CN104371828A - Equipment for extracting jasmine flower perfume essence and essential oil by adopting air current circulation method - Google Patents

Equipment for extracting jasmine flower perfume essence and essential oil by adopting air current circulation method Download PDF

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Publication number
CN104371828A
CN104371828A CN201410640845.7A CN201410640845A CN104371828A CN 104371828 A CN104371828 A CN 104371828A CN 201410640845 A CN201410640845 A CN 201410640845A CN 104371828 A CN104371828 A CN 104371828A
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essential oil
equipment
ice maker
circulation method
jasmine flower
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CN104371828B (en
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雷榜盛
雷宏师
雷宏卫
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)

Abstract

The invention relates to equipment for extracting jasmine flower perfume essence and essential oil by adopting an air current circulation method. The equipment for extracting the jasmine flower perfume essence and essential oil by adopting the air current circulation method is characterized by comprising a perfume essence collecting box and an ice maker, wherein the tops of the perfume essence collecting box and the ice maker are connected by virtue of a pipeline, an induced draft fan is arranged on the pipeline, the bottoms of the perfume essence collecting box and the ice maker are connected by virtue of a return pipe, a bamboo sieve shoe is arranged in the perfume essence collecting box, an insulating layer is arranged on the inner wall of the ice maker, a condensation box is arranged in the ice maker, a condensation pipe is arranged in the condensation box, one end of the condensation pipe is connected with a pipeline, the other end of the condensation pipe is connected with a condensation disk, and exhaust holes are formed in the top of the condensation pipe and the top of the condensation box. The equipment for extracting the jasmine flower perfume essence and the essential oil by adopting the air current circulation method has the characteristics of reasonable structural design, low production cost, safety, sanitation, high essential oil and perfume extraction efficiency and the like.

Description

Airflow circulation method extracts the equipment of jasmine flower perfume and essential oil
Technical field
The present invention relates to the extraction equipment of a kind of jasmine flower perfume and essential oil, be specifically related to the equipment that a kind of airflow circulation method extracts jasmine flower perfume and essential oil.
Background technology
The kind value area of the Flower of Arabian Jasmine of Heng County, Nanning and output all account for about 80% of the whole nation, and accounting for 60% of world's Flower of Arabian Jasmine output, produce nearly 100,000 tons of fresh Flower of Arabian Jasmine per year, is in repute " township of Flower of Arabian Jasmine ".Several jasmine concrete absolute oil manufacturers of the Flower of Arabian Jasmine industry of the Heng County mainly jasmine tea source mill of family more than 130, the industrial structure is comparatively simple, fully utilizes lower.
Flower of Arabian Jasmine elegant fragrance, its essential oil has obvious relaxation effect, rouses oneself neural system; Can also cough gently, nurse and improve skin elasticity, desalination striae of pregnancy and scar, thus price is very expensive.The method extracting Flower of Arabian Jasmine essential oil from Flower of Arabian Jasmine mainly contains: (1) fatty absorption method fat absorption method is with the essential oil grease absorption Flower of Arabian Jasmine, there is the simple advantage of production technique, but the segregation ratio of subsequent fine oil and grease is more difficult, generally be not separated further but use as balm, use range is restricted.(2) extraction adopts low boiling point solvent such as the organic solvents such as sherwood oil, hexane, pentane to soak Flower of Arabian Jasmine, and extraction obtains the mixture of essential oil and organic solvent, and then distillation removing organic solvent, obtains Flower of Arabian Jasmine essential oil.This method extract yield is high, and cost is low, but can cause organic easily residual, makes product fragrance pure not.(3) supercritical CO 2extraction process adopts supercritical CO 2 fluid to soak Flower of Arabian Jasmine, and extraction obtains Flower of Arabian Jasmine essential oil.Supercritical CO 2it is high that extraction process has yield, high quality, but due to supercritical CO 2fluid solvability is too strong, and the non-derived essential oil in Flower of Arabian Jasmine is also extracted out, as protein etc., makes product easy mildew in storage process, limits the range of application of products obtained therefrom.
Chinese Patent Application No. CN02152166.2 discloses a kind of New method for extracting jasmine oil, its method is the fresh Flower of Arabian Jasmine of blowing over layering placement with damp atmosphere, takes the aroma ingredients that Flower of Arabian Jasmine is distributed out of, then uses Capture by Sorbents, until Flower of Arabian Jasmine tells fragrant complete, then with overcritical extraction CO 2essential oil in extraction and recovery sorbent material, obtains pure Flower of Arabian Jasmine essential oil.The Flower of Arabian Jasmine essential oil quality that this method obtains is high, but to account for gas ingredients ratio very little for entrained air aroma ingredients out through moisture, sorbent material is except absorption aromatoising substance, also adsorb and account for most moisture content, thus a large amount of sorbent materials to be used, and products obtained therefrom water content is high, the follow-up water removal phase that needs just can obtain pure product.
At present, also the extraction equipment of some Flower of Arabian Jasmine essential oils is had to be that the fragrance of a flower pump spued by jasmine fresh flower by device of enfleuraging installs to pressurized vessel storage, squeezed the juice by the Flower of Arabian Jasmine slag telling perfume and be filtered into as clear as crystal colored juice, then flower juice and fragrance of a flower gas tank being put into press packet tinning is finished product.But this method efficiency is low, cost is high, is not suitable for scale operation.
Summary of the invention
The object of this invention is to provide that a kind of device structure is reasonable in design, production cost is low, equipment that safety and sanitation, essential oil and the high airflow circulation method of fragrant dew extraction efficiency extract jasmine flower perfume and essential oil.
The present invention is achieved in that
A kind of method flowing circulation method extraction jasmine flower perfume and essential oil, it is characterized in that: the equipment that the method that described airflow circulation method extracts jasmine flower perfume and essential oil adopts, comprise the fragrant case of collection and ice maker, the fragrant case of described collection is connected by pipeline with the top of ice maker, pipeline is provided with induced draft fan, collect fragrant case to be connected by return line with bottom ice maker, collect in fragrant case and be provided with bamboo screen frame (unit), described ice maker inwall is provided with thermal insulation layer, cooling cylinder is provided with in ice maker, prolong is provided with in cooling cylinder, one end of prolong is connected with pipeline, the other end is connected with condensate pans, the top of described prolong and the top of cooling cylinder are equipped with venting hole.
The fragrant chamber interior wall of above-described collection is provided with temperature measurer and moisture content tester.
Above-described bamboo screen frame (unit) is provided with bamboo sieve, and bamboo sieve is provided with sieve aperture.
Automatic temperature control device is provided with in above-described ice maker.
Above-described return line is provided with interchanger.
Above-described return line is also provided with compensation air pump.
The substantive distinguishing features that the present invention gives prominence to and significant progress are:
1, airflow circulation method of the present invention extracts the equipment of jasmine flower perfume and essential oil is obtain jasmine flower perfume and essential oil two kinds of products in the physical method extraction of normal temperature or low temperature at whole leaching process, organic solvent (sherwood oil etc.) is not adopted to extract, fragrance is pure, destruction is not produced to the nutritive value of jasmine flower perfume and essential oil, there is very high using value; Simultaneously Flower of Arabian Jasmine slag still can as the purposes of the aspect such as medicinal extract, feed after squeezing the juice, so started a new pattern in the comprehensive utilization of Flower of Arabian Jasmine, also has great meaning to the industrial structure improving Flower of Arabian Jasmine.
2, jasmine flower perfume and essential oil are directly liquid by condensation by the extraction equipment of jasmine flower perfume of the present invention and essential oil, 100 jin of Flower of Arabian Jasmine can extract 15 ~ 20 jin of jasmine flower perfume and essential oil, extraction efficiency is high, and the jasmine flower perfume of extraction and essential oil have pure natural jasmin; Conventional petroleum ether extraction produces jasmin quintessence oil, and sesame oil yield is thousandth point about five; Airflow circulation method of the present invention produces jasmin quintessence oil, and sesame oil yield is about 2/1000ths, and jasmin quintessence oil fragrance is pure, does not have organic solvent smell.
3, adopt equipment of the present invention to extract jasmine flower perfume and essential oil and need not add any additive and other auxiliary agents, jasmine flower perfume and extraction of essential oil cost low.
4, the device fabrication cost of airflow circulation method extraction jasmine flower perfume of the present invention and essential oil is lower, is convenient to suitability for industrialized production, has good market outlook.
5, the equipment of airflow circulation method extraction jasmine flower perfume of the present invention and essential oil is provided with temperature automatically controlled, the wet system of control, and realize automatic production, energy consumption is low, and production efficiency is high.
Accompanying drawing explanation
Fig. 1 is the main TV structure schematic diagram that airflow circulation method of the present invention extracts the equipment of jasmine flower perfume and essential oil.
The component names that in figure, sequence number is relative:
Collect fragrant case 1, ice maker 2, bamboo screen frame (unit) 3, thermal insulation layer 4, condensate pans 5, prolong 6, cooling cylinder 7, automatic temperature control device 8, induced draft fan 9, pipeline 10, temperature measurer 11, moisture content tester 12, interchanger 13, return line 14, compensate air pump 15, venting hole 16.
Embodiment
Below in conjunction with drawings and Examples, the equipment that airflow circulation method of the present invention extracts jasmine flower perfume and essential oil is further described.
As shown in Figure 1, the equipment of airflow circulation method extraction jasmine flower perfume of the present invention and essential oil comprises the fragrant case 1 of collection, ice maker 2, bamboo screen frame (unit) 3, thermal insulation layer 4, condensate pans 5, prolong 6, cooling cylinder 7, automatic temperature control device 8, induced draft fan 9, pipeline 10, temperature measurer 11, moisture content tester 12, interchanger 13, return line 14, compensate air pump 15 and venting hole 16, the fragrant case 1 of described collection is connected by pipeline 10 with the top of ice maker 2, pipeline 10 is provided with induced draft fan 9, collect fragrant case 1 to be connected by return line 14 with bottom ice maker 2, collect in fragrant case 1 and be provided with bamboo screen frame (unit) 3, ice maker 2 inwall is provided with thermal insulation layer 4, cooling cylinder 7 is provided with in ice maker 2, prolong 6 is provided with in cooling cylinder 7, one end of prolong 6 is connected with pipeline 10, and the top of prolong 6 and the top of cooling cylinder 7 are equipped with venting hole 16, and the other end is connected with condensate pans 5, collect fragrant case 1 inwall and be provided with temperature measurer 11 and moisture content tester 12, described bamboo screen frame (unit) 3 is provided with bamboo sieve, and bamboo sieve is provided with sieve aperture, is provided with automatic temperature control device 8 in ice maker 2, described return line 14 is provided with interchanger 13, return line 14 is also provided with and compensates air pump 15.
Embodiment 1
(1) adopt the Flower of Arabian Jasmine of organic grow, select fine day to pluck afternoon bud large, without parasitosis, the measured jasmonic bud of matter;
(2), after plucking, with the large bamboo or wicker basket dress flower of ventilating, do not press during shipment, Flower of Arabian Jasmine can not be allowed to pile heating, and the indoor fresh organic jasmine flower flower bud being placed on 24 ~ 30 DEG C carry out growing flower 1 ~ 2 hour, open up into fragrance micro-excessive to Flower of Arabian Jasmine;
(3) be all spread out in by micro-for fragrance excessive Flower of Arabian Jasmine on bamboo sieve, bamboo screening layered is put on the shelf of the fragrant case of airtight collection, allow Flower of Arabian Jasmine naturally tell perfume (or spice), the temperature collecting fragrant case is 32 ~ 38 DEG C;
(4) when Flower of Arabian Jasmine starts to tell perfume (or spice), with induced draft fan, the fragrance of Flower of Arabian Jasmine in the fragrant case of collection and moisture are delivered in the ice maker condensate pans of refrigeration chamber, fragrance and moisture flow into cold dish after converging in prolong and being liquefied as the aqueous solution, air is discharged by the venting hole of cooling cylinder top and both sides, be circulated back in the fragrant case of collection, the temperature in ice maker is-15 ~-30 DEG C;
(5) collected in time in the stainless steel cylinder of sealing by the aqueous solution in cold dish, then the aqueous solution is isolated essential oil and lower floor's Flower of Arabian Jasmine perfume on upper strata, continuous flow circulation extraction time is 15 ~ 25 hours, completes until Flower of Arabian Jasmine tells fragrance.

Claims (6)

1. the equipment of an airflow circulation method extraction jasmine flower perfume and essential oil, it is characterized in that: the equipment that the method that described airflow circulation method extracts jasmine flower perfume and essential oil adopts, comprise the fragrant case of collection (1) and ice maker (2), the fragrant case (1) of described collection is connected by pipeline (10) with the top of ice maker (2), pipeline (10) is provided with induced draft fan (9), collect fragrant case (1) to be connected by return line (14) with ice maker (2) bottom, collect in fragrant case (1) and be provided with bamboo screen frame (unit) (3), described ice maker (2) inwall is provided with thermal insulation layer (4), cooling cylinder (7) is provided with in ice maker (2), prolong (6) is provided with in cooling cylinder (7), one end of prolong (6) is connected with pipeline (10), the other end is connected with condensate pans (5), the top of described prolong (6) and the top of cooling cylinder (7) are equipped with venting hole (16).
2. airflow circulation method according to claim 1 extracts the equipment of jasmine flower perfume and essential oil, it is characterized in that: fragrant case (1) inwall of described collection is provided with temperature measurer (11) and moisture content tester (12).
3. airflow circulation method according to claim 1 extracts the equipment of jasmine flower perfume and essential oil, it is characterized in that: described bamboo screen frame (unit) (3) is provided with bamboo sieve, and bamboo sieve is provided with sieve aperture.
4. airflow circulation method according to claim 1 extracts the equipment of jasmine flower perfume and essential oil, it is characterized in that: be provided with automatic temperature control device (8) in described ice maker (2).
5. airflow circulation method according to claim 1 extracts the equipment of jasmine flower perfume and essential oil, it is characterized in that: described return line (14) is provided with interchanger (13).
6. airflow circulation method according to claim 1 extracts the equipment of jasmine flower perfume and essential oil, it is characterized in that: described return line (14) is also provided with and compensates air pump (15).
CN201410640845.7A 2014-11-14 2014-11-14 Circulation of air flow method extracts the equipment of jasmine flower perfume and quintessence oil Active CN104371828B (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105695100A (en) * 2016-02-29 2016-06-22 广西壮族自治区分析测试研究中心 Method for producing jasmine flower hydrolat through filler absorption and equipment thereof
CN107460058A (en) * 2017-09-04 2017-12-12 河南省明天食品有限公司 A kind of extraction equipment and its extracting process of orange osmanthus flower essential oil
CN108219957A (en) * 2018-02-05 2018-06-29 浦江县晶富农业科技有限公司 Rose Essentielle collecting device with filter layer
CN108410619A (en) * 2018-05-30 2018-08-17 新疆农业大学 Rose champignon grape wine process equipment, rose champignon grape wine processing method and the grape wine of preparation
CN108504459A (en) * 2018-05-17 2018-09-07 无锡市鹅湖玫瑰园艺文化有限公司 A kind of Rosa Damascana pure dew extraction equipment
CN109207263A (en) * 2018-10-19 2019-01-15 福建农林大学 A method of makings flower essential oil is prepared by propylene glycol absorption method

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203247246U (en) * 2013-04-27 2013-10-23 中南林业科技大学 Device for collecting natural flowery essential oil
CN203545979U (en) * 2013-11-06 2014-04-16 谢大高 Jasmine essential oil production device

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203247246U (en) * 2013-04-27 2013-10-23 中南林业科技大学 Device for collecting natural flowery essential oil
CN203545979U (en) * 2013-11-06 2014-04-16 谢大高 Jasmine essential oil production device

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105695100A (en) * 2016-02-29 2016-06-22 广西壮族自治区分析测试研究中心 Method for producing jasmine flower hydrolat through filler absorption and equipment thereof
CN107460058A (en) * 2017-09-04 2017-12-12 河南省明天食品有限公司 A kind of extraction equipment and its extracting process of orange osmanthus flower essential oil
CN108219957A (en) * 2018-02-05 2018-06-29 浦江县晶富农业科技有限公司 Rose Essentielle collecting device with filter layer
CN108504459A (en) * 2018-05-17 2018-09-07 无锡市鹅湖玫瑰园艺文化有限公司 A kind of Rosa Damascana pure dew extraction equipment
CN108410619A (en) * 2018-05-30 2018-08-17 新疆农业大学 Rose champignon grape wine process equipment, rose champignon grape wine processing method and the grape wine of preparation
CN109207263A (en) * 2018-10-19 2019-01-15 福建农林大学 A method of makings flower essential oil is prepared by propylene glycol absorption method
CN109207263B (en) * 2018-10-19 2021-09-28 福建农林大学 Method for preparing airiness flower essential oil by propylene glycol adsorption method

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