonate and selenium oxide.Owing to glutamic acid is the main component that monosodium glutamate sodium glutamate plays a role, the hat monosodium glutamate monoammonium glutamate selenium of the present invention can act also as being preced with monosodium glutamate, is used in foodstuff flavouring and increases fresh and additive agent field.In addition, the monoammonium glutamate selenium of the present invention also has benefit selenium establishing-Yang and anti-aging effect, in preparation prevents and treats hepatopathy, stupor disease, impotence, cancer, hypertension, coronary heart disease, myocarditis, Keshan disease and the food of Kaschin-Beck disease and health products, can be widely used.
Description
Technical field
The present invention relates to biochemical industry medicine food field, especially relate to a kind of novel substance hat monosodium glutamate glutamic acid
Ammonium selenium and preparation method thereof.
Background technology
Monosodium glutamate (sodium glutamate, NaC5H8NO4), it is that Japanese aginomoto company in 1909 finds and applies for specially
Profit, containing sodium 13.60%, containing glutamic acid 86.40%, wherein, glutamic acid (C5H9NO4) it is the source of monosodium glutamate.Paddy
Propylhomoserin of many uses, itself, as medicine, can treat hepatic coma disease, it is also possible to produces monosodium glutamate, food
Product additive, spices and for biochemical research.
Selenium Se is people, the necessary nutrient of animal, and as nourishing additive agent, Organic Selenium human body easily absorbs.
The elderly takes in a certain amount of selenium, can be anti-aging.In for, young man, selenium element is favorably improved
Sperm motility.The toxin expelling additionally, selenium element also gives protection against cancer, prevents cardiovascular disease, maintains heart normal operation.
Anti-oxidant, improve immunologic function.To anti-curing cancers, hypertension, coronary heart disease, myocarditis, Keshan disease, big
Joint is sick, has good effect.Therefore World Health Organization's suggestion supplements 200 microgram selenium every day, can
Effectively prevention of various diseases is occurred frequently.The United States Medicine academy of sciences is thought, the minimum dosis toxica of selenium is every day 900
Microgram, if the content of the selenium taken in from diet and selenium product every day is safe less than 400 micrograms.
The flavouring of Selenium Supplement element simultaneously is not had, Now Domestic outer market crown monosodium glutamate paddy ammonia outside Now Domestic
Acid ammonium selenium does not the most occur.
Summary of the invention
It is an object of the invention to fill up the blank of prior art, it is provided that a kind of conjunction being preced with monosodium glutamate monoammonium glutamate selenium
One-tenth method.
The present invention is achieved by the following technical solutions:
A kind of preparation method being preced with monosodium glutamate monoammonium glutamate selenium, comprises the following steps:
(1) glutamic acid, ammonium carbonate and selenium oxide are put into reaction vessel, solid state reaction occurs after grinding；
(2) after fully reacting, product being put into baking oven, heated at constant temperature product is to being completely dried；
(3) after being cooled to room temperature, it is thus achieved that product hat monosodium glutamate monoammonium glutamate selenium.
Further, described step (1) puts into the mol ratio of glutamic acid, ammonium carbonate and selenium oxide is 2004:1000:
1。
Further, the reaction vessel of described step (1) is agitating ball mill.
Further, the chemical reaction of described step (1) is carried out at normal temperatures.
Further, the reaction time of the chemical reaction of described step (1) is 30 minutes.
Further, the heating-up temperature of the chemical reaction of described step (2) is 102 DEG C.
Further, the preparation method of described hat monosodium glutamate monoammonium glutamate selenium also includes step (3): terminate reaction
Product packing, packaging obtain finished product.
Compared with prior art, the invention have the advantages that
The hat monosodium glutamate monoammonium glutamate selenium that the present invention prepares, has another name called selenium-rich hat monosodium glutamate, chemical constitution molecular formula
Se(NH4)2000(C5H8NO4)2004, white crystalline powder, molecular weight 328987.4, containing selenium 0.02%, containing ammonium
10.96%, containing glutamic acid 89.01%, purity is (medicine food level) more than 99%, is dissolved in water.
The hat monosodium glutamate monoammonium glutamate selenium of the present invention is prepared from by glutamic acid, ammonium carbonate and selenium oxide.Due to paddy
Propylhomoserin is the main component that monosodium glutamate sodium glutamate plays a role, and the hat monosodium glutamate monoammonium glutamate selenium of the present invention also can be made
For hat monosodium glutamate, containing glutamic acid 89.01%, common monosodium glutamate contains glutamic acid 86.46%, and delicate flavour is stronger.It is used in food
Product seasoning increases fresh and additive agent field.Additionally, the hat monosodium glutamate monoammonium glutamate selenium of the present invention also has benefit selenium establishing-Yang
With anti-aging effect, preparation prevent and treat hepatopathy, stupor disease, impotence, cancer, hypertension, coronary heart disease,
In the food of myocarditis, Keshan disease and Kaschin-Beck disease and health products, can be widely used..
Accompanying drawing explanation
Fig. 1 is the flow chart of the preparation method of the hat monosodium glutamate monoammonium glutamate selenium of the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing, the preferred embodiments of the present invention are illustrated.The purpose of these embodiments is simply said
Bright property, and should not be construed as limitation of the present invention.
The present embodiment is the preparation method of hat monosodium glutamate monoammonium glutamate selenium, comprises the following steps:
(1) glutamic acid 294848.5g, ammonium carbonate 96064g, selenium oxide 110.96g are weighed, by above-mentioned material
Mixing, puts into agitating ball mill and carries out solid state reaction, and start is reacted half an hour, and reaction generates glutamic acid
Ammonium selenium, chemical equation is: 2004C5H9NO4+1000(NH4)2CO3+SeO2=
Se(NH4)2000(C5H8NO4)2004+1000CO2↑+1002H2O, reaction condition is normal temperature；
(2), after fully reacting 30 minutes, from agitating ball mill, product is released；
(3) product being put into baking oven, constant temperature 102 DEG C adds hot product, to being completely dried；
(4) it is cooled to room temperature, it is thus achieved that product hat monosodium glutamate monoammonium glutamate selenium is weighed, and obtains monoammonium glutamate selenium
328987.4g, then packed products.
The hat monosodium glutamate monoammonium glutamate selenium of the present invention is prepared from by glutamic acid, ammonium carbonate and selenium oxide.Due to paddy
Propylhomoserin is the main component that monosodium glutamate sodium glutamate plays a role, and the hat monosodium glutamate monoammonium glutamate selenium of the present invention also can be made
For hat monosodium glutamate, it is used in foodstuff flavouring and increases fresh and additive agent field.Additionally, the hat monosodium glutamate monoammonium glutamate of the present invention
Selenium also has benefit selenium establishing-Yang and anti-aging effect, preparation prevent and treat hepatopathy, stupor disease, impotence, cancer,
In the food of hypertension, coronary heart disease, myocarditis, Keshan disease and Kaschin-Beck disease and health products, can obtain wide
General application.
These are only the preferred embodiments of the present invention, be not limited to the present invention, for this area
For technical staff, all made within the spirit and principles in the present invention any amendment, equivalent, change
Enter, should be included within the scope of the present invention.
Claims (7)
1. it is preced with a preparation method for monosodium glutamate monoammonium glutamate selenium, comprises the following steps:
(1) glutamic acid, ammonium carbonate and selenium oxide are put into reaction vessel, solid state reaction occurs after grinding；
(2), after fully reacting, product is put into baking oven, heated at constant temperature product；
(3) after being cooled to room temperature, it is thus achieved that product hat monosodium glutamate monoammonium glutamate selenium.
The preparation method of hat monosodium glutamate monoammonium glutamate selenium the most according to claim 1, it is characterised in that: described step
Suddenly (1) puts into the mol ratio of glutamic acid, ammonium carbonate and selenium oxide is 2004:1000:1.
The preparation method of hat monosodium glutamate monoammonium glutamate selenium the most according to claim 1, it is characterised in that: described step
Suddenly the reaction vessel of (1) is agitating ball mill.
The preparation method of hat monosodium glutamate monoammonium glutamate selenium the most according to claim 1, it is characterised in that: described step
Suddenly the chemical reaction of (1) is carried out at normal temperatures.
The preparation method of hat monosodium glutamate monoammonium glutamate selenium the most according to claim 1, it is characterised in that: described step
Suddenly the reaction time of the chemical reaction of (1) is 30 minutes.
The preparation method of hat monosodium glutamate monoammonium glutamate selenium the most according to claim 1, it is characterised in that: described step
Suddenly the heating-up temperature of the chemical reaction of (2) is 102 DEG C.
The preparation method of hat monosodium glutamate monoammonium glutamate selenium the most according to claim 1, it is characterised in that: further,
The preparation method of described monoammonium glutamate selenium also includes step (4): the product terminating reaction dispenses, packaging
Obtain finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410625927.4A CN104447371B (en) | 2014-11-07 | 2014-11-07 | Hat monosodium glutamate monoammonium glutamate selenium and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410625927.4A CN104447371B (en) | 2014-11-07 | 2014-11-07 | Hat monosodium glutamate monoammonium glutamate selenium and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104447371A CN104447371A (en) | 2015-03-25 |
| CN104447371B true CN104447371B (en) | 2016-08-24 |
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ID=52894206
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410625927.4A Expired - Fee Related CN104447371B (en) | 2014-11-07 | 2014-11-07 | Hat monosodium glutamate monoammonium glutamate selenium and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN104447371B (en) |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1135305A (en) * | 1996-02-05 | 1996-11-13 | 胡礼平 | Selenium-added gourmet powder |
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2014
- 2014-11-07 CN CN201410625927.4A patent/CN104447371B/en not_active Expired - Fee Related
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| Publication number | Publication date |
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| CN104447371A (en) | 2015-03-25 |
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| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160824 Termination date: 20171107 |