CN104402391B - A kind of insulation roof slab - Google Patents

A kind of insulation roof slab Download PDF

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CN104402391B
CN104402391B CN201410579889.3A CN201410579889A CN104402391B CN 104402391 B CN104402391 B CN 104402391B CN 201410579889 A CN201410579889 A CN 201410579889A CN 104402391 B CN104402391 B CN 104402391B
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parts
glass fibre
still
mixed liquor
calcium
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CN104402391A (en
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孔蕾蕾
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Jiangsu Aifeite Environmental Protection Materials Co ltd
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Abstract

The invention discloses a kind of insulation roof slab, it is characterized in that: high-strength alpha-type Gypsum Fibrosum is 24 parts~27 parts, calcium-phosphate cement is 12 parts~14 parts, flyash is 30 parts~33 parts, and rosin soap foaming agent is 2.5 parts, and 107 glue are 0.25 part, glass fibre is 2.5 parts, and water is 22 parts~26 parts.Making step includes: (1) dispensing;(2) stirring;(3) compression atomizing, loads extrusion pump by mixed liquor, utilizes extrusion pump by mixed liquor compression atomizing;(4) injection, sprayed by air-flow after glass fibre being cut to certain length by cutting spraying machine, again with atomization mixed liquor spatial mixing and together with spray fall and on mould, form goods bottom and surface layer, make glass fibre and base material reach the most two-dimentional random distribution;(5) intubate;(6) vacuum dehydration;(7) tube drawing;(8) steam curing;(9) demoulding;(10) milling.The warming plate intensity that the present invention makes is high, and density is low.

Description

A kind of insulation roof slab
Technical field
The present invention relates to a kind of insulation roof slab, particularly to the manufacture method of above-mentioned insulation roof slab.
Background technology
Insulation roof slab be applicable to lightweight steel construction, frame structure, brick-and-concrete buildings add layer, light plate type All kinds of buildings such as fast-assembling house, high-rise steel structure.Insulation roof slab lateral rigidity is big, can make roof support by The rigid support of color steel sheet roofing changes flexible support into, thus reduces the steel using amount of support system.But it is existing The performances such as insulation roof slab intensity and insulation are difficult to reach pre-provisioning request, limit the applicable model of insulation roof slab Enclose.
Summary of the invention
The technical problem to be solved is to provide that a kind of heat-insulating property is more preferable, the higher heat insulation house surface of intensity Plate.
To this end, the weight proportion of the composition of raw materials of the insulation roof slab of present invention offer is that high-strength alpha-type Gypsum Fibrosum is 24 parts~27 parts, calcium-phosphate cement is 12 parts~14 parts, and flyash is 30 parts~33 parts, and rosin soap is sent out Infusion is 2.5 parts, and 107 glue are 0.25 part, and glass fibre is 2.5 parts, and water is 22 parts~26 parts.
Present invention also offers the manufacture method of above-mentioned insulation roof slab.
Comprise the following steps that:
(1) dispensing
(2) stirring
High-strength alpha-type Gypsum Fibrosum, calcium-phosphate cement, flyash, rosin soap foaming agent, 107 glue are added water stirring 4~ 6 minutes, stir speed (S.S.) was 60~110r/min;
(3) compression atomizing
Mixed liquor is loaded extrusion pump, utilizes extrusion pump by mixed liquor compression atomizing;
(4) injection
By cutting spraying machine glass fibre is cut to certain length after sprayed by air-flow, then with atomization mixed liquor Spatial mixing and together spray fall and on mould, form goods bottom and surface layer, make glass fibre and base material reach reason The two-dimentional random distribution thought;
(5) intubate
Automatically combination core pipe is penetrated die cavity by tube filling machine;
(6) vacuum dehydration
Roofing thermal-insulating board carries out vacuum dehydration after completing operations for forming;
(7) tube drawing
Watering is used to extract in automatically sandwich layer compound being poured into die cavity;
(8) steam curing
Still is closed behind the door, cold sky in applying vacuum pump evacuation or top gas method to eject still when roofing thermal-insulating board enters still Gas, slowly and equably heats up 1.5~2 hours, and in making still, pressure reaches 0.8MPa gauge pressure, temperature reach 125~ 130℃.Keep temperature 125~130 DEG C 6~8 hours, the most slowly and equably release steam cooling in still 1.5~2 hours, when in still steam pressure be down to its temperature of zero-pressure below 70 DEG C time, still door can be opened;
(9) demoulding
Through billet shift machine automatic demoulding after roofing thermal-insulating board hardening;
(10) milling
Use grinding machine that product surface is ground continuously, make product surface flatness and thickness error less than 1mm.
The warming plate intensity that the present invention makes is high, and density is low, and the technique used is easily controlled.
Detailed description of the invention
Make insulation roof slab with the following methods:
(1) dispensing
High-strength alpha-type Gypsum Fibrosum: 26 parts, calcium-phosphate cement: 13 parts, flyash: 31 parts, rosin soap foaming agent: 2.5 parts, 107 glue: 0.25 part, glass fibre: 2.5 parts, water: 24.75 parts.
Raw material effect is as follows:
High-strength alpha-type Gypsum Fibrosum: high-strength alpha-type Gypsum Fibrosum system semi-hydrated gypsum, has the strongest hydrating capacity, at it and water After mixing, first it is that high-strength alpha-type Gypsum Fibrosum dissolves the metastable saturated solution of formation, dihydrate gypsum in aqueous Quickly at saturated solution crystallize, the crystallize of dihydrate gypsum, destroy the original poised state of semi-hydrated gypsum, can promote It is made to dissolve further, until whole crystallizes are that dihydrate gypsum produces intensity.
Calcium-phosphate cement: the comprcssive strength of roof boarding is within the specific limits along with the increasing of calcium-phosphate cement percentage composition Add and improve, the impact on roof boarding comprcssive strength of table 1 calcium-phosphate cement.Calcium-phosphate cement is worked as under experiment condition When being 1:2 with plaster ratio, intensity reaches maximum.Then present along with the increase comprcssive strength of plaster ratio Downward trend, owing to the increase of Gypsum Fibrosum percentage composition within the specific limits is conducive to tricalcium phosphate hydrated cementitious to generate Hydroxyapatite, the rising of hydroxyapatite conversion ratio will cause the raising of its comprcssive strength;But when Gypsum Fibrosum excess Time, wrap phosphate the most too much, suppressed it to change to hydroxyapatite, thus cause roof boarding Comprcssive strength reduces.
The impact on roof boarding comprcssive strength of table 1 calcium-phosphate cement
High-strength alpha-type Gypsum Fibrosum incorporation Calcium-phosphate cement incorporation Comprcssive strength
24 parts 10 parts 19.8MPa
24 parts 11 parts 21.2MPa
24 parts 12 parts 22.8MPa
24 parts 13 parts 22.9MPa
24 parts 14 parts 23.0MPa
26 parts 11 parts 19.5MPa
26 parts 12 parts 21.8MPa
26 parts 13 parts 23.7MPa
26 parts 14 parts 23.8MPa
26 parts 15 parts 23.9MPa
Flyash: add flyash filler, plays a part deformation, increases intensity reduction cost, and flyash is The fine powder collected from the boiler smoke of burning coal powder power plant, how spherical in shape its granule is, smooth surface, Lycoperdon polymorphum Vitt and Lead.Its chemical composition is mainly SiO2、Fe2O3, CaO etc., the active SiO in flyash2With Ca (OH)2 Effect, generates the hydrated calcium silicate with the hydraulicity, thus improves goods hydrophobicity and intensity.
107 glue system water solublity and the high polymer of emulsion type or organosilicon, after adding in high strength gypsum Binder Materials Gel precipitation and breakdown of emulsion is there is not, to the hardening of gypsum plaster without destruction in gypsum solution medium. And the crosslinking of their own energy air hardening or cross-linked polymeric in acid medium, participating in Gypsum Fibrosum sclerous reaction process In, CaSO can be coated with4Crystal, forms good protective layer, carries out certainly in the interstitial channels between crystal simultaneously Exchange, blocks capillary channel, improves protection against the tide and the anti-condensation ability of gypsum plaster, the crosslinking of high polymer Cohesiveness makes the intensity of goods also increase.
Rosin soap foaming agent: rosin soap foaming agent is internally formed bubble in calcium phosphate cement, these small gas Bubble is wrapped up by calcium-phosphate cement, is evenly dispersed in calcium-phosphate cement slurry, forms stable foam calcium phosphate Cement mortar, foam calcium-phosphate cement is starched and is not only wrapped up gypsum particle, and the space between filler particles, formed and protect The temperature peculiar internal structure of composite light plate.
107 glue: 107 glue play reinforcing agent effect, 107 glue additions are the 0.5%~0.8% of Gypsum Fibrosum, add 107 Glue (polyvinyl formal resin) can significantly improve resistance to water and the intensity of goods, but dosage should be suitable, crosses and adds Enter and affect intensity on the contrary.
Glass fibre: roofing thermal-insulating board mixes glass fibre, can improve roofing thermal-insulating board bending resistance, cracking resistance and resist Impact flexibility performance, its character and consumption play decisive role for the mechanical property of wallboard.Table 2 is glass The fiber impact on roofing thermal-insulating board intensity, shows in table that roofing thermal-insulating board bending strength is affected relatively by glass fibre Greatly, relatively small on comprcssive strength impact, contrast volume is 2.5 parts and the mechanical index do not mixed, bending strength Improving 50%, comprcssive strength improves 13.2%.Roofing thermal-insulating board bending resistance when the incorporation of glass fibre is less Intensity increases with the increase of the incorporation of glass fibre, and when more than 2.5 parts, bending strength is not further added by, This is owing to the contact condition of gypsum plaster Yu glass fibre is caused.It addition, after glass fibre excess, Roof heat insulation sheet metal forming is relatively difficult.Considering, glass fibre volume is defined as 2.5 parts.
The impact on roofing thermal-insulating board intensity of table 2 glass fibre
Glass fibre incorporation Bending strength Comprcssive strength
Do not mix 5.6MPa 22.8MPa
0.5 part 6.8MPa 23.6MPa
1 part 7.3MPa 24.1MPa
1.5 part 7.8MPa 24.8MPa
2 parts 8.1MPa 25.3MPa
2.5 part 8.4MPa 25.5MPa
3 parts 8.5MPa 25.8MPa
(2) stirring
High-strength alpha-type Gypsum Fibrosum, calcium-phosphate cement, flyash, rosin soap foaming agent, 107 glue are added water stirring 4~ 6 minutes, stir speed (S.S.) was 60~110r/min.
(3) compression atomizing
Mixed liquor is loaded extrusion pump, utilizes extrusion pump by mixed liquor compression atomizing.
(4) injection
Sprayed by air-flow after glass fibre being cut to certain length by cutting spraying machine, then mix with atomization Liquid spatial mixing and together spray fall and on mould, form goods bottom and surface layer, make glass fibre reach with base material Preferably two dimension random distribution.
(5) intubate
Automatically combination core pipe is penetrated die cavity by tube filling machine.
(6) vacuum dehydration
Roofing thermal-insulating board carries out vacuum dehydration after completing operations for forming.
(7) tube drawing
Watering is used to extract in automatically sandwich layer compound being poured into die cavity.
(8) steam curing
Still is closed behind the door, cold sky in applying vacuum pump evacuation or top gas method to eject still when roofing thermal-insulating board enters still Gas, to ensure in still that pressure is pure steam or the pressure close to pure steam ensures roofing thermal-insulating board chemical reaction institute Need temperature.For preventing owing to thermal (temperature difference) stress causes warming plate crackle, slowly and equably heat up 1.5~2 hours, In making still, pressure reaches 0.8MPa gauge pressure, and temperature reaches 125~130 DEG C.Keep temperature 125~130 DEG C 6~8 Hour, it is ensured that compound carries out chemical reaction.The most slowly and equably release steam cooling 1.5~2 in still Hour, to prevent warming plate from too fast crack occurring because lowering the temperature.When in still, steam pressure is down to its temperature of zero-pressure and is existed When less than 70 DEG C, still door can be opened.
(9) demoulding
Through billet shift machine automatic demoulding after roofing thermal-insulating board hardening.
(10) milling
Use grinding machine that product surface is ground continuously, make product surface flatness and thickness error less than 1mm.
The warming plate intensity that the present invention makes is high, and density is low, and technique is easily controlled.
Testing roofing thermal-insulating board in embodiment, roofing thermal-insulating board physical property is as shown in table 3.Table shows Showing that roofing thermal-insulating board comprcssive strength is high, air shrinkage value is less, heat conductivility is good.
The physical property of table 3 roofing thermal-insulating board
Numbering Surface density (kg/m3) Comprcssive strength (MPa) Air shrinkage value (mm/m) Heat conductivity (W/ (m.k))
1 45 25.3 0.67 0.2578
2 44 25.0 0.69 0.2592
3 45 25.1 0.66 0.2586
4 43 24.9 0.70 0.2603
5 42 24.7 0.71 0.2614
6 46 25.5 0.65 0.2569

Claims (1)

1. an insulation roof slab, is characterized in that: high-strength alpha-type Gypsum Fibrosum is 24 parts~27 parts, calcium-phosphate cement Being 12 parts~14 parts, flyash is 30 parts~33 parts, and rosin soap foaming agent is 2.5 parts, and 107 glue are 0.25 Part, glass fibre is 2.5 parts, and water is 22 parts~26 parts;
Making step includes following:
(1) dispensing
(2) stirring
High-strength alpha-type Gypsum Fibrosum, calcium-phosphate cement, flyash, rosin soap foaming agent, 107 glue are added water and stir 4~6 Minute, stir speed (S.S.) is 60~110r/min;
(3) compression atomizing
Mixed liquor is loaded extrusion pump, utilizes extrusion pump by mixed liquor compression atomizing;
(4) injection
Sprayed by air-flow after glass fibre being cut to certain length by cutting spraying machine, then exist with atomization mixed liquor Spatial mixing together spray are fallen and are formed goods bottom and surface layer on mould, make glass fibre and base material reach preferable Two dimension random distribution;
(5) intubate
Automatically combination core pipe is penetrated die cavity by tube filling machine;
(6) vacuum dehydration
Roofing thermal-insulating board carries out vacuum dehydration after completing operations for forming;
(7) tube drawing
Watering is used to extract in automatically sandwich layer compound being poured into die cavity;
(8) steam curing
Still is closed behind the door, cold sky in applying vacuum pump evacuation or top gas method to eject still when roofing thermal-insulating board enters still Gas, slowly and equably heats up 1.5~2 hours, and in making still, pressure reaches 0.8MPa gauge pressure, temperature reach 125~ 130℃.Keep temperature 125~130 DEG C 6~8 hours, the most slowly and equably release in still steam cooling 1.5~ 2 hours, when in still steam pressure be down to its temperature of zero-pressure below 70 DEG C time, still door can be opened;
(9) demoulding
Through billet shift machine automatic demoulding after roofing thermal-insulating board hardening;
(10) milling
Use grinding machine that product surface is ground continuously, make product surface flatness and thickness error less than 1mm.
CN201410579889.3A 2014-10-15 2014-10-15 A kind of insulation roof slab Active CN104402391B (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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CN104402391B true CN104402391B (en) 2016-11-30

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2592273C1 (en) * 2015-07-20 2016-07-20 Юлия Алексеевна Щепочкина Crude mixture for producing construction material
CN108793913A (en) * 2018-07-17 2018-11-13 合肥万之景门窗有限公司 A kind of preparation method of inorganic heat preservation environment-friendly type energy-saving material

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2037760U (en) * 1988-10-08 1989-05-17 国家建筑材料工业局南京玻璃纤维研究设计院 Thermally-insulating roof board made of high-strength mineral wool
CN1093584C (en) * 1996-09-13 2002-10-30 朱恒杰 Inorganic thermal insulation sound-proof fire-proof foam material and its production method
CN2393931Y (en) * 1999-05-24 2000-08-30 樊志 Light building slab structure
CN1247177A (en) * 1999-09-21 2000-03-15 窦新艺 Components of light concrete wall
CN1322208C (en) * 2005-06-17 2007-06-20 林野 Construction thermal insulation energy-saving plate with polystyrene panel sandwiched steel wire mesh core

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C06 Publication
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C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20191128

Address after: 221000 No.9 Xingye Road, Lingang Industrial Park, Pizhou City, Xuzhou City, Jiangsu Province

Patentee after: Jiangsu Sanzhou Machinery Technology Co.,Ltd.

Address before: 325000 Zhejiang Province, Wenzhou city Lucheng District Station Avenue Lijing garden 17 building 804

Patentee before: Kong Leilei

TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20200511

Address after: 224300 No.50, Panlong Avenue, Panwan Town, Sheyang County, Yancheng City, Jiangsu Province

Patentee after: Jiangsu aifeite environmental protection materials Co.,Ltd.

Address before: 221000 No.9 Xingye Road, Lingang Industrial Park, Pizhou City, Xuzhou City, Jiangsu Province

Patentee before: Jiangsu Sanzhou Machinery Technology Co.,Ltd.

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A type of insulated roof panel

Granted publication date: 20161130

Pledgee: Bank of China Limited Sheyang Branch

Pledgor: Jiangsu aifeite environmental protection materials Co.,Ltd.

Registration number: Y2024980011475