CN104356452A - Method for preparing vibration damping rubber - Google Patents
Method for preparing vibration damping rubber Download PDFInfo
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- CN104356452A CN104356452A CN201410651270.9A CN201410651270A CN104356452A CN 104356452 A CN104356452 A CN 104356452A CN 201410651270 A CN201410651270 A CN 201410651270A CN 104356452 A CN104356452 A CN 104356452A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L9/00—Compositions of homopolymers or copolymers of conjugated diene hydrocarbons
- C08L9/06—Copolymers with styrene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
- C08J3/247—Heating methods
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a method for preparing vibration damping rubber. The method comprises the following steps of plastifying 100 parts (by weight) of styrene-butadiene rubber in a rubber mixing mill for 10-15 minutes, then, adding 20-60 parts (by weight) of silicon dioxide, 2-20 parts (by weight) of diethyl suberate, 1-4 parts (by weight) of anti-aging agent, 1-5 parts (by weight) of vulcanizing agent, 1-5 parts (by weight) of accelerant and 3-8 parts (by weight) of cross-linking agent, milling for 30-60 minutes at the temperature of 50-60 DEG C, carrying out extrusion molding, and vulcanizing for 50-60 minutes at the temperature of 130-140 DEG C, thereby obtaining the vibration damping rubber. Compared with the existing vibration damping rubber, the method disclosed by the invention has the advantage that the creep property of the rubber can be obviously improved.
Description
Technical field
The present invention relates to a kind of preparation method of vibration isolation rubber.
Background technology
For reducing vibration and the noise of motor vehicle, generally adopt vibration isolation rubber to reach this object, for this kind of vibration isolation rubber, there is good creep properties, otherwise will directly affect life-span and a machine safety of product, but the compressive creep index of existing vibration isolation rubber generally reaches 15-30%.
Summary of the invention
The technical problem to be solved in the present invention overcomes existing defect, provides a kind of preparation method of vibration isolation rubber.
In order to solve the problems of the technologies described above, the invention provides following technical scheme:
A preparation method for vibration isolation rubber, comprises the steps:
Plasticate styrene-butadiene rubber(SBR) 100 weight part on rubber mixing machine 10-15 minute, then silicon-dioxide 20-60 weight part is added, suberic acid diethyl ester 2-20 weight part, anti-aging agent 1-4 weight part, vulcanizing agent 1-5 weight part, promotor 1-5 weight part, linking agent 3-8 weight part, at 50-60 DEG C after mixing 30-60 minute, extrusion moulding, at 130-140 DEG C, sulfuration 50-60 minute, obtains vibration isolation rubber.
When mixing, also add protection wax 1-3 weight part and stearic acid 1-3 weight part.
Compared with existing vibration isolation rubber, the inventive method obtains the creep properties energy that obviously can improve rubber.
Embodiment
Below the preferred embodiments of the present invention are described, should be appreciated that preferred embodiment described herein is only for instruction and explanation of the present invention, is not intended to limit the present invention.
embodiment 1
By weight, after being plasticated on rubber mixing machine 10 minutes by 100 parts, styrene-butadiene rubber(SBR), then (specific surface area is 160-180m to add silicon-dioxide
2/ g) 20 parts, suberic acid diethyl ester 2 parts, antioxidant 4010NA 1 part, 1 part, sulphur, Vulcanization accelerator TMTD 1 part, 3 parts, linking agent zinc oxide, 1 part, protection wax paraffin and stearic acid 1 part, at 50 DEG C after mixing 50 minutes, extrusion moulding, sulfuration 50 minutes at 130 DEG C, obtain vibration isolation rubber, compressive creep index: 8%.
embodiment 2
By weight, after being plasticated on rubber mixing machine 15 minutes by 100 parts, styrene-butadiene rubber(SBR), then (specific surface area is 160-180m to add silicon-dioxide
2/ g) 60 parts, suberic acid diethyl ester 10 parts, antioxidant 4010NA 3 parts, 3 parts, sulphur, Vulcanization accelerator TMTD 4 parts, 5 parts, linking agent zinc oxide, 2 parts, protection wax paraffin and stearic acid 2 parts, at 55 DEG C after mixing 50 minutes, extrusion moulding, sulfuration 50 minutes at 140 DEG C, obtain vibration isolation rubber, compressive creep index: 8.5%.
embodiment 3
By weight, after being plasticated on rubber mixing machine 10 minutes by 100 parts, styrene-butadiene rubber(SBR), then (specific surface area is 160-180m to add silicon-dioxide
2/ g) 40 parts, suberic acid diethyl ester 20 parts, antioxidant 4010NA 4 parts, 5 parts, sulphur, Vulcanization accelerator TMTD 5 parts, 8 parts, linking agent zinc oxide, 1 part, protection wax paraffin and stearic acid 1 part, at 60 DEG C after mixing 50 minutes, extrusion moulding, sulfuration 60 minutes at 130 DEG C, obtain vibration isolation rubber, compressive creep index: 7.5%.
Compressive creep index is according to GB/T 19242-2003 standard detection.
Last it is noted that the foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, although with reference to previous embodiment to invention has been detailed description, for a person skilled in the art, it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (2)
1. a preparation method for vibration isolation rubber, comprises the steps:
Plasticate styrene-butadiene rubber(SBR) 100 weight part on rubber mixing machine 10-15 minute, then silicon-dioxide 20-60 weight part is added, suberic acid diethyl ester 2-20 weight part, anti-aging agent 1-4 weight part, vulcanizing agent 1-5 weight part, promotor 1-5 weight part, linking agent 3-8 weight part, at 50-60 DEG C after mixing 30-60 minute, extrusion moulding, at 130-140 DEG C, sulfuration 50-60 minute, obtains vibration isolation rubber.
2. the preparation method of vibration isolation rubber according to claim 1, is characterized in that, when mixing, add protection wax 1-3 weight part and stearic acid 1-3 weight part.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410651270.9A CN104356452A (en) | 2014-11-17 | 2014-11-17 | Method for preparing vibration damping rubber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410651270.9A CN104356452A (en) | 2014-11-17 | 2014-11-17 | Method for preparing vibration damping rubber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104356452A true CN104356452A (en) | 2015-02-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410651270.9A Pending CN104356452A (en) | 2014-11-17 | 2014-11-17 | Method for preparing vibration damping rubber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104356452A (en) |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102241843A (en) * | 2011-05-22 | 2011-11-16 | 浙江省天台祥和实业有限公司 | Composition for manufacturing shock pad on high-speed railway or bridge |
| CN103044730A (en) * | 2011-10-17 | 2013-04-17 | 青岛茂林橡胶制品有限公司 | Rubber-metal damping and buffering rubber sleeve and preparation method thereof |
| CN103242573A (en) * | 2013-05-14 | 2013-08-14 | 青岛宝丰盛福华进出口密封件有限公司 | Rubber damping gum cover and preparation method thereof |
| CN103539983A (en) * | 2013-09-18 | 2014-01-29 | 青岛博玉特橡塑制品有限公司 | Wear-resisting pressure-proof rubber shock-absorbing block |
| CN103539970A (en) * | 2013-09-18 | 2014-01-29 | 青岛博玉特橡塑制品有限公司 | High-temperature resistant rubber damping block |
| CN104098799A (en) * | 2014-06-18 | 2014-10-15 | 滁州天成有机硅高分子材料有限公司 | Shock-absorbing mixing rubber for cushion pad |
-
2014
- 2014-11-17 CN CN201410651270.9A patent/CN104356452A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102241843A (en) * | 2011-05-22 | 2011-11-16 | 浙江省天台祥和实业有限公司 | Composition for manufacturing shock pad on high-speed railway or bridge |
| CN103044730A (en) * | 2011-10-17 | 2013-04-17 | 青岛茂林橡胶制品有限公司 | Rubber-metal damping and buffering rubber sleeve and preparation method thereof |
| CN103242573A (en) * | 2013-05-14 | 2013-08-14 | 青岛宝丰盛福华进出口密封件有限公司 | Rubber damping gum cover and preparation method thereof |
| CN103539983A (en) * | 2013-09-18 | 2014-01-29 | 青岛博玉特橡塑制品有限公司 | Wear-resisting pressure-proof rubber shock-absorbing block |
| CN103539970A (en) * | 2013-09-18 | 2014-01-29 | 青岛博玉特橡塑制品有限公司 | High-temperature resistant rubber damping block |
| CN104098799A (en) * | 2014-06-18 | 2014-10-15 | 滁州天成有机硅高分子材料有限公司 | Shock-absorbing mixing rubber for cushion pad |
Non-Patent Citations (1)
| Title |
|---|
| 林孔勇等: "《橡胶工业手册 第六分册：工业橡胶制品》", 30 June 1995, article "《橡胶工业手册 第六分册：工业橡胶制品》" * |
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| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150218 |