CN104399261B - Prepare the equipment of concentrate - Google Patents

Prepare the equipment of concentrate Download PDF

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Publication number
CN104399261B
CN104399261B CN201410708604.1A CN201410708604A CN104399261B CN 104399261 B CN104399261 B CN 104399261B CN 201410708604 A CN201410708604 A CN 201410708604A CN 104399261 B CN104399261 B CN 104399261B
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China
Prior art keywords
unit
switch
pipeline
boiler
sampling
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Active
Application number
CN201410708604.1A
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Chinese (zh)
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CN104399261A (en
Inventor
丁杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Gaoyou Sina Chemical Machinery Equipment Co., Ltd.
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Heng Tian Bio Tech Ltd Huainan
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Priority to CN201510800437.8A priority Critical patent/CN105344118A/en
Priority to CN201510800092.6A priority patent/CN105396307A/en
Priority to CN201510796496.2A priority patent/CN105435474A/en
Priority to CN201510796569.8A priority patent/CN105289019A/en
Priority to CN201510794053.XA priority patent/CN105363226A/en
Priority to CN201410708604.1A priority patent/CN104399261B/en
Priority to CN201510796109.5A priority patent/CN105457319A/en
Priority to CN201510795785.0A priority patent/CN105396306A/en
Priority to CN201510799395.0A priority patent/CN105413203A/en
Priority to CN201510795711.7A priority patent/CN105396305A/en
Application filed by Heng Tian Bio Tech Ltd Huainan filed Critical Heng Tian Bio Tech Ltd Huainan
Priority to CN201510796688.3A priority patent/CN105435475A/en
Publication of CN104399261A publication Critical patent/CN104399261A/en
Priority to AU2015100476A priority patent/AU2015100476A4/en
Priority to AU2015100475A priority patent/AU2015100475A4/en
Priority to IES20150263A priority patent/IES86678B2/en
Priority to IE20150242A priority patent/IE86889B1/en
Priority to GB1520927.3A priority patent/GB2536756B/en
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Publication of CN104399261B publication Critical patent/CN104399261B/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10Vacuum distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D5/00Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
    • G01N1/2035Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N2001/1031Sampling from special places
    • G01N2001/105Sampling from special places from high-pressure reactors or lines
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
    • G01N1/2035Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
    • G01N2001/205Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping using a valve
    • G01N2001/2057Sample chamber in a valve/piston

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Commercial Cooking Devices (AREA)

Abstract

The present invention relates to concentrate preparation field, particular but not exclusively relate to a kind of equipment utilizing low pressure low boiling to prepare concentrate, it comprises boiler unit, stores stream unit, cooling unit, decompressing unit, it is characterized in that the sidewall of boiler unit is provided with sampling unit near bottom place, the upper cover of boiler unit is provided with condensing unit; The sampling cavity of sampling unit run through matrix above and below, equivalent pressure cavity penetrates from the front of matrix and runs through the front and back of sampling cavity; The closed barrel storing stream unit is communicated by the first pipeline, second pipe, the 3rd pipeline, the 4th pipeline and the external world; The output channel of boiler unit, outlet conduit, inlet channel respectively with store the second switch, the input of cooling unit, the output of cooling unit that flow unit and connect, the 3rd switch storing stream unit connects with the input of decompressing unit, and the first switch and the 4th switch that store stream unit connect with air.Concentrator disclosed by the invention has good reliability and thickening efficiency is high.

Description

Prepare the equipment of concentrate
Technical field
The present invention relates to concentrate preparation field, particular but not exclusively relate to a kind of equipment utilizing low pressure low boiling to prepare concentrate.
Background technology
The boiling point of water reduces along with the reduction of air pressure, therefore reducing pressure can make water seethe with excitement at relatively low temperatures, the water of boiling constantly makes liquid water transitions be hot water and steam, the water vapour of heat can be condensed into water smoke at cold and hot interface place, a large amount of water smoke pools water droplet, and a large amount of water droplets accumulates current.Above-mentioned principle can be utilized the moisture in mixed liquor, thus improve the concentration of mixed liquor.
Summary of the invention
The object of the invention is to solve the problem, and a kind of equipment utilizing low pressure low boiling to prepare concentrate is provided.
For this reason, the invention provides a kind of equipment preparing concentrate, it comprises boiler unit, stores stream unit, cooling unit, decompressing unit, boiler unit has airtight structure, its inner bottom part is provided with charging aperture, discharging opening and heating unit, it is characterized in that, the sidewall of boiler unit is provided with sampling unit near bottom place, and the upper cover of boiler unit is provided with condensing unit.
Particularly, the collection unit of condensing unit is positioned at the inside of upper cover, collection unit comprises the strip being close to crown in lid and converges bar, is close to the collector ring of lid inner peripheral surface, the opening of collector ring is towards the top of lid, collector ring and lid form chamber of confluxing, the end that strip converges bar extends to chamber of confluxing, and chamber of confluxing is in communication with the outside by output channel.Strip converges bar and is provided with the binding face corresponding to crown in lid, two sides perpendicular to binding face are symmetrically arranged with the first arc surface of phase concave, the end face being parallel to binding face is provided with the second arc surface of indent, spill proof edge is formed between first arc surface and the second arc surface, strip converges bar and is provided with the first inclined plane and the second inclined plane near top, first inclined plane and the second inclined plane angle are obtuse angle, second inclined plane more converges to strip that the top of bar is close more to tilt to binding face, more to converging, the top of bar is close more to tilt to binding face first inclined plane, second arc surface extends to the second inclined plane, first arc surface extends to the first inclined plane.The monolateral cross section of collector ring is " L " shape, and the base vertical of " L " is in the inner peripheral surface of upper cover, and the stile of " L " is parallel to the inner peripheral surface of upper cover.The cooling end of condensing unit is positioned at the outside of upper cover, cooling end comprises the annular wafer of multiple coaxial setting, annular wafer is arranged along the crown of lid, the axis of annular wafer and the axis coaxle of lid are arranged, the outer crown of lid is close in the bottom of annular wafer, apical ring is provided with inlet channel, and base ring is provided with outlet conduit.
Particularly, sampling unit comprises matrix, motion bar, spacer pin, sampling cavity, thieff hatch, axle sleeve, equivalent pressure cavity, sampling cavity run through matrix above and below, equivalent pressure cavity is column blind hole, and equivalent pressure cavity penetrates from the front of matrix and runs through the front and back of sampling cavity; Axle sleeve and equivalent pressure cavity interference fit, motion bar and axle sleeve closed are slidably matched, and spacer pin is anchored on motion bar, and front or the back side of spacer pin and sampling cavity coordinate, be provided with gas-permeable channels in matrix, the head and the tail two ends of gas-permeable channels are communicated with ambient atmosphere with equivalent pressure cavity respectively.
Particularly, store stream unit and comprise the cylindrical shell of sealing, the first pipeline, second pipe, the 3rd pipeline, the 4th pipeline, the first switch, second switch, the 3rd switch, the 4th switch and water level mark pipe, cylindrical shell is communicated by the first pipeline, second pipe, the 3rd pipeline, the 4th pipeline and the external world, and the first pipeline, second pipe, the 3rd pipeline, the 4th pipeline realize opening and closing respectively by the first switch, second switch, the 3rd switch, the 4th switch.
Advantageously, the connecting relation of each unit is: the output channel in the chamber of confluxing of boiler unit with store the second switch flowing unit and connect, the outlet conduit of the cooling end of boiler unit is connected with the input of cooling unit by switch, the inlet channel of the cooling end of boiler unit is connected with the output of cooling unit by switch, the 3rd switch storing stream unit is connected with the input of decompressing unit by pipeline, and the first switch and the 4th switch that store stream unit connect with air.
Again particularly, the inner spout of described output channel is near the top of the conflux bottom in chamber and the stile far below " L ", and the bottom of described inlet channel is fixedly connected with the top of lid, and the bottom of inlet channel is provided with multiple delivery port.
Again particularly, the top of described annular wafer reduces to the distance of the bottom surface of lid with the increase of diameter itself.
Advantageously, when described spacer pin coordinates with the front of sampling cavity, motion bar is in pull-out location, and thieff hatch is positioned at the outside of matrix; When spacer pin coordinates with the back side of sampling cavity, motion bar is in insertion position, and thieff hatch is positioned at the inside of sampling cavity.
Advantageously, described gas-permeable channels extends to the front of matrix, and the sampling cavity of sampling unit is positioned at boiler, and handle is positioned at outside boiler.
Advantageously, the first described pipeline is positioned at cylindrical shell and locates near bottom, the inner spout of second pipe is near the bottom of cylindrical shell but higher than the inner spout of the first pipeline, the inner spout of the 3rd pipeline and the inner spout of the 4th pipeline are near the top of cylindrical shell, and second switch and the 3rd switch are fixedly connected by coupling block and realize synchronization action.
Particularly, synchronization action is realized by following structure, there is the coupling block with switch knob respective profile, at its head and the tail two ends, respectively through hole is set, also through hole is set in the relevant position of switch knob simultaneously, between handle coupling block being arranged on two switches, by two circular shafts, handle and coupling block are connected, then by back-up ring, circular shaft, handle, coupling block three are fixed.
Beneficial effect
The stream second switch of unit and the 3rd switch of storing disclosed by the invention is fixedly connected by coupling block and realizes synchronization action, improve the reliability of equipment, following deficiency can be avoided: 1. when decompressing unit reduces pressure to boiler, need second switch and the 3rd switch open, if second switch is opened, and unlatching forgotten by the 3rd switch, still rests on closed condition, then decompressing unit cannot reduce pressure to boiler, causes decompressing unit to do work invalid; If the 3rd switch open, and second switch forgets unlatching, still rests on closed condition, then decompressing unit cannot reduce pressure to boiler, causes decompressing unit to do work invalid; 2. store stream unit when carrying out draining, second switch and the 3rd switch is needed to close, if the 3rd switch cuts out, and second switch forgets closedown, still rests on opening, then when unlatching the 4th switch, hydraulic pressure in cylindrical shell is entered second pipe by extraneous atmospheric pressure, and water enters boiler by second switch and the 5th switch, and the water of refluence is spilled in the concentrate prepared after being full of chamber of confluxing, cause concentrate concentration to reduce, concentrate unsuccessfully.
When sampling unit samples the solution in boiler, without the need to stopping concentration process, more not needing the upper cover opening boiler, by the thieff hatch of sampling unit, the solution in boiler being taken out, carry out the pressure at balancing activity bar two ends by gas-permeable channels, realize the non-resistance sampling of motion bar.
The multiple coaxial setting of boiler upper cover and in ladder the cooling end of the condensing unit that the annular wafer of dress is formed, add the contact surface of boiler upper cover and cooling fluid, improve the cooling effectiveness of cooling fluid.
Strip converges the first arc surface and second arc surface of bar setting, adds cold and hot interface, improves the condensation efficiency of vapours.
Strip converges the spill proof edge of bar setting by the surface tension effects of liquid, condensed drop is slipped to along the first arc surface and the second arc surface and confluxes in chamber, avoid condensed drop and directly drop onto in concentrate, cause thickening efficiency to reduce.
When the moment that second switch and the 3rd switch are unlocked, the water in pipeline will be pushed back in boiler, due to the cushioning effect in chamber of confluxing, water be rested on and confluxes in chamber, instead of directly enter in concentrate.
Accompanying drawing explanation
Reference accompanying drawing is in the explanation of the embodiment provided as non-limiting example below, and the present invention and superiority thereof will be better understood, and accompanying drawing is as follows:
Fig. 1 is the stereogram preparing concentrate equipment disclosed by the invention;
Fig. 2 is the stereogram of the boiler in Fig. 1;
Fig. 3 is the exploded perspective view of boiler in Fig. 2;
Fig. 4 is the stereogram after boiler in Fig. 3 removes upper cover;
Fig. 5 is the top view of the upper cover of boiler in Fig. 3;
Fig. 6 is the stereogram of the upper cover in Fig. 5;
Fig. 7 is the stereogram at another visual angle of upper cover in Fig. 5;
Fig. 8 is the exploded perspective view of the upper cover in Fig. 5;
Fig. 9 is the sectional view along A-A direction in Fig. 5;
Figure 10 is the sectional view along B-B direction in Fig. 5;
Figure 11 is the partial enlarged drawing at I place in Figure 12;
Figure 12 is the stereogram of the single strip convergence bar in Fig. 8;
Figure 13 is the partial enlarged drawing at II place in Figure 12;
Figure 14-18 is stereograms of the sampling unit in Fig. 3, and wherein motion bar is positioned at diverse location;
Figure 19 is the exploded perspective view of the sampling unit in Fig. 3;
Figure 20 is the fragmentary perspective cross sectional view of the sampling unit in Fig. 3;
Figure 21-23 is half sectional views of sampling unit, and wherein motion bar is positioned at diverse location;
Figure 24 is the fragmentary perspective cross sectional view storing stream unit in Fig. 1;
Figure 25 is the enlarged top portion isometric figure storing stream unit in Figure 24;
The exploded perspective view of the second switch in Figure 26 Figure 25 and the 3rd switch;
Description of reference numerals
1. boiler unit; 11. upper covers; 12. heating units; 13. sidewalls; 14. sampling units; 15. charging apertures; 16. discharging openings; 1101. lid; 1102. collector ring; 1103. strips converge bar; 1104. annular wafer; 1105. output channel; 1106. inlet channel; 1107. outlet conduit; 1108. admission line; 1109. delivery port; 1103a. binding face; 1103b. the first arc surface; 1103c. the second arc surface; 1103d. spill proof edge; 1103e. the second inclined plane; 1103f. the first inclined plane; 1103g. the 3rd inclined plane; 1401. matrix; 1402. spacer pin; 1403. motion bar; 1404. thieff hatch; 1405. sampling cavity; 1406. handle; 1407. axle sleeve; 1408. gas-permeable channels; 1409. equivalent pressure cavity; 2. store stream unit; 20. coupling blocks; 21. cylindrical shells; 22. the 4th switches; 23. the 3rd switches; 24. second switches; 25. first switches; 26. water level mark pipes; 27. the 4th pipelines; 28. the 3rd pipelines; 29. second pipes; 210. first pipelines; 201. circular shaft; 3. cooling unit; 4. decompressing unit.
Detailed description of the invention
In order to distinguish the inner spout of component and the outer mouth of pipe, port pipeline being positioned at container is called inner spout, and the port be positioned at by pipeline outside container is called the outer mouth of pipe.
As shown in Figure 1, the equipment preparing concentrate disclosed by the invention, it comprises boiler unit 1, store stream unit 2, cooling unit 3, decompressing unit 4, the output channel 1105 in the chamber of confluxing of boiler unit 1 with store the second switch 24 flowing unit 2 and connect, the outlet conduit 1107 of the cooling end of boiler unit 1 is connected by the input of switch with cooling unit 3, the inlet channel 1106 of the cooling end of boiler unit 1 is connected by the output of switch with cooling unit 3, the 3rd switch 23 storing stream unit 2 is connected by the input of pipeline with decompressing unit 4, the first switch 25 and the 4th switch 22 that store stream unit 2 connect with air.
As in Figure 2-4, the sidewall 13 of boiler unit 1 is provided with sampling unit 14 near bottom place, the upper cover 11 of boiler unit 1 is provided with condensing unit, and boiler unit 1 has airtight structure, and its inner bottom part is provided with charging aperture 15, discharging opening 16 and heating unit 12.
As Fig. 5, 6, 9, shown in 10, the cooling end of condensing unit is positioned at the outside of upper cover 11, cooling end comprises the annular wafer 1104 of multiple coaxial setting, annular wafer 1104 is arranged along the crown of lid 1101, the axis of annular wafer 1104 and the axis coaxle of lid 1101 are arranged, the outer crown of lid 1101 is close in the bottom of annular wafer 1104, the top of annular wafer 1104 reduces to the distance of the bottom surface of lid 1101 with the increase of diameter itself, apical ring is provided with inlet channel 1106, the bottom of inlet channel 1106 is fixedly connected with the top of lid 1101, the bottom of inlet channel 1106 is provided with multiple delivery port 1109, base ring is provided with outlet conduit 1107, water at low temperature flows to apical ring by inlet channel 1106, apical ring overflows after being full of water at low temperature to next ring, water at low temperature sequentially overflows each ring, finally discharge from the outlet conduit 1107 of base ring, obviously, the water temperature of apical ring is lower than the water temperature of base ring.
As Fig. 7, 8, 9, shown in 10, the collection unit of condensing unit is positioned at the inside of upper cover 11, collection unit comprises the strip being close to crown in lid 1101 and converges bar 1103, be close to the collector ring 1102 of lid 1101 inner peripheral surface, the opening of collector ring 1102 is towards the top of lid 1101, collector ring 1102 and lid 1101 form chamber of confluxing, the end that strip converges bar 1103 extends to chamber of confluxing, the monolateral cross section of collector ring 1102 is " L " shape, the base vertical of " L " is in the inner peripheral surface of upper cover 11, the stile of " L " is parallel to the inner peripheral surface of upper cover 11, chamber of confluxing is in communication with the outside by output channel 1105, the inner spout of output channel 1105 is near the top of the conflux bottom in chamber and the stile far below " L ".
As Figure 11, 12, shown in 13, strip converges bar 1103 and is provided with the binding face 1103a corresponding to crown in lid 1101, two sides perpendicular to binding face 1103a are symmetrically arranged with the first arc surface 1103b of phase concave, the end face being parallel to binding face 1103a is provided with the second arc surface 1103c of indent, spill proof edge 1103d is formed between first arc surface 1103b and the second arc surface 1103c, strip converges bar 1103 and is provided with the first inclined plane 1103f and the second inclined plane 1103e near top, first inclined plane 1103f and the second inclined plane 1103e angle are obtuse angle, second inclined plane 1103e more converges to strip that the top of bar 1103 is close more to tilt to binding face 1103a, more to converging, the top of bar is close more to tilt to binding face 1103a first inclined plane 1103f, second arc surface 1103c extends to the second inclined plane 1103e, first arc surface 1103b extends to the first inclined plane 1103f.Strip converges bar 1103 and is symmetrically arranged with the 3rd inclined plane 1103g near the first inclined plane 1103f end, strip is converged bar 1103 and is configured to a wedge angle near the first beveled end by the 3rd inclined plane 1103g, and multiple strip converges bar 1103 and matches with face the mode be close to by the 3rd inclined plane 1103g and evenly form a circle around wedge angle.
After the first arc surface 1103b that the strip that vapours in boiler encounters low temperature converges bar 1103 or the second arc surface 1103c, be condensed into drop, under the synergy of spill proof edge 1103d and Surface Tension of Liquid Drops, drop converges the first arc surface 1103b of bar 1103 or the second arc surface 1103c along strip and is slipped to and confluxes in chamber, discharges chamber of confluxing after the drop confluxed in chamber collects by output channel 1105.
As shown in Figure 19,20, sampling unit 14 comprises matrix 1401, motion bar 1403, spacer pin 1402, sampling cavity 1405, thieff hatch 1404, axle sleeve 1407, equivalent pressure cavity 1409.
As shown in figure 21, sampling cavity 1405 run through matrix 1401 above and below, equivalent pressure cavity 1409 is column blind hole, penetrates from the front of matrix 1401, runs through the two sides, front and back of sampling cavity 1405; Axle sleeve 1407 and equivalent pressure cavity 1409 interference fit, motion bar 1403 and axle sleeve 1407 closed are slidably matched, and spacer pin 1402 is anchored on motion bar 1403.
As shown in Figure 21,22, front or the back side of spacer pin 1402 and sampling cavity 1405 coordinate, and when spacer pin 1402 coordinates with the front of sampling cavity 1405, motion bar 1403 is in pull-out location, and thieff hatch 1404 is positioned at the outside of matrix 1401, with reference to Figure 16-17; When spacer pin 1402 coordinates with the back side of sampling cavity 1405, motion bar is in insertion position, and thieff hatch 1404 is positioned at the inside of sampling cavity 1405, with reference to Figure 14,15.
As shown in figure 20, gas-permeable channels 1408 is provided with in matrix 1401, the head and the tail two ends of gas-permeable channels 1408 are communicated with ambient atmosphere with equivalent pressure cavity 1409 respectively, gas-permeable channels 1408 extends to the front of matrix 1401, make the air pressure of equivalent pressure cavity 1409 consistent with ambient pressure by gas-permeable channels 1408, thus make motion bar 1403 activity more flexible, motion bar 1403 is provided with handle 1406 near matrix 1401 front, the diameter of handle 1406 is greater than the internal diameter of axle sleeve 1407, the sampling cavity 1405 of sampling unit 14 is positioned at boiler, and handle 1406 is positioned at outside boiler.
As Figure 24, shown in 25, store the cylindrical shell 21 that stream unit 2 comprises sealing, first pipeline 210, second pipe 29, 3rd pipeline 28, 4th pipeline 27, first switch 25, second switch 24, 3rd switch 23, 4th switch 22 and water level mark pipe 26, cylindrical shell 21 is by the first pipeline 210, second pipe 29, 3rd pipeline 28, 4th pipeline 27 and the external world communicate, first pipeline 210, second pipe 29, 3rd pipeline 28, 4th pipeline 27 is respectively by the first switch 25, second switch 24, 3rd switch 23, 4th switch 22 realizes opening and closing, first pipeline 210 is positioned at cylindrical shell 21 near bottom place, the inner spout of second pipe 29 is near the bottom of cylindrical shell 21 but higher than the inner spout of the first pipeline 210, the inner spout of the 3rd pipeline 28 and the inner spout of the 4th pipeline 27 are near the top of cylindrical shell 21.
As shown in figure 26, second switch 24 and the 3rd switch 23 synchronization action, both are realized by following structure by synchronization action, there is the coupling block 20 with switch knob respective profile, at its head and the tail two ends, respectively through hole is set, simultaneously also through hole is set in the relevant position of switch knob, between handle coupling block 20 being arranged on two switches, by two circular shafts 201, handle and coupling block 20 are connected, then by back-up ring, circular shaft 201, handle, coupling block 20 three are fixed.
The equipment preparing concentrate disclosed by the invention comprises decompression process, condensation process, stores and flow through journey, drainage procedure, sampling process.
Decompression process: close the first switch 25, the 4th switch 22 and the 6th switch, opens second switch 24, the 3rd switch 23, the 5th switch, the 7th switch, the 8th switch and the 9th switch.Open decompressing unit 4, make the gas in boiler enter decompressing unit 4 by the 5th switch, second switch 24, the 3rd switch 23, the 9th switch successively, from but air pressure in boiler reduce.
Condensation process: open cooling unit 3, the cooling fluid of cooling unit 3 is circulated by the 7th switch, apical ring, base ring and the 8th switch successively, makes the temperature of boiler top cover lower than the temperature of vapours in boiler by cooling fluid.
Open the heating unit 12 in boiler, the temperature of liquid to be concentrated in boiler is improved, because low pressure in boiler makes the boiling point of the moisture in solution to be concentrated also reduce, so make the water in solution to be concentrated seethe with excitement at a lower temperature, and then produce the water vapour of heat, the water vapour of heat is encountered the rear condensation of strip convergence bar 1103 of boiler upper cover 11 relative low temperature and is gathered into water droplet, under the synergy of spill proof edge 1103d and water drops surface tension force, water droplet converges the first arc surface 1103b of bar 1103 or the second arc surface 1103c along strip and is slipped to and confluxes in chamber, conflux to summarize in chamber and converge from strip the water that bar 1103 landing gets off.By condensation process, the moisture in the solution to be concentrated in boiler is constantly transferred to and confluxes in chamber, and then moisture in solution to be concentrated is reduced.
Store and flow through journey: after the water level confluxed in chamber exceedes the inner spout of output channel 1105, the water confluxed in chamber is discharged to by output channel 1105 and stores in stream unit 2, successively by the 5th switch, second switch 24, store to flow through in journey and there will be following three kinds of situations: 1. the air pressure in boiler is greater than the air pressure stored in stream unit 2,2. the air pressure in boiler equals to store the air pressure in stream unit 2, and the air pressure 3. in boiler is lower than the air pressure stored in stream unit 2.
During the situation 1 of being in, the water confluxed in chamber stores stream unit 2 from being pressed under the influence of air pressure; During the situation 2 of being in, because chamber of confluxing is higher than storing stream unit 2, so the water confluxed in chamber flows under gravity store stream unit 2; During the situation 3 of being in, open decompressing unit 4, the air pressure stored in stream unit 2 is reduced, and lower than the air pressure in boiler, makes situation 3 become situation 1 or 2; Store stream unit 2 by above three kinds of mode retainings.
Due to heating unit 12 continuous heating in boiler, so the temperature in boiler is higher than the temperature stored in stream unit 2, namely cause the air pressure in boiler higher than the air pressure stored in stream unit 2, therefore heating can impel the appearance of situation 1.
After the concentrate in boiler reaches predetermined concentration, heating unit 12 stops heating, air pressure in boiler declines, in order to avoid occurring that air pressure in boiler is lower than the air pressure stored in stream unit 2, decompressing unit 4 is needed to start, making to store air pressure in stream unit 2 lower than the air pressure in boiler by decompressing unit 4, entering to store stream unit 2 by remaining the condensed hydraulic pressure of water vapour in boiler.Because the water level confluxed in chamber is higher than output channel 1105 inner spout, so the water vapour in boiler can not directly enter store stream unit 2, thus reduce the harmful effect of water vapour to decompressing unit 4, inner spout due to second pipe 29 is positioned at the bottom place near cylindrical shell 21, and the inner spout of the 3rd pipeline 28 is near the top place of cylindrical shell 21, so when decompressing unit 4 works, avoid water and be immediately inhaled into the 3rd pipeline 28 after second pipe 29 is forced out, the top water that can reduce in cylindrical shell 21 that the inner spout of the 3rd pipeline 28 is arranged in cylindrical shell 21 enters the risk of the 3rd pipeline 28.
Drainage procedure: after the water level mark pipe 26 display water level stored in stream unit 2 reaches predetermined value, first close second switch 24, because second switch 24 and the 3rd switch 23 are by coupling block 20 synchronous interaction, so, while closing second switch 24, the 3rd switch 23 is also closed, after this, the water of condensation in boiler is by the chamber temporary reservoir that confluxes, after second switch 24 and the 3rd switch 23 are closed, store stream unit 2 to keep apart with boiler, open the 4th switch 22, make to store the air pressure flowed in unit 2 equal with extraneous atmospheric pressure, after air pressure balance, open the first switch 25, due to the effect of gravity, the water stored in stream unit 2 flows out from the first switch 25, realize the draining storing stream unit 2.After storing the water in stream unit 2 and be drained, first close the first switch 25 and the 4th switch 22, make to store stream unit 2 and isolated from atmosphere, open second switch 24 again, 3rd switch 23 is also unlocked simultaneously, due to store stream unit 2 in air pressure higher than the air pressure in boiler, so the moment that second switch 24 and the 3rd switch 23 are unlocked, water in pipeline will be pushed back in boiler, due to the cushioning effect in chamber of confluxing, water is rested on and confluxes in chamber, instead of directly enter in concentrate, after the air pressure stored in stream unit 2 and the air pressure balance in boiler, the condensed water of buffer memory in chamber that confluxes flows under gravity and stores stream unit 2, in order to maintain the environment under low pressure in boiler, need to open decompressing unit 4, the air pressure in boiler is made to maintain predetermined value, decompressing unit 4 open after can accelerate the water confluxed in chamber enter store stream unit 2.
Sampling process: with reference to Figure 21,22,23, sample by the concentrate in sampling unit 14 pairs of boilers in concentration process, and Concentration Testing is carried out to sampling.Before sampling, in order to improve accuracy in detection, first by handle 1406 quick rotation, as shown in figure 18, effect by centrifugal force makes the concentrate remained in thieff hatch 1404 be thrown out of, then by the direction signs on handle 1406, make thief hole upward, concentrate enters thieff hatch 1404, pull out motion bar 1403 afterwards to pull-out location, detect the concentrate in thieff hatch 1404 by detecting pen, or rotate motion bar 1403, make thieff hatch 1404 down, the concentrate in thieff hatch 1404 instills in vessel under gravity.After sampling, motion bar 1403 is pushed back to insertion position.
After concentrate in boiler reaches predetermined concentration, first close heating unit 12, decompressing unit 4, the 5th switch, open the 6th switch again, extraneous gas enters boiler internal by admission line 1108, makes the air pressure in boiler and ambient atmosphere pressure balanced, air pressure in boiler raises than time concentrated, the boiling point of the water in concentrate also increases, because heating unit 12 is closed, so the water in concentrate stops boiling, concentrate no longer loses moisture, and namely concentrate keeps existing concentration.Open discharging opening 16, the concentrate prepared is flowed out by discharging opening 16, after concentrate is drained, close discharging opening 16, open charging aperture 15, make liquid to be concentrated enter boiler by charging aperture 15, after liquid to be concentrated reaches scheduled volume, close charging aperture 15 and the 6th switch, boiler and ambient atmosphere are isolated, enters next concentration flow path.
Obviously, can solution to be concentrated be inputted at boiler or while exporting concentrate, the water stored in stream unit 2 be discharged.Detailed process is: first close the 9th switch, open the 6th switch, due to draught head, the water confluxed in chamber is pressed into and stores stream unit 2, until boiler, store stream both unit 2 in air pressure and atmospheric pressure balance after, the water confluxed in chamber flows under gravity and stores stream unit 2, opens the first switch 25 simultaneously, and the water stored in stream unit 2 is discharged.
Decompressing unit 4 is aspiration pump or vavuum pump.Cooling unit 3 is provided with input and output, cooling fluid enters cooling unit 3 from input, the heat of cooling fluid is dispersed in air by the fin by cooling unit 3, and then makes the temperature of cooling fluid of cooling unit 3 output lower than the temperature of the cooling fluid of input.

Claims (9)

1. prepare the equipment of concentrate for one kind, it comprises boiler unit (1), stores stream unit (2), cooling unit (3), decompressing unit (4), boiler unit (1) has airtight structure, its inner bottom part is provided with charging aperture (15), discharging opening (16) and heating unit (12), it is characterized in that
The sidewall (13) of boiler unit (1) is provided with sampling unit (14) near bottom place, and the upper cover (11) of boiler unit (1) is provided with condensing unit; The collection unit of condensing unit is positioned at the inside of upper cover (11), collection unit comprises the strip being close to lid (1101) interior crown and converges bar (1103), is close to the collector ring (1102) of lid (1101) inner peripheral surface, the opening of collector ring (1102) is towards the top of lid (1101), collector ring (1102) and lid (1101) form chamber of confluxing, the end that strip converges bar (1103) extends to chamber of confluxing, and chamber of confluxing is in communication with the outside by output channel (1105); The cooling end of condensing unit is positioned at the outside of upper cover (11), cooling end comprises the annular wafer (1104) of multiple coaxial setting, annular wafer (1104) is arranged along the crown of lid (1101), the axis of annular wafer (1104) and the axis coaxle of lid (1101) are arranged, the outer crown of lid (1101) is close in the bottom of annular wafer (1104), apical ring is provided with inlet channel (1106), and base ring is provided with outlet conduit (1107); Sampling unit (14) comprises matrix (1401), motion bar (1403), spacer pin (1402), sampling cavity (1405), thieff hatch (1404), axle sleeve I, shaft sleeve II, equivalent pressure cavity (1409), sampling cavity (1405) run through matrix (1401) above and below, equivalent pressure cavity (1409) is column blind hole, and equivalent pressure cavity (1409) penetrates from the front of matrix (1401) and runs through the front and back of sampling cavity (1405); Axle sleeve I and equivalent pressure cavity (1409) interference fit, motion bar (1403) is slidably matched with axle sleeve I and shaft sleeve II closed simultaneously, spacer pin (1402) is anchored on motion bar (1403), front or the back side of spacer pin (1402) and sampling cavity (1405) coordinate, be provided with gas-permeable channels (1408) in matrix (1401), the head and the tail two ends of gas-permeable channels (1408) are communicated with ambient atmosphere with equivalent pressure cavity (1409) respectively;
Store the cylindrical shell (21) that stream unit (2) comprises sealing, first pipeline (210), second pipe (29), 3rd pipeline (28), 4th pipeline (27), first switch (25), second switch (24), 3rd switch (23), 4th switch (22) and water level mark pipe (26), cylindrical shell (21) is by the first pipeline (210), second pipe (29), 3rd pipeline (28), 4th pipeline (27) and the external world communicate, first pipeline (210), second pipe (29), 3rd pipeline (28), 4th pipeline (27) is respectively by the first switch (25), second switch (24), 3rd switch (23), 4th switch (22) realizes opening and closing,
The connecting relation of each unit is:
The output channel (1105) in the chamber of confluxing of boiler unit (1) with store the second switch (24) flowing unit (2) and connect, the outlet conduit (1107) of the cooling end of boiler unit (1) is connected by the input of switch with cooling unit (3), the inlet channel (1106) of the cooling end of boiler unit (1) is connected by the output of switch with cooling unit (3), the 3rd switch (23) storing stream unit (2) is connected by the input of pipeline with decompressing unit (4), the first switch (25) and the 4th switch (22) that store stream unit (2) connect with air.
2. a kind of equipment preparing concentrate according to claim 1, it is characterized in that described strip converges bar (1103) and is provided with the corresponding binding face of interior crown (1103a) with lid (1101), two sides perpendicular to binding face (1103a) are symmetrically arranged with first arc surface (1103b) of phase concave, the end face being parallel to binding face (1103a) is provided with second arc surface (1103c) of indent, spill proof edge (1103d) is formed between first arc surface (1103b) and the second arc surface (1103c), strip converges bar (1103) and top is provided with the first inclined plane (1103f) and the second inclined plane (1103e), first inclined plane (1103f) and the second inclined plane (1103e) angle are obtuse angle, second inclined plane (1103e) more converges to strip that the top of bar (1103) is close more to tilt to binding face (1103a), more to converging, the top of bar is close more to tilt to binding face (1103a) first inclined plane (1103f), second arc surface (1103c) extends to the second inclined plane (1103e), first arc surface (1103b) extends to the first inclined plane (1103f).
3. a kind of equipment preparing concentrate according to claim 1, it is characterized in that the monolateral cross section of described collector ring (1102) is for " L " shape, the base vertical of " L " is in the inner peripheral surface of upper cover (11), and the stile of " L " is parallel to the inner peripheral surface of upper cover (11).
4. a kind of equipment preparing concentrate according to claim 3, it is characterized in that the top of the inner spout of described output channel (1105) near the conflux bottom in chamber and the stile far below " L ", the bottom of described inlet channel (1106) is fixedly connected with the top of lid (1101), and the bottom of inlet channel (1106) is provided with multiple delivery port (1109).
5. a kind of equipment preparing concentrate according to claim 1, is characterized in that the top of described annular wafer (1104) reduces to the distance of the bottom surface of lid (1101) with the increase of diameter itself.
6. a kind of equipment preparing concentrate according to claim 1, when it is characterized in that described spacer pin (1402) coordinates with the front of sampling cavity (1405), motion bar (1403) is in pull-out location, and thieff hatch (1404) is positioned at the outside of matrix (1401); When spacer pin (1402) coordinates with the back side of sampling cavity (1405), motion bar (1403) is in insertion position, and thieff hatch (1404) is positioned at the inside of sampling cavity (1405).
7. a kind of equipment preparing concentrate according to claim 1, it is characterized in that described gas-permeable channels (1408) extends to the front of matrix (1401), the sampling cavity (1405) of sampling unit (14) is positioned at boiler, and handle (1406) is positioned at outside boiler.
8. a kind of equipment preparing concentrate according to claim 1, it is characterized in that described the first pipeline (210) is positioned at cylindrical shell (21) near bottom place, the inner spout of second pipe (29) is near the bottom of cylindrical shell (21) but higher than the inner spout of the first pipeline (210), the inner spout of the 3rd pipeline (28) and the inner spout of the 4th pipeline (27) are near the top of cylindrical shell (21), and second switch (24) and the 3rd switch (23) are fixedly connected by coupling block (20) and realize synchronization action.
9. a kind of equipment preparing concentrate according to claim 8, it is characterized in that described synchronization action is realized by following structure, have and the coupling block of switch knob respective profile (20), at its head and the tail two ends, respectively through hole is set, also through hole is set in the relevant position of switch knob simultaneously, coupling block (20) is arranged between two switch knobs, by two circular shafts (201), switch knob and coupling block (20) are connected, then by back-up ring, circular shaft (201), switch knob, coupling block (20) three are fixed.
CN201410708604.1A 2014-11-28 2014-11-28 Prepare the equipment of concentrate Active CN104399261B (en)

Priority Applications (16)

Application Number Priority Date Filing Date Title
CN201510800092.6A CN105396307A (en) 2014-11-28 2014-11-28 Concentrated solution preparation equipment through low pressure and low boiling point, and working method of equipment
CN201510796569.8A CN105289019A (en) 2014-11-28 2014-11-28 Equipment possessing boiler for preparing concentrated solution and working method thereof
CN201510794053.XA CN105363226A (en) 2014-11-28 2014-11-28 Concentrate preparation device with boiler and working method thereof
CN201410708604.1A CN104399261B (en) 2014-11-28 2014-11-28 Prepare the equipment of concentrate
CN201510796109.5A CN105457319A (en) 2014-11-28 2014-11-28 Concentrate preparing equipment provided with boiler
CN201510795785.0A CN105396306A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and using low pressure and low boiling point for preparation of concentrated solution
CN201510796688.3A CN105435475A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquor by utilizing low pressure and low boiling point and working method thereof
CN201510795711.7A CN105396305A (en) 2014-11-28 2014-11-28 Equipment using low pressure and low boiling point for preparation of concentrated solution
CN201510800437.8A CN105344118A (en) 2014-11-28 2014-11-28 Device with boiler for preparing concentrate
CN201510796496.2A CN105435474A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and used for preparing concentrated liquor by utilizing low pressure and low boiling point
CN201510799395.0A CN105413203A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquid through low pressure and low boiling point
AU2015100476A AU2015100476A4 (en) 2014-11-28 2015-04-14 Design method for concentrates preparation device
AU2015100475A AU2015100475A4 (en) 2014-11-28 2015-04-14 Concentrates preparation device
IES20150263A IES86678B2 (en) 2014-11-28 2015-08-11 Concentrates preparation device
IE20150242A IE86889B1 (en) 2014-11-28 2015-08-11 Concentrates preparation device
GB1520927.3A GB2536756B (en) 2014-11-28 2015-11-27 Concentrates preparation device

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CN201410708604.1A CN104399261B (en) 2014-11-28 2014-11-28 Prepare the equipment of concentrate

Related Child Applications (10)

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CN201510796569.8A Division CN105289019A (en) 2014-11-28 2014-11-28 Equipment possessing boiler for preparing concentrated solution and working method thereof
CN201510799395.0A Division CN105413203A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquid through low pressure and low boiling point
CN201510795711.7A Division CN105396305A (en) 2014-11-28 2014-11-28 Equipment using low pressure and low boiling point for preparation of concentrated solution
CN201510800092.6A Division CN105396307A (en) 2014-11-28 2014-11-28 Concentrated solution preparation equipment through low pressure and low boiling point, and working method of equipment
CN201510796496.2A Division CN105435474A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and used for preparing concentrated liquor by utilizing low pressure and low boiling point
CN201510796109.5A Division CN105457319A (en) 2014-11-28 2014-11-28 Concentrate preparing equipment provided with boiler
CN201510795785.0A Division CN105396306A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and using low pressure and low boiling point for preparation of concentrated solution
CN201510796688.3A Division CN105435475A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquor by utilizing low pressure and low boiling point and working method thereof
CN201510800437.8A Division CN105344118A (en) 2014-11-28 2014-11-28 Device with boiler for preparing concentrate
CN201510794053.XA Division CN105363226A (en) 2014-11-28 2014-11-28 Concentrate preparation device with boiler and working method thereof

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CN201510800092.6A Withdrawn CN105396307A (en) 2014-11-28 2014-11-28 Concentrated solution preparation equipment through low pressure and low boiling point, and working method of equipment
CN201510796109.5A Withdrawn CN105457319A (en) 2014-11-28 2014-11-28 Concentrate preparing equipment provided with boiler
CN201510796496.2A Withdrawn CN105435474A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and used for preparing concentrated liquor by utilizing low pressure and low boiling point
CN201510796688.3A Withdrawn CN105435475A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquor by utilizing low pressure and low boiling point and working method thereof
CN201410708604.1A Active CN104399261B (en) 2014-11-28 2014-11-28 Prepare the equipment of concentrate
CN201510796569.8A Withdrawn CN105289019A (en) 2014-11-28 2014-11-28 Equipment possessing boiler for preparing concentrated solution and working method thereof
CN201510795711.7A Withdrawn CN105396305A (en) 2014-11-28 2014-11-28 Equipment using low pressure and low boiling point for preparation of concentrated solution
CN201510800437.8A Withdrawn CN105344118A (en) 2014-11-28 2014-11-28 Device with boiler for preparing concentrate
CN201510794053.XA Withdrawn CN105363226A (en) 2014-11-28 2014-11-28 Concentrate preparation device with boiler and working method thereof
CN201510799395.0A Withdrawn CN105413203A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquid through low pressure and low boiling point
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CN201510800092.6A Withdrawn CN105396307A (en) 2014-11-28 2014-11-28 Concentrated solution preparation equipment through low pressure and low boiling point, and working method of equipment
CN201510796109.5A Withdrawn CN105457319A (en) 2014-11-28 2014-11-28 Concentrate preparing equipment provided with boiler
CN201510796496.2A Withdrawn CN105435474A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and used for preparing concentrated liquor by utilizing low pressure and low boiling point
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CN201510800437.8A Withdrawn CN105344118A (en) 2014-11-28 2014-11-28 Device with boiler for preparing concentrate
CN201510794053.XA Withdrawn CN105363226A (en) 2014-11-28 2014-11-28 Concentrate preparation device with boiler and working method thereof
CN201510799395.0A Withdrawn CN105413203A (en) 2014-11-28 2014-11-28 Equipment for preparing concentrated liquid through low pressure and low boiling point
CN201510795785.0A Withdrawn CN105396306A (en) 2014-11-28 2014-11-28 Equipment provided with boiler and using low pressure and low boiling point for preparation of concentrated solution

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CN114570043A (en) * 2022-03-17 2022-06-03 广东环美环保产业发展有限公司 Mother liquor drying evaporator

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CN101327407A (en) * 2007-06-20 2008-12-24 天津工业大学 Apparatus and method for evaporating and concentrating liquid
EP2233895A1 (en) * 2007-12-25 2010-09-29 OG Systems Limited Method and device for flow metering and for forming a fluid medium sample
CN103977579A (en) * 2014-06-01 2014-08-13 吉首大学 Proportional concentration and evaporation device
CN204233789U (en) * 2014-11-28 2015-04-01 厦门艾卓工业设计有限公司 Prepare the equipment of concentrate

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CN105344118A (en) 2016-02-24
CN104399261A (en) 2015-03-11
IES20150263A2 (en) 2016-06-01
CN105396307A (en) 2016-03-16
CN105435474A (en) 2016-03-30
IE86889B1 (en) 2018-04-04
IES86678B2 (en) 2016-07-27
CN105457319A (en) 2016-04-06
IE20150242A1 (en) 2016-06-01
AU2015100476A4 (en) 2015-05-14
CN105396306A (en) 2016-03-16
CN105435475A (en) 2016-03-30
GB201520927D0 (en) 2016-01-13
CN105289019A (en) 2016-02-03
CN105363226A (en) 2016-03-02
GB2536756B (en) 2017-11-22
AU2015100475A4 (en) 2015-05-14
CN105396305A (en) 2016-03-16
CN105413203A (en) 2016-03-23
GB2536756A (en) 2016-09-28

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