CN1044293A - Method for extracting horseradish oil - Google Patents
Method for extracting horseradish oil Download PDFInfo
- Publication number
- CN1044293A CN1044293A CN 89105008 CN89105008A CN1044293A CN 1044293 A CN1044293 A CN 1044293A CN 89105008 CN89105008 CN 89105008 CN 89105008 A CN89105008 A CN 89105008A CN 1044293 A CN1044293 A CN 1044293A
- Authority
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- China
- Prior art keywords
- horseradish
- raw material
- distillation
- oil
- water
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000000034 method Methods 0.000 title claims abstract description 30
- 239000010655 horseradish oil Substances 0.000 title claims description 19
- 240000003291 Armoracia rusticana Species 0.000 claims abstract description 40
- 235000011330 Armoracia rusticana Nutrition 0.000 claims abstract description 38
- 239000002994 raw material Substances 0.000 claims abstract description 31
- 238000004821 distillation Methods 0.000 claims description 28
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000003921 oil Substances 0.000 claims description 11
- 238000010298 pulverizing process Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 5
- 238000010521 absorption reaction Methods 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 3
- 239000000796 flavoring agent Substances 0.000 abstract description 4
- 235000019634 flavors Nutrition 0.000 abstract description 4
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 238000003672 processing method Methods 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 239000000741 silica gel Substances 0.000 description 5
- 229910002027 silica gel Inorganic materials 0.000 description 5
- 239000000284 extract Substances 0.000 description 4
- 238000007670 refining Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 241000390128 Eutrema Species 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000002808 molecular sieve Substances 0.000 description 2
- 235000011837 pasties Nutrition 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 241001293164 Eutrema japonicum Species 0.000 description 1
- 241001529246 Platymiscium Species 0.000 description 1
- 235000000760 Wasabia japonica Nutrition 0.000 description 1
- ZOJBYZNEUISWFT-UHFFFAOYSA-N allyl isothiocyanate Chemical compound C=CCN=C=S ZOJBYZNEUISWFT-UHFFFAOYSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000012264 purified product Substances 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
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- Fats And Perfumes (AREA)
Abstract
A kind of processing method of extracting its oil content from the plant horseradish mainly is to adopt control certain temperature and pressure to distill.Use method of the present invention the oil content of horseradish more than 90% can be extracted, include the various aromatoising substances of horseradish simultaneously in the oil, keep the natural sweet-smelling of horseradish.The processing horseradish method ratio that this method processing horseradish adopts together at present, less manpower, province's energy consumption, yield height, horseradish is natural flavour mountaineous dense when edible.Simultaneously, the horseradish residue can be used as feed or other deep processing raw material again.
Description
The present invention is a kind of by the production method of extracting its oil content in the plant roots and stems, exactly is by extracting horse radish oil in horseradish (Wasabia) rhizome.
Horseradish (Wasabia) belongs to the wasabi platymiscium, is a kind of natural flavouring.At present except that bright horseradish be directly used in edible, the processing of also smoking dry plate and pulvis.But technology and the method for extracting horse radish oil from horseradish still report few.
The invention provides a kind of processing method of from horseradish, extracting horse radish oil.Use this method and can be effectively the oil content of horseradish be proposed, the raw material of capable of using as feed again and other the further deep processing of the horseradish residue after using simultaneously.
Technical process of the present invention such as Fig. 1 comprise: the cleaning of 1 raw material, 2 raw material pulverizing, 3 single flashs, 4 second distillations, 5 several main parts such as refining.Specifically raw material cleans and carries out in rinse bath or similar containers.Fresh horseradish raw material is sent in the pulverizer after cleaning.Raw material becomes the mashed prod of 15～30 order fineness after crushed, as being raw material with the horseradish dry plate, directly raw material being dropped into pulverizer and wear into 15～30 purpose powder.In crushing process, a grain fineness of raw material is too small, and oil yield can not increase when surpassing 30 orders, but the course of processing produces a large amount of foams, makes the post-treatment operation become unfavorable.It is comparatively suitable when therefore the raw material after pulverizer is pulverized becomes 15～30 order fineness.Pulverizing back raw material adds water by a certain percentage and stirs well.The amount that adds water in the raw material and be for the ease of distillation, water does not influence the extraction of horse radish oil, but the water excess distillation time is long, and it is also uneconomical that energy consumption is big, the very few increase of the water yield repeats the distillatory number of times.Therefore, use fresh horseradish as raw material in raw material: water is 1: 2 ratio, promptly adds the water of 2 times of amounts in the raw material; Use dried horseradish sheet to be raw material, in raw material: water is 1: 6 ratio, promptly adds water by 6 times of heavy amounts of raw material.Raw material adds water and stirs back one-tenth pasty state.The raw material of pasty state is delivered in the still kettle and is distilled.Distillation comprises single flash and two processes of second distillation, and single distilled still kettle can be combined into by one or several still kettles, and single distilled temperature remains on 100～120 ℃, and distillation time is no less than 10 minutes, is generally 20～60 minutes.The cut that comes out through single flash enters the second distillation still and carries out second distillation, and second distillation keeps and the single flash uniform temp, and promptly 100～120 ℃, distillation time can be shorter than single flash, finishes in 20～40 minutes.Once, second distillation can be under normal pressure or gauge pressure be 1 and carry out below the normal atmosphere.The product that distills out is the thick horse radish oil that contains small amount of moisture.Thick horse radish oil enters separator and makes with extra care, and treating process can be used (1) absorption method or (2) distillation method.
(1) absorption method: add silica gel or other in the separator and remove moisture in the thick horse radish oil as molecular sieve dehydration agent etc.Silica gel behind the absorption moisture or molecular sieve can dewater, and regeneration is back to be reused.
(2) distillation method: the separator of distillation method is made of still kettle.Use steam heated still, keep 100～105 ℃ of still temperature, distillation time is 10～30 minutes, and distillation is carried out under normal pressure.
The horse radish oil that utilizes the present invention to extract, major ingredient are redskin and part isomer, contain the part fragrant substance simultaneously.Therefore, adopt this production method, make not only that oil content extracts in the horseradish, and extract in the oil content and contain the contained fragrant matter of horseradish, make the horse radish oil that is extracted keep the natural flavour mountaineous of natural horseradish.
Example 1, bright horseradish extract horse radish oil
Get bright horseradish, send into pulverizer and pulverize after cleaning (100 kilograms), add 200 kg of water in the crushing process, the fineness after the pulverizing is greater than 15 orders.
Horseradish mashed prod through pulverizing drops in the single flash still and distills.105 ℃ of distillation temperatures were distilled 30 minutes, and gauge pressure is 0.5 normal atmosphere in the still kettle.Overhead product is collected overhead product through the water-cooled cooling system in the still kettle.
Collecting overhead product through single flash enters the second distillation still and carries out second distillation.115 ℃ of distillation temperatures, distillation time is no less than 20 minutes, and gauge pressure 0.4 normal atmosphere in the still kettle distills out cut and collects product through the water cooling system cooling.
The thick horse radish oil that second distillation is collected enters separator and makes with extra care.When adopting silica gel adsorption refining, add silica gel in the separator, stir several minutes after, static 10 minutes with horse radish oil isolate purified product, after silica gel absorbs moisture, recycle after the drying regeneration.
Per 100 kilograms of raw materials can get oily 0.18 kilogram.Oil-containing is 0.2% in the bright horseradish.The yield of oil is 90%.
Example 2, horseradish dry plate extract horse radish oil
With being ground into the following powder of 20 orders in 100 kilograms of horseradish dry plates input pulverizers, add 600 kilograms of stirrings of water and obtain mashed prod.
Carry out single flash, second distillation and refining by example 1 described condition and process, obtain 0.8 kilogram of refining horse radish oil.The oleaginousness of dried horseradish is 1%.Adopting the inventive method, is 80% with dried horseradish for the stock oil extraction yield.
Utilize horseradish (bright, dry product), adopt method of the present invention effectively its oil content to be extracted, and keep the natural flavor of natural horseradish. This method is produced horse radish oil and is processed into the horseradish dry plate than horseradish, saves manpower (60%), fuel (40%) and packing charge (80%). And edible horse radish oil is also convenient, natural flavour mountaineous dense than horseradish and horseradish dry plate. Simultaneously this production method is extracted the later horseradish residue of oil content and be can be used as again feed or other deep processing raw material.
Claims (4)
1, a kind of method, this method of extracting its oil content from the plant horseradish is:
(1) with raw material pulverizing;
(2) raw material after the pulverizing distills, and comprises single flash, two processes of second distillation, and distillation temperature is 100～120 ℃, and distillation is carried out below the normal atmosphere at normal pressure or 1 of gauge pressure;
(3) distillation after product make with extra care the product horse radish oil.
2, in accordance with the method for claim 1, it is characterized in that raw material powder is broken into a grain of 15～30 order fineness.
3, according to claim 1,2 described methods, drop into a certain proportion of water in the raw material after it is characterized in that pulverizing, to bright horseradish is raw material in raw material: the ratio of water=1: 2 is a raw material in raw material to dried horseradish: stir after the ratio of water=1: 6 adds entry.
4, in accordance with the method for claim 1, it is characterized in that treating process can carry out with (1) absorption method, (2) distillation method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 89105008 CN1021578C (en) | 1989-01-19 | 1989-01-19 | Horseradish Oil Extraction Method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 89105008 CN1021578C (en) | 1989-01-19 | 1989-01-19 | Horseradish Oil Extraction Method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1044293A true CN1044293A (en) | 1990-08-01 |
| CN1021578C CN1021578C (en) | 1993-07-14 |
Family
ID=4855780
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 89105008 Expired - Fee Related CN1021578C (en) | 1989-01-19 | 1989-01-19 | Horseradish Oil Extraction Method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1021578C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093167C (en) * | 1997-06-09 | 2002-10-23 | 贵州省岑巩县精细化工厂 | Process for extracting essences from root of fir |
| CN102603406A (en) * | 2012-03-28 | 2012-07-25 | 常熟市南洋化肥有限公司 | Horseradish soil fertilizer composition for preventing and curing soil-borne disease |
| CN108130192A (en) * | 2018-02-28 | 2018-06-08 | 浙江舟山彩麟之食品有限公司 | A kind of method that high-purity mustard essential oil is extracted in the seed from mustard |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1313583C (en) * | 2005-01-17 | 2007-05-02 | 天津商学院 | Reclamation of horse radish oil by using macroporous adsorbent resin |
-
1989
- 1989-01-19 CN CN 89105008 patent/CN1021578C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1093167C (en) * | 1997-06-09 | 2002-10-23 | 贵州省岑巩县精细化工厂 | Process for extracting essences from root of fir |
| CN102603406A (en) * | 2012-03-28 | 2012-07-25 | 常熟市南洋化肥有限公司 | Horseradish soil fertilizer composition for preventing and curing soil-borne disease |
| CN108130192A (en) * | 2018-02-28 | 2018-06-08 | 浙江舟山彩麟之食品有限公司 | A kind of method that high-purity mustard essential oil is extracted in the seed from mustard |
| CN108130192B (en) * | 2018-02-28 | 2021-07-06 | 浙江舟山彩麟之食品有限公司 | Method for extracting high-purity mustard essential oil from mustard seeds |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1021578C (en) | 1993-07-14 |
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