CN104371212B - High-performance steel wire-wound hydraulic sebific duct novel high polymer mixing material - Google Patents
High-performance steel wire-wound hydraulic sebific duct novel high polymer mixing material Download PDFInfo
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- CN104371212B CN104371212B CN201410565028.XA CN201410565028A CN104371212B CN 104371212 B CN104371212 B CN 104371212B CN 201410565028 A CN201410565028 A CN 201410565028A CN 104371212 B CN104371212 B CN 104371212B
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- steel wire
- vulcanizing agent
- carbon black
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
- C08L27/02—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L27/04—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
- C08L27/06—Homopolymers or copolymers of vinyl chloride
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F16—ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
- F16L—PIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
- F16L11/00—Hoses, i.e. flexible pipes
- F16L11/04—Hoses, i.e. flexible pipes made of rubber or flexible plastics
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/18—Applications used for pipes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a kind of high-performance steel wire-wound hydraulic sebific duct novel high polymer mixing material, it is made up of the raw material of following parts by weight：6,420 15 20 parts of butyronitrile, 35 40 parts of alloy PVC, haloflex CM352F 30 40,1.5 2 parts of zinc oxide, 8 10 parts of magnesia, 1 1.5 parts of age resistor, 0 15 parts of silica 1,50 60 parts of carbon black, 24 parts of antiozonant, 25 35 parts of fine particle calcium carbonate, 30 40 parts of dibutyl ester, 1 1.5 parts of sulphur, 0.5 1 parts of accelerator CBS, 23 parts of vulcanizing agent P1682；Described antiozonant is microwax B10；Described carbon black is N330 carbon blacks；Described age resistor is N, N nickel dibutyl dithiocarbamates.The outer glue rubber mix material helps effect prepared by inventive formulation is to increase the pulse number of the product in use, improves the phenomenons such as outward appearance crackle, bubbling, improves the quality of product, increase the service life.
Description
Technical field
The present invention relates to rubber materials, more particularly to high-performance steel wire-wound hydraulic sebific duct macromolecule mixing material.
Background technology
Current oil, chemical industry, coal, mining industry, automobile, agricultural machinery, construction machinery industry, all a large amount of hydraulic drives of demand are soft
Pipe, flexible pipe is because its noise is low, transmission efficiency, softness, it is easy to install and by extensive use.Due to the hair of every profession and trade
Exhibition, requirement more and more higher of the market to hydraulic hose, pulse behaviors, durability to required flexible pipe are proposed higher want
Ask.According to the problem of discovery in producing in recent years and market survey, the outer colloidality of existing steel wire wound hydraulic hose is not enough, leads
Cause finished product hydralic hose pulse behaviors poor, while being also easy to produce the outer glue not phenomenon such as viscous, bubbling, outward appearance crackle, influence the product
Normally use.
The content of the invention
The technical problem to be solved in the present invention is that the outer colloidality of existing steel wire wound hydraulic hose is not enough, causes finished fluid
Moulding pipe pulse behaviors are poor, while the problems such as being also easy to produce not viscous outer glue, bubbling, outward appearance crackle, influences the normal of the product to use,
To solve the above problems, providing high-performance steel wire-wound hydraulic sebific duct macromolecule mixing material.
The purpose of the present invention is realized in the following manner：
High-performance steel wire-wound hydraulic sebific duct macromolecule mixing material, is made up of the raw material of following parts by weight：Butyronitrile 6420
15-20 parts, it is 35-40 parts of alloy PVC, haloflex CM352F 30-40,1.5-2 parts of zinc oxide, 8-10 parts of magnesia, anti-
Old agent 1-1.5 parts, 0-15 parts of silica 1,50-60 parts of carbon black, 2-4 parts of antiozonant, 25-35 parts of fine particle calcium carbonate, dioctyl ester 30-
40 parts, 1-1.5 parts of sulphur, 0.5-1 parts of accelerator CBS, 2-3 parts of vulcanizing agent T1682;Described antiozonant is microwax
B10。
Described carbon black is N330 carbon blacks.
Described age resistor is N, N- nickel dibutyl dithiocarbamates.
Relative to prior art, the present invention can solve the problem that existing because there is the outer colloidality of steel wire wound hydraulic hose not enough, be led
The finished product hydralic hose pulse behaviors of cause are poor, and be also easy to produce outer glue not glue, bubbling, outward appearance crackle the problems such as.Pass through the present invention
Outer glue rubber mix material helps effect prepared by formula is to increase the pulse number of the product in use, improves outward appearance
The phenomenons such as crackle, bubbling, improve the quality of product, increase the service life.
Embodiment
Embodiment 1：
High-performance steel wire-wound hydraulic sebific duct macromolecule mixing material, is made up of the raw material of following parts by weight：Butyronitrile 6420
15-20 parts, it is 35-40 parts of alloy PVC, haloflex CM352F 30-40,1.5-2 parts of zinc oxide, 8-10 parts of magnesia, anti-
Old agent 1-1.5 parts, 0-15 parts of silica 1,50-60 parts of carbon black, 2-4 parts of antiozonant, 25-35 parts of fine particle calcium carbonate, dioctyl ester 30-
40 parts, 1-1.5 parts of sulphur, 0.5-1 parts of accelerator CBS, 2-3 parts of vulcanizing agent T1682;Described antiozonant is microwax
B10；Described carbon black is N330 carbon blacks；Described age resistor is N, N- nickel dibutyl dithiocarbamates.
The present invention clicks step preparation：Each material is weighed by weight, is placed in banbury, 100oC-110 oC temperature
Under the conditions of, 8min-12min is kneaded, after the completion of mixing plus vulcanizing agent, is parked, parks more than 12h.Then heat refining, pressure are carried out
Go out, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire hydraulic sebific duct with outer glue novel high polymer mixing material.
Embodiment 2：
In the present embodiment, following raw material is weighed：Butyronitrile 642015kg, alloy PVC 35kg, haloflex CM352F
30 kg, the kg of zinc oxide 1.5, magnesia 8kg, N, the kg of N- nickel dibutyl dithiocarbamates 1, the kg of silica 10,
The kg of N330 carbon blacks 50, microwax B102 kg, the kg of fine particle calcium carbonate 25, the kg of dioctyl ester 30, the kg of sulphur 1, the kg of accelerator CBS 0.5,
The kg of vulcanizing agent T1682 2.
The material weighed up is placed in banbury, under 100oC temperature conditionss, 8min is kneaded, after the completion of mixing plus vulcanizing agent,
Parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire hydraulic
Sebific duct is with outer glue novel high polymer mixing material.
Embodiment 3：
In the present embodiment, following raw material is weighed：Butyronitrile 642017.5kg, alloy PVC 37.5kg, haloflex
The kg of CM352F 35, the kg of zinc oxide 1.75, magnesia 9kg, N, the kg of N- nickel dibutyl dithiocarbamates 1.25, dioxy
The kg of 12.5 kg, N330 carbon black of SiClx 55, microwax B103 kg, the kg of fine particle calcium carbonate 30, dioctyl ester 35kg, the kg of sulphur 1.25, rush
Enter the kg of agent CBS 0.75, the kg of vulcanizing agent T1682 2.5.
The material weighed up is placed in banbury, under 101oC temperature conditionss, 9min is kneaded, after the completion of mixing plus vulcanizing agent,
Parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire hydraulic
Sebific duct is with outer glue novel high polymer mixing material.
Embodiment 4：
In the present embodiment, following raw material is weighed：Butyronitrile 642020kg, alloy PVC40kg, haloflex CM352F
40 kg, the kg of zinc oxide 2, magnesia 10kg, N, the kg of N- nickel dibutyl dithiocarbamates 1.5, the kg of silica 15,
N330 carbon blacks 60kg, microwax B104 kg, the kg of fine particle calcium carbonate 35, dioctyl ester 40kg, the kg of sulphur 1.5, the kg of accelerator CBS 1, sulphur
The kg of agent T1682 3.
The material weighed up is placed in banbury, under 105oC temperature conditionss, 11min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 5：
In the present embodiment, following raw material is weighed：Butyronitrile 642016kg, alloy PVC36kg, haloflex CM352F
32kg, zinc oxide 1.6kg, magnesia 8.3kg, N, the kg of N- nickel dibutyl dithiocarbamates 1.1, silica 1 1kg,
N330 carbon blacks 52kg, microwax B102.3 kg, the kg of fine particle calcium carbonate 26, dioctyl ester 31kg, the kg of sulphur 1.1, accelerator CBS 0.6
Kg, the kg of vulcanizing agent T1682 2.1.
The material weighed up is placed in banbury, under 108oC temperature conditionss, 10min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 6：
In the present embodiment, following raw material is weighed：Butyronitrile 642018kg, alloy PVC37kg, haloflex CM352F
34kg, zinc oxide 1.7kg, magnesia 8.5kg, N, N- nickel dibutyl dithiocarbamates 1.3kg, silica 1 2kg,
N330 carbon blacks 54kg, microwax B102.1 kg, the kg of fine particle calcium carbonate 27, dioctyl ester 33kg, the kg of sulphur 1.2, accelerator CBS 0.7
Kg, the kg of vulcanizing agent T1682 2.3.
The material weighed up is placed in banbury, under 110oC temperature conditionss, 10min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 7：
In the present embodiment, following raw material is weighed：Butyronitrile 642017kg, alloy PVC38kg, haloflex CM352F
36kg, zinc oxide 1.9kg, magnesia 8.6kg, N, N- nickel dibutyl dithiocarbamates 1.4kg, silica 1 4kg,
N330 carbon blacks 56kg, microwax B102.5 kg, the kg of fine particle calcium carbonate 28, dioctyl ester 36kg, sulphur 1.4kg, accelerator CBS 0.9
Kg, the kg of vulcanizing agent T1682 2.4.
The material weighed up is placed in banbury, under 107oC temperature conditionss, 11min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 8：
In the present embodiment, following raw material is weighed：Butyronitrile 642019kg, alloy PVC39kg, haloflex CM352F
39kg, zinc oxide 1.8kg, magnesia 8.8kg, N, N- nickel dibutyl dithiocarbamates 1.2kg, silica 1 3kg,
N330 carbon blacks 58kg, microwax B102.7kg, fine particle calcium carbonate 29kg, dioctyl ester 32kg, sulphur 1.3kg, accelerator CBS 0.8kg, sulphur
The kg of agent T1682 2.6.
The material weighed up is placed in banbury, under 110oC temperature conditionss, 11min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 9：
In the present embodiment, following raw material is weighed：Butyronitrile 642019.7kg, alloy PVC39.5kg, haloflex
CM352F 31kg, the 75kg of zinc oxide 1., magnesia 9.1kg, N, N- nickel dibutyl dithiocarbamates 1.34kg, titanium dioxide
Silicon 11.5kg, N330 carbon black 59kg, microwax B102.8kg, fine particle calcium carbonate 31kg, dioctyl ester 39kg, sulphur 1.35kg, accelerator
CBS 0.56kg, vulcanizing agent T1682 2.9kg.
The material weighed up is placed in banbury, under 105oC temperature conditionss, 10min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 10：
In the present embodiment, following raw material is weighed：Butyronitrile 642018.6kg, alloy PVC35.6kg, haloflex
CM352F 33kg, zinc oxide 1.86kg, magnesia 9.3kg, N, N- nickel dibutyl dithiocarbamates 1.47kg, titanium dioxide
Silicon 13.7kg, N330 carbon black 51kg, microwax B103.1kg, fine particle calcium carbonate 33kg, dioctyl ester 37kg, sulphur 1.45kg, accelerator
CBS 0.95kg, vulcanizing agent T1682 2.8kg.
The material weighed up is placed in banbury, under 105oC temperature conditionss, 10min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 11：
In the present embodiment, following raw material is weighed：Butyronitrile 642017.4kg, alloy PVC38.6kg, haloflex
CM352F 37kg, zinc oxide 1.98kg, magnesia 9.4kg, N, N- nickel dibutyl dithiocarbamates 1.15kg, titanium dioxide
Silicon 14.6kg, N330 carbon black 53kg, microwax B103.4kg, fine particle calcium carbonate 34kg, dioctyl ester 38kg, sulphur 1.1kg, accelerator
CBS 0.77kg, vulcanizing agent T1682 2.7kg.
The material weighed up is placed in banbury, under 104oC temperature conditionss, 12min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 12：
In the present embodiment, following raw material is weighed：Butyronitrile 642016.5kg, alloy PVC37.4kg, haloflex
CM352F 38kg, zinc oxide 1.55kg, magnesia 9.6kg, N, N- nickel dibutyl dithiocarbamates 1.28kg, titanium dioxide
Silicon 10.5kg, N330 carbon black 50.8kg, microwax B103.3kg, fine particle calcium carbonate 30.5kg, dioctyl ester 34kg, sulphur 1.18kg, rush
Enter agent CBS 0.66kg, vulcanizing agent T1682 2.2kg.
The material weighed up is placed in banbury, under 109oC temperature conditionss, 12min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 13：
In the present embodiment, following raw material is weighed：Butyronitrile 642015.4kg, alloy PVC36.7kg, haloflex
CM352F 30.5kg, zinc oxide 1.67kg, magnesia 9.5kg, N, N- nickel dibutyl dithiocarbamates 1.43kg, dioxy
SiClx 10.8kg, N330 carbon black 57kg, microwax B103.5kg, fine particle calcium carbonate 27.5kg, dioctyl ester 33.7kg, sulphur 1.28kg,
Accelerator CBS 0.85kg, vulcanizing agent T1682 2.1kg.
The material weighed up is placed in banbury, under 104oC temperature conditionss, 8min is kneaded, after the completion of mixing plus vulcanizing agent,
Parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire hydraulic
Sebific duct is with outer glue novel high polymer mixing material.
Embodiment 14：
In the present embodiment, following raw material is weighed：Butyronitrile 642018.3kg, alloy PVC38.2kg, haloflex
CM352F 35.6kg, zinc oxide 1.62kg, magnesia 9.9kg, N, N- nickel dibutyl dithiocarbamates 1.37kg, dioxy
SiClx 12.8kg, N330 carbon black 55.7kg, microwax B103.7kg, fine particle calcium carbonate 33.6kg, dioctyl ester 38.2kg, sulphur
1.43kg, accelerator CBS 0.91kg, vulcanizing agent T1682 2.4kg.
The material weighed up is placed in banbury, under 107oC temperature conditionss, 11min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
Embodiment 15：
In the present embodiment, following raw material is weighed：Butyronitrile 642019.4kg, alloy PVC37.8kg, haloflex
CM352F 39.2kg, zinc oxide 1.93kg, magnesia 9.8kg, N, N- nickel dibutyl dithiocarbamates 1.18kg, dioxy
SiClx 13.9kg, N330 carbon black 58.8kg, microwax B103.9kg, fine particle calcium carbonate 29.4kg, dioctyl ester 34.6kg, sulphur
1.31kg, accelerator CBS 0.73kg, vulcanizing agent T1682 2.7kg.
The material weighed up is placed in banbury, under 106oC temperature conditionss, 10min is kneaded, mixing plus vulcanizing agent are completed
Afterwards, parked, park more than 12h.Then carry out heat refining, extrude, vulcanize 40 minutes in 150 oC and be molded, produce the steel wire liquid
The effective outer glue novel high polymer mixing material of moulding.
The present invention is as shown in the table with the performance comparison of outer glue mixing material with steel wire wound hydraulic hose before：
Claims (1)
1. high-performance steel wire-wound hydraulic sebific duct macromolecule mixing material, it is characterised in that：It is made up of the raw material of following parts by weight：
15-20 parts of butyronitrile 6420,35-40 parts of alloy PVC, haloflex CM352F 30-40,1.5-2 parts of zinc oxide, magnesia
8-10 parts, 1-1.5 parts of age resistor, 0-15 parts of silica 1,50-60 parts of carbon black, 2-4 parts of antiozonant, 25-35 parts of fine particle calcium carbonate,
30-40 parts of dioctyl ester, 1-1.5 parts of sulphur, 0.5-1 parts of accelerator CBS, 2-3 parts of vulcanizing agent T1682；Described antiozonant
For microwax B10；Described carbon black is N330 carbon blacks；Described age resistor is N, N- nickel dibutyl dithiocarbamates.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410565028.XA CN104371212B (en) | 2014-10-22 | 2014-10-22 | High-performance steel wire-wound hydraulic sebific duct novel high polymer mixing material |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410565028.XA CN104371212B (en) | 2014-10-22 | 2014-10-22 | High-performance steel wire-wound hydraulic sebific duct novel high polymer mixing material |
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| CN104371212A CN104371212A (en) | 2015-02-25 |
| CN104371212B true CN104371212B (en) | 2017-08-04 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105602040A (en) * | 2016-01-28 | 2016-05-25 | 漯河市邦威橡胶有限公司 | High-pressure braided-hose inner-layer rubber and preparing method thereof |
| CN105602042A (en) * | 2016-01-29 | 2016-05-25 | 漯河市邦威橡胶有限公司 | High-pressure braided-hose inner-layer rubber |
| CN106854301A (en) * | 2016-11-30 | 2017-06-16 | 东阳市朗晟橡塑有限公司 | A kind of multipurpose novel rubber tube and preparation method thereof |
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| JP2007269862A (en) * | 2006-03-30 | 2007-10-18 | Toyoda Gosei Co Ltd | Rubber composition and rubber hose for fuel system |
| CN101555327B (en) * | 2009-05-19 | 2011-01-26 | 天津鹏翎胶管股份有限公司 | Formulation of high-concentration ozone resistant rubber tube |
| CN102734571B (en) * | 2012-07-02 | 2014-07-02 | 漯河市利通橡胶有限公司 | Compact steel wire braided rubber hose and preparation method thereof |
| CN104100783B (en) * | 2013-04-12 | 2015-12-02 | 漯河市亿博橡胶科技有限公司 | A kind of ultrahigh pressure steel wire winding flexible pipe of composite material |
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Address after: The intersection of Luohe city in Henan province 462000 Yancheng District Longjiang road and State Road 107 west road south 500 meters Patentee after: Henan goodway Hydraulic Technology Co. Ltd. Address before: In Luohe city of Henan province 462300 Yancheng District Longjiang road and Taihang Road intersection angle Patentee before: LUOHE GUTEWEI RUBBER PRODUCTS CO., LTD. |
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Granted publication date: 20170804 Termination date: 20191022 |