CN104432490A - Sweetsop extractive preparation method and application of sweetsop extractive in cigarettes - Google Patents
Sweetsop extractive preparation method and application of sweetsop extractive in cigarettes Download PDFInfo
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- CN104432490A CN104432490A CN201410667945.9A CN201410667945A CN104432490A CN 104432490 A CN104432490 A CN 104432490A CN 201410667945 A CN201410667945 A CN 201410667945A CN 104432490 A CN104432490 A CN 104432490A
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- manaca
- filter
- extract
- cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a sweetsop extractive preparation method. The method comprises the steps that sweetsops are peeled, smashed and beaten into pulp, 85wt% to 95wt% ethanol water with the weight which is four times that of the sweetsops is added into the sweetsops, heating and backflowing are carried out for 2 h, immediate filtration is carried out, filter residues are used in the next step, and filter liquor is retained; 30wt% ethanol water with the weight which is five times that of the filter residues is added into the filter residues, heating and backflowing are carried out for 2 h, immediate filtration is carried out, and then the filter liquor is decompressed and concentrated to obtain concentrate A; the concentrate A and the original filter liquor are mixed to be placed at 0 DEG C to be filtered in a standing mode, and the filter liquor is decompressed and concentrated to obtain faint yellow liquor which is the sweetsop extractive. The preparation method is simple and practical, and is easy to operate and implement; the obtained sweetsop extractive can be sprayed on cut tobaccos of cigarettes, and the cigarettes are obtained in a coiled mode, so that the cigarette remaining taste is effectively improved, the sweet taste of the cigarettes is improved, smoke gas is fine and smooth, and the aroma concentration of the cigarettes is improved.
Description
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of preparation method of manaca extract, the invention still further relates to the application of described manaca extract in cigarette simultaneously.
Background technology
Along with developing rapidly of science and technology and improving constantly of health of people consciousness, various natural product joins in cigarette by increasing tobacco enterprise, thus reaches the effect that safety non-toxic improves cigarette quality and mouthfeel harmfully.
Manaca, also known as Sakyamuni, be a kind of tropical fruit (tree), fruit is fresh and sweet, and the snow-white mouthfeel of pulp is careful, and the micro-acid of the fragrant and sweet point of band again, local flavor is excellent.Every 100 grams of manaca pulp contain: moisture is 8.36 grams, soluble solid is 18.0wt% ~ 26.0wt%, and fat is 0.14wt% ~ 0.3wt%, and mineral matter is 0.6wt% ~ 0.7wt%, carbohydrate is 23.9wt%, calcium is 0.2wt%, and phosphorus is 0.04wt%, and iron is 1.0wt%, organic acid is 0.42wt%, total reducing sugar is 15.3wt% ~ 18.3wt%, and vitamin C is 0.265 gram, and protein is 1.55 grams.Manaca contains abundant vitamin C, has hypoglycemic effect, is also best anti-oxidant fruit, can effective delaying skin aging, skin whitening; Manaca fiber content is higher, effectively can promote enterocinesia.Manaca extract effectively can resist 12 kinds of malignant cells simultaneously.
Research for manaca mainly concentrates on the active anticancer aspect of Annona lactone now, and its extract is used for tobacco business, and there is not been reported.Be that development of raw materials develops new high-grade cigarette additive with manaca, the suction quality of cigarette can be improved, expand its application in cigarette, wide market prospects will be had.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of manaca extract and the application in cigarette.
The present invention also aims to described manaca extract joins in the pipe tobacco of production process, can effectively improve cigarette pleasant impression, improves cigarette sweet moisture feeling, makes flue gas fine and smooth, increases cigarette flavor concentration.
Object of the present invention is achieved by the following technical programs.
Except as otherwise noted, percentage of the present invention is percetage by weight.
A first aspect of the present invention relates to a kind of preparation method of manaca extract, and it comprises the following steps:
(1) manaca after clean peeling is broken into pulpous state;
(2) in manaca slurry, add 85wt% ~ 95wt% ethanol water of its weight 4 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, filter residue is used for next step, and filtrate retains for subsequent use;
(3) in the filter residue in step (2), add the 30wt% ethanol water of its weight 5 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, it is 1.200 ± 0.006g/cm that gained filtrate is evaporated to density at 40 ± 2 DEG C
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, gained weak yellow liquid is cigarette manaca extract.
In the preferred embodiment of a first aspect of the present invention, in step (3), the filter residue in step (2) is repeatedly leached with the 30wt% ethanol water of its weight 5 times amount, and be heated to 90 ± 2 DEG C of backflow 2h, then filter while hot, at 40 ± 2 DEG C, being evaporated to density after the filtrate at every turn obtained being merged is 1.200 ± 0.006g/cm
3, obtain concentrate A.Step (4) is afterwards still identical.
A second aspect of the present invention relates to the manaca extract prepared by the preparation method of manaca extract described in above-mentioned first aspect.
A third aspect of the present invention relates to the purposes of manaca extract in cigarette according to second aspect.This manaca extract can be applicable to production of cigarettes, does not need to change cigarette original processing technology during application, can directly be added in cigarette shreds by manaca extract.Concrete grammar is: after manaca extract is diluted 4 times of weight with the amount ultra-pure water of cigarette shreds weight 0.3wt%, be sprayed onto on cigarette shreds, prepare cigarette in existing mode in the mode of spraying.
A fourth aspect of the present invention relates to the pipe tobacco comprising described manaca extract.This pipe tobacco can be used for preparation tradition and lights type cigarette or prepare electric heating type cigarette.
The cigarette and the blank cigarette that add manaca extract carry out sensory evaluating smoking, and smoking result shows, manaca extract of the present invention can improve cigarette pleasant impression, improve cigarette sweet moisture feeling, make flue gas fine and smooth, improve cigarette flavor concentration.
Accompanying drawing explanation
Nothing
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, but embodiment is not limited to the technical solution.
Embodiment 1
(1) accurately take the manaca after 2kg peeling, put in juice extractor fragmentation of pulling an oar and obtain manaca slurry.
(2) soaked with the 85wt% ethanol water of its weight 4 times amount by manaca slurry, reflux 2h at temperature 90 DEG C, filters while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(3) the 30wt% ethanol water adding its weight 5 times amount to the filter residue in step (2) leaches, be heated to 90 ± 2 DEG C of backflow 2h, after filtering while hot, repeat this leaching-Jia hot reflux-filtration step several times while hot to filter residue, at 40 ± 2 DEG C, being evaporated to density after merging the filtrate at every turn obtained is 1.200 ± 0.006g/cm
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 398g, be cigarette manaca extract.
Embodiment 2
(1) accurately take the manaca after 2kg peeling, put in juice extractor fragmentation of pulling an oar and obtain manaca slurry.
(2) soaked with the 95wt% ethanol water of its weight 4 times amount by manaca slurry, reflux 2h at temperature 90 DEG C, filters while hot, and filter residue is used for next step, and filtrate is for subsequent use.
(3) the 30wt% ethanol water of its weight 5 times amount is added to the filter residue in step (2), be heated to 90 ± 2 DEG C of backflow 2h, after filtering while hot, repeat this leaching-Jia hot reflux-filtration step several times while hot to filter residue, at 40 ± 2 DEG C, being evaporated to density after merging the filtrate at every turn obtained is 1.200 ± 0.006g/cm
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, obtain weak yellow liquid 411g, be cigarette manaca extract.
Manaca extract in above-described embodiment is used for cloud and mist tobacco leaf formulation, manaca extract is got by the 0.3wt% of cigarette shreds weight, dilute with the ultra-pure water of 4 times of weight, then be sprayed onto on cigarette shreds in the mode of spraying, balance 48h under constant temperature (22 ± 1 DEG C) constant humidity (relative humidity 60 ± 2wt%), roll into Cigarette.The cigarette of gained and blank cigarette transfer to specialty member of smoking carry out sense organ contrast smoke panel test, result is as follows:
Above content is the further description made the present invention in conjunction with concrete preferred embodiment.For general technical staff of the technical field of the invention, the obvious modification made without departing from the inventive concept of the premise, performance or purposes identical, all should be considered as protection scope of the present invention.
Claims (5)
1. a preparation method for manaca extract, is characterized in that comprising the following steps:
(1) manaca after clean peeling is broken into pulpous state;
(2) in manaca slurry, add 85wt% ~ 95wt% ethanol water of its weight 4 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, filter residue is used for next step, and filtrate retains for subsequent use;
(3) in the filter residue in step (2), add the 30wt% ethanol water of its weight 5 times amount, be heated to 90 ± 2 DEG C of backflow 2h, filter while hot, it is 1.200 ± 0.006g/cm that gained filtrate is evaporated to density at 40 ± 2 DEG C
3, obtain concentrate A;
(4) step (3) gained concentrate A is mixed with step (2) gained filtrate be placed on 0 DEG C at leave standstill after 36h and filter, it is 0.920 ± 0.006g/cm that filtrate is evaporated to density at 40 DEG C
3, gained weak yellow liquid is cigarette manaca extract.
2. the preparation method of manaca extract according to claim 1, it is characterized in that in step (3), the filter residue in step (2) repeatedly being leached with the 30wt% ethanol water of its weight 5 times amount, and filter while hot after being all heated to 90 ± 2 DEG C of backflow 2h, at 40 ± 2 DEG C, being evaporated to density after the filtrate at every turn obtained being merged is 1.200 ± 0.006g/cm. at every turn
3, obtain concentrate A.
3. the manaca extract prepared of the preparation method of manaca extract according to claim 1.
4. the purposes of manaca extract according to claim 1 in cigarette, is characterized in that manaca extract to dilute with the amount ultra-pure water relative to cigarette shreds weight 0.3wt%, is then sprayed onto on cigarette shreds in the mode of spraying.
5. comprise the pipe tobacco of the manaca extract described in claim 1 or 2.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410667945.9A CN104432490B (en) | 2014-11-20 | 2014-11-20 | A kind of manaca extract and the application in cigarette |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410667945.9A CN104432490B (en) | 2014-11-20 | 2014-11-20 | A kind of manaca extract and the application in cigarette |
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| Publication Number | Publication Date |
|---|---|
| CN104432490A true CN104432490A (en) | 2015-03-25 |
| CN104432490B CN104432490B (en) | 2016-03-09 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410667945.9A Active CN104432490B (en) | 2014-11-20 | 2014-11-20 | A kind of manaca extract and the application in cigarette |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107201274A (en) * | 2017-06-13 | 2017-09-26 | 武汉黄鹤楼香精香料有限公司 | Method and the application of tobacco aromaticss are extracted by raw material of tamarind |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101155920A (en) * | 2005-02-28 | 2008-04-02 | 奈良先端科学技术大学院大学 | Reducing levels of nicotinic alkaloids in plants |
| CN101575324A (en) * | 2009-05-15 | 2009-11-11 | 贵州正鑫药业有限公司 | Preparation method for extracting anticancer valid-position medicine SHIKEMOXIN from sweetsop |
| CN102754784A (en) * | 2012-08-08 | 2012-10-31 | 天宁香料（江苏）有限公司 | Method for preparing tamarind fruit extract and application of same in edible essence |
-
2014
- 2014-11-20 CN CN201410667945.9A patent/CN104432490B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101155920A (en) * | 2005-02-28 | 2008-04-02 | 奈良先端科学技术大学院大学 | Reducing levels of nicotinic alkaloids in plants |
| CN101575324A (en) * | 2009-05-15 | 2009-11-11 | 贵州正鑫药业有限公司 | Preparation method for extracting anticancer valid-position medicine SHIKEMOXIN from sweetsop |
| CN102754784A (en) * | 2012-08-08 | 2012-10-31 | 天宁香料（江苏）有限公司 | Method for preparing tamarind fruit extract and application of same in edible essence |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107201274A (en) * | 2017-06-13 | 2017-09-26 | 武汉黄鹤楼香精香料有限公司 | Method and the application of tobacco aromaticss are extracted by raw material of tamarind |
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| Publication number | Publication date |
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| CN104432490B (en) | 2016-03-09 |
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