CN104381427A - Compound traditional Chinese medicine preservative, and preparation method and use thereof - Google Patents
Compound traditional Chinese medicine preservative, and preparation method and use thereof Download PDFInfo
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- CN104381427A CN104381427A CN201410544990.5A CN201410544990A CN104381427A CN 104381427 A CN104381427 A CN 104381427A CN 201410544990 A CN201410544990 A CN 201410544990A CN 104381427 A CN104381427 A CN 104381427A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 28
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- 230000002335 preservative effect Effects 0.000 title abstract description 12
- 150000001875 compounds Chemical class 0.000 title abstract 3
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- 239000000341 volatile oil Substances 0.000 claims abstract description 11
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- 239000000203 mixture Substances 0.000 claims description 35
- 239000007788 liquid Substances 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 28
- 235000009421 Myristica fragrans Nutrition 0.000 claims description 16
- 239000001702 nutmeg Substances 0.000 claims description 16
- 244000062241 Kaempferia galanga Species 0.000 claims description 10
- 235000013421 Kaempferia galanga Nutrition 0.000 claims description 10
- 244000132436 Myrica rubra Species 0.000 claims description 10
- 235000002594 Solanum nigrum Nutrition 0.000 claims description 10
- 210000000582 semen Anatomy 0.000 claims description 10
- WBYWAXJHAXSJNI-VOTSOKGWSA-M .beta-Phenylacrylic acid Natural products [O-]C(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-M 0.000 claims description 9
- WBYWAXJHAXSJNI-SREVYHEPSA-N Cinnamic acid Chemical compound OC(=O)\C=C/C1=CC=CC=C1 WBYWAXJHAXSJNI-SREVYHEPSA-N 0.000 claims description 9
- 241001251949 Xanthium sibiricum Species 0.000 claims description 9
- 235000013985 cinnamic acid Nutrition 0.000 claims description 9
- 229930016911 cinnamic acid Natural products 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 9
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 claims description 9
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- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 abstract 1
- 241000723347 Cinnamomum Species 0.000 abstract 1
- AXMVYSVVTMKQSL-UHFFFAOYSA-N UNPD142122 Natural products OC1=CC=C(C=CC=O)C=C1O AXMVYSVVTMKQSL-UHFFFAOYSA-N 0.000 abstract 1
- 150000001299 aldehydes Chemical class 0.000 abstract 1
- 229940117916 cinnamic aldehyde Drugs 0.000 abstract 1
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 abstract 1
- 235000017803 cinnamon Nutrition 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 abstract 1
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Abstract
The present invention discloses a compound Chinese traditional medicine preservative preparation method which consists of the following steps: firstly preparing the extract of traditional Chinese medicine, and then adding mixed Amomum kravanh powder, cinnamon aldehyde and Fructus xanthii essential oil into the extract. The weight of 1000 parts by mass of the traditional Chinese medicine extract is used as a basis, 10-30 parts by weight of Amomum kravanh powder, 1-5 parts by weight of cinnamic aldehyde and 1-5 parts by weight of Fructus xanthii essential oil are added into the extract. The compound Chinese traditional medicine preservative uses natural Chinese herbs as raw materials, thereby having no toxic and side effects and having a fragrant flavor, and vegetables and fruits preserved by the preservative need no special washing when being eaten. The preservative has a longer preservation time, can effectively reduce the occurrence of bad fruits and is especially suitable for the preservation of picked fruits in the process of storage and transportation and for the household food storage.
Description
Technical field
The invention belongs to the technical field of antistaling agent, be specifically related to a kind of herbal mixture antistaling agent, its preparation method and application thereof.
Background technology
At present, domesticly constantly work out various effective preservation method, larger contribution has been made to the quality of long-time fruit and vegetable preservation.Because conventional chemical preservative can have impact to health, and to environment etc., from natural Chinese medicinal herb material, therefore extract fresh-keeping for fruits and vegetables or the flesh of fish of active material, receive the extensive concern of people.The fresh-keeping advantage of Chinese herbal medicine has: toxicity is low or non-toxic, easily decomposes after entering human body, and nutritious etc.The appearance of Traditional Chinese medicine preservative, more determines the status of crude antistaling agent.There is abundant natural vegetable Chinese herbal medicine resource in China, provides good basis for developing safe and effective crude antistaling agent.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of preparation method of herbal mixture antistaling agent, and the inventive method adopts natural Chinese medicinal herb material to be that herbal mixture antistaling agent prepared by raw material, without any side effects, need not rinse especially time edible.Herbal mixture antistaling agent prepared by the present invention has longer fresh keeping time, effectively reduces the bad fruit rate of fruits and vegetables, is particularly suitable for orchard worker and plucks fresh-keeping and family's fruit-vegetable food keeping-freshness storage in rear storage and transport process.
It is as follows that the present invention solves the technical scheme that above-mentioned technology adopts:
A preparation method for herbal mixture antistaling agent, first prepares Chinese medical extract clear liquid, in described Chinese medical extract clear liquid, then adds nutmeg, cinnamic acid and achene of Siberian cocklebur essential oil be mixed with and obtain; Based on the weight of Chinese medical extract clear liquid described in 1000 mass parts, the addition of described nutmeg is 10-30 weight portion, and the addition of cinnamic acid is 1-5 weight portion, and the addition of achene of Siberian cocklebur essential oil is 1-5 weight portion.
Described Chinese medical extract clear liquid is prepared by the raw material of following weight portion: galangal 15-50 weight portion, black nightshade 20-60 weight portion, semen brassicae 20-50 weight portion, folium eucalypti 15-30 weight portion.
The concrete preparation method of described Chinese medical extract clear liquid is: each Chinese medicine takes and to be soaked in water respectively afterwards, then heats extraction, obtains each folk prescription decoction, and is merged by each folk prescription decoction, after filtration described Chinese medical extract clear liquid; When wherein each prescription side decocts, the water yield of use is the 5-10 times amount of corresponding folk prescription Chinese medicine respectively.
The concrete preparation method of described Chinese medical extract clear liquid can also be: each Chinese medicine weighs and merges into Chinese medicine composition, is soaked in water, then heats extraction, obtains described Chinese medical extract clear liquid after filtration; When wherein decocting, the water yield of use is the 5-10 times amount of described Chinese medicine composition.
Described nutmeg is that the superfine powder of beating is ground in cardamom oven dry afterwards.
Described nutmeg average diameter is less than 10 μm.
Relative to prior art, the present invention has following advantage:
1, the present invention adopts natural Chinese medicinal herb material to be that herbal mixture antistaling agent prepared by raw material, without any side effects, need not rinse especially time edible.
2, the herbal mixture antistaling agent that prepared by the present invention has longer fresh keeping time, effectively reduces the bad fruit rate of fruits and vegetables, is particularly suitable for orchard worker and plucks fresh-keeping and family's fruit-vegetable food keeping-freshness storage in rear storage and transport process.
3, herbal mixture antistaling agent preparation method of the present invention is simple, is easy to promote, and is particularly suitable for applying in wide rural area.
4, the herbal mixture antistaling agent prepared of the present invention is easy to use, only needs to be sprayed directly on fruits and vegetables or processed fish meat products just can reach fresh-keeping effect, convenient operation.
5, the present invention adopts specific Chinese medicine preparation, and fresh-keeping effect is remarkable.Owing to there is synergy between each traditional Chinese medicine ingredients, can effective antibacterial bacteriostatic, the eupnea that fruits and vegetables can be kept again to oppress, effectively prevents the loss of moisture, therefore can realize significant fresh-keeping effect.
6, the present invention is on the basis of Chinese medicine extract, add nutmeg, cinnamic acid and achene of Siberian cocklebur essential oil, on the one hand, the interphase interaction of these three kinds of compositions and Chinese medicine extract, improve the fresh-keeping effect of Chinese medicine extract, effectively extend storage stability and the validity of Traditional Chinese medicine preservative of the present invention on the other hand.
Detailed description of the invention
In order to understand content of the present invention better, be described further below in conjunction with specific embodiment.Should be understood that these embodiments only for the present invention is further described, and be not used in and limit the scope of the invention.In addition should be understood that, after having read content of the present invention, person skilled in art makes some nonessential change or adjustment to the present invention, still belongs to protection scope of the present invention.
1, the preparation of antistaling agent
The preparation of embodiment 1 herbal mixture antistaling agent of the present invention
The preparation of Chinese medical extract clear liquid:
Galangal 50g, with the water soaking 5-10 hour of 500g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of galangal is obtained;
Black nightshade 25g, with the water soaking 5-10 hour of 250g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of black nightshade is obtained;
Semen brassicae 25g, with the water soaking 5-10 hour of 250g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of semen brassicae is obtained;
Folium eucalypti 15g, with the water soaking 5-10 hour of 150g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of folium eucalypti is obtained;
Above-mentioned four kinds of folk prescription decoctions are merged, after filtration, obtains Chinese medical extract clear liquid.
Weigh the above-mentioned Chinese medical extract clear liquid of 1000g, add nutmeg 10g, cinnamic acid 1g, achene of Siberian cocklebur essential oil 1g; Shake up at a high speed, namely prepare herbal mixture antistaling agent of the present invention.
Described nutmeg is that the superfine powder of beating is ground in cardamom oven dry afterwards.
The preparation of embodiment 2 herbal mixture antistaling agent of the present invention
The preparation of Chinese medical extract clear liquid:
Galangal 15g, with the water soaking 5-10 hour of 125g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of galangal is obtained;
Black nightshade 50g, with the water soaking 5-10 hour of 400g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of black nightshade is obtained;
Semen brassicae 45g, with the water soaking 5-10 hour of 360g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of semen brassicae is obtained;
Folium eucalypti 25g, with the water soaking 5-10 hour of 200g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of folium eucalypti is obtained;
Above-mentioned four kinds of folk prescription decoctions are merged, after filtration, obtains Chinese medical extract clear liquid.
Weigh the above-mentioned Chinese medical extract clear liquid of 1000g, add nutmeg 30g, cinnamic acid 2.5g, achene of Siberian cocklebur essential oil 2.5g; Shake up at a high speed, namely prepare herbal mixture antistaling agent of the present invention.
Described nutmeg is that the superfine powder of beating is ground in cardamom oven dry afterwards.
The preparation of embodiment 3 herbal mixture antistaling agent of the present invention
The preparation of Chinese medical extract clear liquid:
Galangal 30g, with the water soaking 5-10 hour of 240g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of galangal is obtained;
Black nightshade 60g weight portion, with the water soaking 5-10 hour of 300g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of black nightshade is obtained;
Semen brassicae 50g, with the water soaking 5-10 hour of 250g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of semen brassicae is obtained;
Folium eucalypti 30g, with the water soaking 5-10 hour of 300g; Then by direct for soak boiled rear slow fire boiling 3-6 hour, the folk prescription decoction of folium eucalypti is obtained;
Above-mentioned four kinds of folk prescription decoctions are merged, after filtration, obtains Chinese medical extract clear liquid.
Weigh the above-mentioned Chinese medical extract clear liquid of 1000g, add nutmeg 10g, cinnamic acid 4g, achene of Siberian cocklebur essential oil 5g; Shake up at a high speed, namely prepare herbal mixture antistaling agent of the present invention.
Described nutmeg is that the superfine powder of beating is ground in cardamom oven dry afterwards.
2, preserve test
2.1 experimental situations and by the selection of fresh-keeping object
1) preserve test carries out respectively at the natural environment of four seasons spring, summer, autumn and winter Various Seasonal
2) isoperibol about 3-4 degree Celsius
3) by the selection of fresh-keeping object:
1. every heavily about 100g after green vegetables de-etiolation leaf;
2. the micro-Huang of banana is general blue or green without the every only heavily about 80g of scar
3. often only 250g is weighed without scar red fuji apple
4. strawberry field now plucks strawberry every part 100g
5. fresh harvesting every part, red bayberry 100g
6. without each heavy about 200g of scar pear
7. without hindering each heavy 300g of Huanghua Pear
8. fresh water big head kills rear boneless fillet every part about 100g
That 9. slaughtered the same day weighs 300g without bone pork every part
2.2 grouping experiment methods:
(1) fresh-keeping treating method: evenly spray medicament embodiment 1 product of the present invention by fresh-keeping article with sprayer;
(2) hold with following packaging respectively with the test articles of non-Preservation Treatment after Preservation Treatment:
1. ceramic fruit tray is naked puts;
2. blotting paper parcel;
3. PE preservative film parcel.
2.3 experimental result contrasts
1. pear and apple ten days under different environmental conditions, whether Preservation Treatment is not significantly distinguished, and therefore family's meaning is not quite fresh-keeping.But treated after 2 weeks, bad fruit rate will well below not process.Therefore, antistaling agent of the present invention has greater significance for the accumulating after orchard worker's harvesting.
2. the Huanghua Pear Ninth Heaven under different environmental conditions Preservation Treatment whether also obviously do not distinguish, then manifesting respectively after 11 days, is therefore also that accumulating meaning is greater than family's preservation.Wherein one group of 3 pear adopting PE preservative film to wrap up after spraying with medicament of the present invention, still intact after 180 days under refrigeration temperature constant state, and other groups occur from the tenth daystart just progressively has rotten scar.Rotten scar mark is there is in the refrigeration pears comprised without Preservation Treatment after 26 days.
3. green vegetables under identical condition, and through on average the delaying 3-5 days and start jaundice than not process of Preservation Treatment, rot in blade face.
4. banana is distinguished not obvious within seven days, and after Preservation Treatment, a longest banana just started to occur rotten vestige at about 36 days.And undressed respectively from the 11st day just well-done rotten, the longest one is also just well-done rotten at 29 days.
5. fresh water big head sheet, under similarity condition, through the delaying 2-6 days and start to go bad than not process of Preservation Treatment.
6. strawberry naked that put wrap up with blotting paper just had any different at the 4th day, undressed have three to six strawberry surface to have qualitative change.Put strawberry through Preservation Treatment naked and have one on 5th day, within the 6th day, have two, the 7th talent has more than three.More obvious with the contrast of PE preservative film parcel experiment, start there is envenomation than there is no prolongation five talent processed.
7. the naked ratio of being rivals in a contest of red bayberry, the bad fruit rate at the 3rd day without any process reaches more than 50%, through antistaling agent process reach the 6th talent 50% bad fruit rate.The experiment of PE preservative film parcel, not, antistaling agent sprays and the bad fruit rate at the 9th day of PE parcel just has 50%.
8. have peculiar smell to be produced as contrast without bone pork with pork, after Preservation Treatment, average energy extends 1-4 talent generation peculiar smell.
2.4 preserve test brief summaries
Antistaling agent process of the present invention is greater than for the meaning of fruit (apple and pears) accumulating that family is fresh-keeping deposits, and the fresh-keeping effect of red bayberry also has certain accumulating meaning.Other fresh-keeping meaning of fruits and vegetables family is greater than accumulating.Under temperature constant state, fresh-keeping effect is better, and effect is apparent that red bayberry most, is secondly fillet, pork and strawberry.
3, the stability experiment of antistaling agent
3.1 prepare Chinese medical extract clear liquid
Weigh following raw material: galangal 50g, black nightshade 25g, semen brassicae 25g, folium eucalypti 15g,
Above-mentioned four kinds of medicinal materials are merged, is soaked in water, then heats extraction, after filtration, obtain Chinese medical extract clear liquid; During decoction, the water yield of use is 10 times amount of described Chinese medicine composition.
Weigh the above-mentioned Chinese medical extract clear liquid of 1000g, for subsequent use.
Each Chinese medicine weighs and merges into Chinese medicine composition, is soaked in water, then heats extraction, obtains described Chinese medical extract clear liquid after filtration; When wherein decocting, the water yield of use is the 5-10 times amount of described Chinese medicine composition.
The grouping experiment of 3.2 additives
The following six kinds of antistaling agents of preparation:
Above-mentioned antistaling agent A-D is loaded on reagent bottle respectively, label A-D, and all seals, deposit in indoor temperature 25 DEG C.
Color and luster in process is deposited to above-mentioned antistaling agent and sediment is observed, has following result:
After depositing 60 days, in antistaling agent A-D, the color and luster of antistaling agent C is the most shallow, and sediment does not almost have; Antistaling agent D color and luster is the darkest; Antistaling agent B sediment is maximum.
After depositing 100 days, in antistaling agent A-D, it is the brightest to remain antistaling agent C, and color and luster is the most shallow.
3.3 effect experimental depositing rear antistaling agent
After depositing 100 days with 4 kinds of antistaling agents of preparation in 3.2, unpacking, then carries out safety effect experiment to the red bayberry that the same day plucks.Red bayberry is weighed pack low-temperature preservation respectively, observes and records cosmetic variation and the percentage of water loss of red bayberry.Do not adopt the red bayberry of any antistaling agent process as blank.Processing mode is: spray with sprayer Direct Uniform.
Percentage of water loss computing formula: the weight of percentage of water loss=(weight after initial weight-fresh-keeping)/initial.Red bayberry percentage of water loss and outward appearance as shown in the table:
Visible, antistaling agent C, after adding cinnamic acid, nutmeg and achene of Siberian cocklebur essential oil three kinds of materials, fresh-keeping effect significantly improves.
As mentioned above, just the present invention can be realized preferably.
Claims (10)
1. a preparation method for herbal mixture antistaling agent, is characterized in that, first prepares Chinese medical extract clear liquid, in described Chinese medical extract clear liquid, then adds nutmeg, cinnamic acid and achene of Siberian cocklebur essential oil be mixed with and obtain; Based on the weight of Chinese medical extract clear liquid described in 1000 mass parts, the addition of described nutmeg is 10-30 weight portion, and the addition of cinnamic acid is 1-5 weight portion, and the addition of achene of Siberian cocklebur essential oil is 1-5 weight portion.
2. the preparation method of a kind of herbal mixture antistaling agent according to claim 1, it is characterized in that, described Chinese medical extract clear liquid is prepared by the raw material of following weight portion: galangal 15-50 weight portion, black nightshade 20-60 weight portion, semen brassicae 20-50 weight portion, folium eucalypti 15-30 weight portion.
3. the preparation method of a kind of herbal mixture antistaling agent according to claim 1, it is characterized in that, the concrete preparation method of described Chinese medical extract clear liquid is: each Chinese medicine is soaked in water after weighing respectively, then extraction is heated, obtain each folk prescription decoction, and each folk prescription decoction is merged, obtain described Chinese medical extract clear liquid after filtration; When wherein each prescription side decocts, the water yield of use is the 5-10 times amount of corresponding folk prescription Chinese medicine respectively.
4. the preparation method of a kind of herbal mixture antistaling agent according to claim 1, it is characterized in that, the concrete preparation method of described Chinese medical extract clear liquid is: each Chinese medicine weighs and merges into Chinese medicine composition, is soaked in water, then heat extraction, after filtration, obtain described Chinese medical extract clear liquid; When wherein decocting, the water yield of use is the 5-10 times amount of described Chinese medicine composition.
5. the preparation method of a kind of herbal mixture antistaling agent according to claim 1-4 any one, is characterized in that, described nutmeg is that the superfine powder of beating is ground in cardamom oven dry afterwards.
6. the preparation method of a kind of herbal mixture antistaling agent according to claim 1-4 any one, is characterized in that, described nutmeg average diameter is less than 10 μm.
7. a herbal mixture antistaling agent, is characterized in that, adopts the method described in claim 1-6 any one to prepare.
8. the application of herbal mixture antistaling agent according to claim 7, is characterized in that, fresh-keeping for fruit-vegetable foods such as red bayberry, fillet, pork and strawberries.
9. the application of herbal mixture antistaling agent according to claim 7, is characterized in that, treats on fresh-keeping fruit-vegetable food, meat or fish described in being sprayed directly on by described herbal mixture antistaling agent.
10. for the preparation of a Chinese medical extract clear liquid for herbal mixture antistaling agent, it is characterized in that, be prepared from by the raw material of following parts by weight: galangal 15-50 weight portion, black nightshade 20-60 weight portion, semen brassicae 20-50 weight portion, folium eucalypti 15-30 weight portion.
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| CN106135396A (en) * | 2016-07-08 | 2016-11-23 | 黄云波 | A kind of anti-rotten Traditional Chinese medicinal spray in fruit and vegerable transport |
| CN106234560A (en) * | 2016-07-29 | 2016-12-21 | 张毅 | Cardamine urhaniana O.E.Schulz in food processing as the application in antistaling agent and method thereof |
| CN106509083A (en) * | 2016-10-11 | 2017-03-22 | 常州市鼎日环保科技有限公司 | Preparation method for fresh-keeping film coating agent for fruits |
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| CN114903080A (en) * | 2022-05-30 | 2022-08-16 | 中国热带农业科学院分析测试中心 | Alpinia katsumadai essential oil banana preservative and preservation method |
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| CN102310966A (en) * | 2010-07-01 | 2012-01-11 | 郑州大学 | Storage mildew-proof and moth-proof packaging hemp cloth and preparation method thereof |
| CN103238657A (en) * | 2013-05-22 | 2013-08-14 | 南通市德心食品有限公司 | Green and safe chilled pork preservative |
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2014
- 2014-10-15 CN CN201410544990.5A patent/CN104381427B/en not_active Expired - Fee Related
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| CN105028621A (en) * | 2015-08-27 | 2015-11-11 | 太仓市永发农场专业合作社 | Composite preservative of Hongmei apricot |
| CN106135396A (en) * | 2016-07-08 | 2016-11-23 | 黄云波 | A kind of anti-rotten Traditional Chinese medicinal spray in fruit and vegerable transport |
| CN106234560A (en) * | 2016-07-29 | 2016-12-21 | 张毅 | Cardamine urhaniana O.E.Schulz in food processing as the application in antistaling agent and method thereof |
| CN106509083A (en) * | 2016-10-11 | 2017-03-22 | 常州市鼎日环保科技有限公司 | Preparation method for fresh-keeping film coating agent for fruits |
| CN106857789A (en) * | 2017-02-28 | 2017-06-20 | 浦北县龙腾食品有限公司 | The preparation method of official's field grass carp piece |
| CN114903080A (en) * | 2022-05-30 | 2022-08-16 | 中国热带农业科学院分析测试中心 | Alpinia katsumadai essential oil banana preservative and preservation method |
| CN114903080B (en) * | 2022-05-30 | 2024-04-05 | 中国热带农业科学院分析测试中心 | Semen katsumadai essential oil banana preservative and preservation method |
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